HomeMy WebLinkAbout14- May, 28, 2014 Hydrocarbon Summary Allied EngineeringANALYTICAL SUMMARY REPORT ANALYTICAL SUMMARY REPORT ANALYTICAL SUMMARY REPORT ANALYTICAL SUMMARY REPORT
The analyses presented in this report were performed by Energy Laboratories, Inc., 3161 E. Lyndale Ave., Helena,
MT 59604, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory
Analytical Report, the QA/QC Summary Report, or the Case Narrative.
The results as reported relate only to the item(s) submitted for testing.
If you have any questions regarding these test results, please call.
Lab ID Client Sample ID Collect Date Receive Date Matrix Test
Report Approved By:
H14050122-001 S2-B @ 2.0'-3.5' 04/21/14 11:00 05/07/14 Soil EPH-Ultrasonic Extraction
Methanol Extraction for Volatiles
Hydrocarbons, Extractable
Petroleum-Scrn
Volatile Petroleum Hydrocarbons
Moisture
H14050122-002 S3-B @ 2.0'-3.5' 04/21/14 15:00 05/07/14 Soil Same As Above
H14050122-003 S5-B @ 2.0'-3.5' 04/24/14 10:00 05/07/14 Soil Same As Above
Allied Engineering Services Inc
Project Name: PDMC Site
Work Order: H14050122
32 S Discovery Dr
Bozeman, MT 59718-6958
May 28, 2014
Energy Laboratories Inc Helena MT received the following 3 samples for Allied Engineering Services Inc on 5/7/2014 for
analysis.
Page 1 of 21
Project: PDMC Site
CLIENT: Allied Engineering Services Inc
Work Order: H14050122 CASE NARRATIVE
05/28/14 Report Date:
Prep Comments for Sample H14050122-001A, Test HC-5035-VPH: The prep hold time was exceeded by 11.0 days.
Prep Comments for Sample H14050122-002A, Test HC-5035-VPH: The prep hold time was exceeded by 10.9 days.
Prep Comments for Sample H14050122-003A, Test HC-5035-VPH: The prep hold time was exceeded by 8.07 days.
Prep Comments for Sample H14050122-001A, Test HC-5035-VPH: The prep hold time was exceeded by 11.0 days.
Prep Comments for Sample H14050122-002A, Test HC-5035-VPH: The prep hold time was exceeded by 10.9 days.
Prep Comments for Sample H14050122-003A, Test HC-5035-VPH: The prep hold time was exceeded by 8.07 days.
Prep Comments for Sample H14050122-001A, Test HC-5035-VPH: The prep hold time was exceeded by 11.0 days.
Prep Comments for Sample H14050122-002A, Test HC-5035-VPH: The prep hold time was exceeded by 10.9 days.
Prep Comments for Sample H14050122-003A, Test HC-5035-VPH: The prep hold time was exceeded by 8.07 days.
Prep Comments for Sample H14050122-001A, Test HC-3550A-EPH: The prep hold time was exceeded by 10.9 days.
Prep Comments for Sample H14050122-002A, Test HC-3550A-EPH: The prep hold time was exceeded by 10.7 days.
Prep Comments for Sample H14050122-003A, Test HC-3550A-EPH: The prep hold time was exceeded by 7.96 days.
Prep Comments for Sample H14050122-001A, Test HC-3550A-EPH: The prep hold time was exceeded by 10.9 days.
Prep Comments for Sample H14050122-002A, Test HC-3550A-EPH: The prep hold time was exceeded by 10.7 days.
Prep Comments for Sample H14050122-003A, Test HC-3550A-EPH: The prep hold time was exceeded by 7.96 days.
Prep Comments for Sample H14050122-001A, Test HC-3550A-EPH: The prep hold time was exceeded by 10.9 days.
Prep Comments for Sample H14050122-002A, Test HC-3550A-EPH: The prep hold time was exceeded by 10.7 days.
Prep Comments for Sample H14050122-003A, Test HC-3550A-EPH: The prep hold time was exceeded by 7.96 days.
Prep Comments for Sample H14050122-001A, Test HC-5035-VPH: The prep hold time was exceeded by 11.0 days.
Prep Comments for Sample H14050122-002A, Test HC-5035-VPH: The prep hold time was exceeded by 10.9 days.
Prep Comments for Sample H14050122-003A, Test HC-5035-VPH: The prep hold time was exceeded by 8.07 days.
Prep Comments for Sample H14050122-001A, Test HC-3550A-EPH: The prep hold time was exceeded by 10.9 days.
Prep Comments for Sample H14050122-002A, Test HC-3550A-EPH: The prep hold time was exceeded by 10.7 days.
Prep Comments for Sample H14050122-003A, Test HC-3550A-EPH: The prep hold time was exceeded by 7.96 days.
Prep Comments for Sample H14050122-001A, Test HC-3550A-EPH: The prep hold time was exceeded by 10.9 days.
Prep Comments for Sample H14050122-002A, Test HC-3550A-EPH: The prep hold time was exceeded by 10.7 days.
Prep Comments for Sample H14050122-003A, Test HC-3550A-EPH: The prep hold time was exceeded by 7.96 days.
Prep Comments for Sample H14050122-001A, Test HC-5035-VPH: The prep hold time was exceeded by 11.0 days.
Prep Comments for Sample H14050122-002A, Test HC-5035-VPH: The prep hold time was exceeded by 10.9 days.
Prep Comments for Sample H14050122-003A, Test HC-5035-VPH: The prep hold time was exceeded by 8.07 days.
Prep Comments for Sample H14050122-001A, Test HC-5035-VPH: The prep hold time was exceeded by 11.0 days.
Prep Comments for Sample H14050122-002A, Test HC-5035-VPH: The prep hold time was exceeded by 10.9 days.
Prep Comments for Sample H14050122-003A, Test HC-5035-VPH: The prep hold time was exceeded by 8.07 days.
Prep Comments for Sample H14050122-001A, Test HC-3550A-EPH: The prep hold time was exceeded by 10.9 days.
Prep Comments for Sample H14050122-002A, Test HC-3550A-EPH: The prep hold time was exceeded by 10.7 days.
Prep Comments for Sample H14050122-003A, Test HC-3550A-EPH: The prep hold time was exceeded by 7.96 days.
Prep Comments for Sample H14050122-001A, Test HC-3550A-EPH: The prep hold time was exceeded by 10.9 days.
Prep Comments for Sample H14050122-002A, Test HC-3550A-EPH: The prep hold time was exceeded by 10.7 days.
Prep Comments for Sample H14050122-003A, Test HC-3550A-EPH: The prep hold time was exceeded by 7.96 days.
Prep Comments for Sample H14050122-001A, Test HC-3550A-EPH: The prep hold time was exceeded by 10.9 days.
Prep Comments for Sample H14050122-002A, Test HC-3550A-EPH: The prep hold time was exceeded by 10.7 days.
Prep Comments for Sample H14050122-003A, Test HC-3550A-EPH: The prep hold time was exceeded by 7.96 days.
Prep Comments for Sample H14050122-001A, Test HC-3550A-EPH: The prep hold time was exceeded by 10.9 days.
Prep Comments for Sample H14050122-002A, Test HC-3550A-EPH: The prep hold time was exceeded by 10.7 days.
Prep Comments for Sample H14050122-003A, Test HC-3550A-EPH: The prep hold time was exceeded by 7.96 days.
Prep Comments for Sample H14050122-001A, Test HC-3550A-EPH: The prep hold time was exceeded by 10.9 days.
Prep Comments for Sample H14050122-002A, Test HC-3550A-EPH: The prep hold time was exceeded by 10.7 days.
Prep Comments for Sample H14050122-003A, Test HC-3550A-EPH: The prep hold time was exceeded by 7.96 days.
Page 2 of 21
LABORATORY ANALYTICAL REPORT
Client: Allied Engineering Services Inc
Project: PDMC Site
Lab ID: H14050122-001
Client Sample ID: S2-B @ 2.0'-3.5'
Collection Date: 04/21/14 11:00
Matrix: Soil
Report Date: 05/28/14
DateReceived: 05/07/14
Prepared by Helena, MT Branch
Analyses Result Units Analysis Date / By RL Method
MCL/
QCL Qualifiers
PHYSICAL CHARACTERISTICS
05/10/14 15:32 / cmm 0.2 wt% 19.8 Moisture SW3550A
PETROLEUM HYDROCARBONS-VOLATILE
05/12/14 19:39 / kjw 0.12 mg/kg-dry ND Methyl tert-butyl ether (MTBE) MA-VPH 0.08
05/12/14 19:39 / kjw 0.062 mg/kg-dry ND Benzene MA-VPH 0.04
05/12/14 19:39 / kjw 0.062 mg/kg-dry ND Toluene MA-VPH 10
05/12/14 19:39 / kjw 0.062 mg/kg-dry ND Ethylbenzene MA-VPH 10
05/12/14 19:39 / kjw 0.062 mg/kg-dry ND m+p-Xylenes MA-VPH
05/12/14 19:39 / kjw 0.062 mg/kg-dry ND o-Xylene MA-VPH
05/12/14 19:39 / kjw 0.062 mg/kg-dry ND Xylenes, Total MA-VPH 30
05/12/14 19:39 / kjw 0.12 mg/kg-dry ND Naphthalene MA-VPH 9
05/12/14 19:39 / kjw 2.5 mg/kg-dry ND C9 to C10 Aromatics MA-VPH 100
05/12/14 19:39 / kjw 2.5 mg/kg-dry ND C5 to C8 Aliphatics MA-VPH 40
05/12/14 19:39 / kjw 2.5 mg/kg-dry ND C9 to C12 Aliphatics MA-VPH 90
05/12/14 19:39 / kjw 2.5 mg/kg-dry ND Total Purgeable Hydrocarbons MA-VPH 100
05/12/14 19:39 / kjw 70-130 %REC 85.0 Surr: VPH Aromatics Surrogate MA-VPH
05/12/14 19:39 / kjw 70-130 %REC 82.0 Surr: VPH Aliphatics Surrogate MA-VPH
- Note 1: The C5 to C8 Aliphatics value is corrected for aromatic constituents Benzene and Toluene.
- Note 2: The C9 to C12 Aliphatics value is corrected for aromatic constituents Ethylbenzene, m+p-Xylenes, o-Xylene and C9 to C10 Aromatics.
EXTRACTABLE PETROLEUM HYDROCARBONS-SCREEN ANALYSIS
*05/13/14 00:57 / jdh 25 mg/kg-dry 225 Total Extractable Hydrocarbons SW8015M 200
05/13/14 00:57 / jdh 40-140 %REC 94.0 Surr: o-Terphenyl SW8015M
- Note: Total Extractable Hydrocarbons are defined as the total hydrocarbon responses regardless of elution time.
- *=The reported value exceeds the Maximum Contaminant Limit (MCL). The MCLs listed for target analyte and hydrocarbon range values are the most
conservative Montana DEQ RBSLs. These limits may not apply to your samples.
Report
Definitions:
RL - Analyte reporting limit. MCL - Maximum contaminant level.
QCL - Quality control limit. ND - Not detected at the reporting limit.
* - The result exceeds the MCL.
Page 3 of 21
LABORATORY ANALYTICAL REPORT
Client: Allied Engineering Services Inc
Project: PDMC Site
Lab ID: H14050122-002
Client Sample ID: S3-B @ 2.0'-3.5'
Collection Date: 04/21/14 15:00
Matrix: Soil
Report Date: 05/28/14
DateReceived: 05/07/14
Prepared by Helena, MT Branch
Analyses Result Units Analysis Date / By RL Method
MCL/
QCL Qualifiers
PHYSICAL CHARACTERISTICS
05/10/14 15:32 / cmm 0.2 wt% 23.1 Moisture SW3550A
PETROLEUM HYDROCARBONS-VOLATILE
05/12/14 20:47 / kjw 0.13 mg/kg-dry ND Methyl tert-butyl ether (MTBE) MA-VPH 0.08
05/12/14 20:47 / kjw 0.065 mg/kg-dry ND Benzene MA-VPH 0.04
05/12/14 20:47 / kjw 0.065 mg/kg-dry ND Toluene MA-VPH 10
05/12/14 20:47 / kjw 0.065 mg/kg-dry ND Ethylbenzene MA-VPH 10
05/12/14 20:47 / kjw 0.065 mg/kg-dry ND m+p-Xylenes MA-VPH
05/12/14 20:47 / kjw 0.065 mg/kg-dry ND o-Xylene MA-VPH
05/12/14 20:47 / kjw 0.065 mg/kg-dry ND Xylenes, Total MA-VPH 30
05/12/14 20:47 / kjw 0.13 mg/kg-dry ND Naphthalene MA-VPH 9
05/12/14 20:47 / kjw 2.6 mg/kg-dry ND C9 to C10 Aromatics MA-VPH 100
05/12/14 20:47 / kjw 2.6 mg/kg-dry ND C5 to C8 Aliphatics MA-VPH 40
05/12/14 20:47 / kjw 2.6 mg/kg-dry ND C9 to C12 Aliphatics MA-VPH 90
05/12/14 20:47 / kjw 2.6 mg/kg-dry ND Total Purgeable Hydrocarbons MA-VPH 100
05/12/14 20:47 / kjw 70-130 %REC 83.0 Surr: VPH Aromatics Surrogate MA-VPH
05/12/14 20:47 / kjw 70-130 %REC 80.0 Surr: VPH Aliphatics Surrogate MA-VPH
- Note 1: The C5 to C8 Aliphatics value is corrected for aromatic constituents Benzene and Toluene.
- Note 2: The C9 to C12 Aliphatics value is corrected for aromatic constituents Ethylbenzene, m+p-Xylenes, o-Xylene and C9 to C10 Aromatics.
EXTRACTABLE PETROLEUM HYDROCARBONS-SCREEN ANALYSIS
*05/13/14 01:44 / jdh 13 mg/kg-dry 701 Total Extractable Hydrocarbons SW8015M 200
05/13/14 01:44 / jdh 40-140 %REC 105 Surr: o-Terphenyl SW8015M
- Note: Total Extractable Hydrocarbons are defined as the total hydrocarbon responses regardless of elution time.
- *=The reported value exceeds the Maximum Contaminant Limit (MCL). The MCLs listed for target analyte and hydrocarbon range values are the most
conservative Montana DEQ RBSLs. These limits may not apply to your samples.
Report
Definitions:
RL - Analyte reporting limit. MCL - Maximum contaminant level.
QCL - Quality control limit. ND - Not detected at the reporting limit.
* - The result exceeds the MCL.
Page 4 of 21
LABORATORY ANALYTICAL REPORT
Client: Allied Engineering Services Inc
Project: PDMC Site
Lab ID: H14050122-003
Client Sample ID: S5-B @ 2.0'-3.5'
Collection Date: 04/24/14 10:00
Matrix: Soil
Report Date: 05/28/14
DateReceived: 05/07/14
Prepared by Helena, MT Branch
Analyses Result Units Analysis Date / By RL Method
MCL/
QCL Qualifiers
PHYSICAL CHARACTERISTICS
05/10/14 15:32 / cmm 0.2 wt% 15.5 Moisture SW3550A
PETROLEUM HYDROCARBONS-VOLATILE
05/12/14 21:55 / kjw 0.12 mg/kg-dry ND Methyl tert-butyl ether (MTBE) MA-VPH 0.08
05/12/14 21:55 / kjw 0.059 mg/kg-dry ND Benzene MA-VPH 0.04
05/12/14 21:55 / kjw 0.059 mg/kg-dry ND Toluene MA-VPH 10
05/12/14 21:55 / kjw 0.059 mg/kg-dry ND Ethylbenzene MA-VPH 10
05/12/14 21:55 / kjw 0.059 mg/kg-dry ND m+p-Xylenes MA-VPH
05/12/14 21:55 / kjw 0.059 mg/kg-dry ND o-Xylene MA-VPH
05/12/14 21:55 / kjw 0.059 mg/kg-dry ND Xylenes, Total MA-VPH 30
05/12/14 21:55 / kjw 0.12 mg/kg-dry ND Naphthalene MA-VPH 9
J 05/12/14 21:55 / kjw 2.4 mg/kg-dry 2.1 C9 to C10 Aromatics MA-VPH 100
05/12/14 21:55 / kjw 2.4 mg/kg-dry ND C5 to C8 Aliphatics MA-VPH 40
J 05/12/14 21:55 / kjw 2.4 mg/kg-dry 0.83 C9 to C12 Aliphatics MA-VPH 90
05/12/14 21:55 / kjw 2.4 mg/kg-dry 2.7 Total Purgeable Hydrocarbons MA-VPH 100
05/12/14 21:55 / kjw 70-130 %REC 83.0 Surr: VPH Aromatics Surrogate MA-VPH
05/12/14 21:55 / kjw 70-130 %REC 81.0 Surr: VPH Aliphatics Surrogate MA-VPH
- Note 1: The C5 to C8 Aliphatics value is corrected for aromatic constituents Benzene and Toluene.
- Note 2: The C9 to C12 Aliphatics value is corrected for aromatic constituents Ethylbenzene, m+p-Xylenes, o-Xylene and C9 to C10 Aromatics.
EXTRACTABLE PETROLEUM HYDROCARBONS-SCREEN ANALYSIS
*05/13/14 03:17 / jdh 12 mg/kg-dry 231 Total Extractable Hydrocarbons SW8015M 200
05/13/14 03:17 / jdh 40-140 %REC 114 Surr: o-Terphenyl SW8015M
- Note: Total Extractable Hydrocarbons are defined as the total hydrocarbon responses regardless of elution time.
- *=The reported value exceeds the Maximum Contaminant Limit (MCL). The MCLs listed for target analyte and hydrocarbon range values are the most
conservative Montana DEQ RBSLs. These limits may not apply to your samples.
Report
Definitions:
RL - Analyte reporting limit. MCL - Maximum contaminant level.
QCL - Quality control limit. ND - Not detected at the reporting limit.
* - The result exceeds the MCL. J - Estimated value. The analyte was present but less
than the reporting limit.
Page 5 of 21
Project: PDMC Site
Client: Allied Engineering Services Inc
Work Order: H14050122
QA/QC Summary Report
05/28/14 Report Date:
Analyte Result %REC RPD Low Limit High Limit RPDLimit RL Units Qual
Prepared by Helena, MT Branch
Method: MA-VPH Batch: 24472
Lab ID: LCS-24472 05/12/14 11:50 Laboratory Control Sample Run: VARIAN1_140512A
2-Methylpentane 80 70 130 0.10 1.99 mg/kg-dry
n-Butylcyclohexane 85 70 130 2.12 mg/kg-dry
n-Decane 77 70 130 1.92 mg/kg-dry
n-Pentane 73 30 130 0.10 1.83 mg/kg-dry
Methyl tert-butyl ether (MTBE) 91 70 130 0.10 2.26 mg/kg-dry
Benzene 97 70 130 0.050 2.44 mg/kg-dry
Toluene 98 70 130 0.050 2.45 mg/kg-dry
Ethylbenzene 101 70 130 0.050 2.52 mg/kg-dry
m+p-Xylenes 106 70 130 0.050 5.29 mg/kg-dry
o-Xylene 104 70 130 0.050 2.60 mg/kg-dry
Naphthalene 91 70 130 0.10 2.27 mg/kg-dry
Total Purgeable Hydrocarbons 84 70 130 2.0 31.6 mg/kg-dry
Surr: VPH Aromatics Surrogate 98 70 130 0.050
Surr: VPH Aliphatics Surrogate 97 70 130 0.050
Lab ID: MB-24472 05/12/14 13:18 Method Blank Run: VARIAN1_140512A
Methyl tert-butyl ether (MTBE) 0.10 ND mg/kg-dry
Benzene 0.050 ND mg/kg-dry
Toluene 0.050 ND mg/kg-dry
Ethylbenzene 0.050 ND mg/kg-dry
m+p-Xylenes 0.050 ND mg/kg-dry
o-Xylene 0.050 ND mg/kg-dry
Naphthalene 0.10 ND mg/kg-dry
C9 to C10 Aromatics 2.0 ND mg/kg-dry
C5 to C8 Aliphatics 2.0 ND mg/kg-dry
C9 to C12 Aliphatics 2.0 ND mg/kg-dry
Total Purgeable Hydrocarbons 2.0 ND mg/kg-dry
Xylenes, Total 0.050 ND mg/kg-dry
Surr: VPH Aromatics Surrogate 94 70 130 0.050
Surr: VPH Aliphatics Surrogate 93 70 130 0.050
Lab ID: H14050119-022AMS 05/13/14 17:53 Sample Matrix Spike Run: VARIAN1_140513A
Methyl tert-butyl ether (MTBE) 88 70 130 0.13 2.86 mg/kg-dry
Benzene 93 70 130 0.065 3.03 mg/kg-dry
Toluene 94 70 130 0.065 3.06 mg/kg-dry
Ethylbenzene 97 70 130 0.065 3.14 mg/kg-dry
m+p-Xylenes 102 70 130 0.065 6.60 mg/kg-dry
o-Xylene 100 70 130 0.065 3.25 mg/kg-dry
Naphthalene 81 70 130 0.13 2.64 mg/kg-dry
Total Purgeable Hydrocarbons 75 70 130 2.6 36.7 mg/kg-dry
Surr: VPH Aromatics Surrogate 84 70 130 0.065
Surr: VPH Aliphatics Surrogate 82 70 130 0.065
Qualifiers:
RL - Analyte reporting limit. ND - Not detected at the reporting limit.
Page 6 of 21
Project: PDMC Site
Client: Allied Engineering Services Inc
Work Order: H14050122
QA/QC Summary Report
05/28/14 Report Date:
Analyte Result %REC RPD Low Limit High Limit RPDLimit RL Units Qual
Prepared by Helena, MT Branch
Method: MA-VPH Batch: 24472
Lab ID: H14050119-022AMSD 05/13/14 18:28 Sample Matrix Spike Duplicate Run: VARIAN1_140513A
Methyl tert-butyl ether (MTBE) 104 70 130 20 0.13 17 3.37 mg/kg-dry
Benzene 111 70 130 20 0.065 17 3.60 mg/kg-dry
Toluene 112 70 130 20 0.065 18 3.65 mg/kg-dry
Ethylbenzene 115 70 130 20 0.065 17 3.74 mg/kg-dry
m+p-Xylenes 120 70 130 20 0.065 16 7.77 mg/kg-dry
o-Xylene 119 70 130 20 0.065 17 3.85 mg/kg-dry
Naphthalene 114 70 130 20 0.13 34 3.70 mg/kg-dry R
Total Purgeable Hydrocarbons 89 70 130 20 2.6 17 43.4 mg/kg-dry
Surr: VPH Aromatics Surrogate 86 70 130 0.065
Surr: VPH Aliphatics Surrogate 82 70 130 0.065
Method: MA-VPH Analytical Run: R97036
Lab ID: CCV_0512GC203r-S 05/12/14 10:51 Continuing Calibration Verification Standard
1,2,4-Trimethylbenzene 99 75 125 0.10 2.48 mg/kg-dry
2,2,4-Trimethylpentane 95 75 125 0.10 2.38 mg/kg-dry
2-Methylpentane 94 75 125 0.10 2.35 mg/kg-dry
n-Butylcyclohexane 80 75 125 1.99 mg/kg-dry
n-Decane 77 75 125 1.93 mg/kg-dry
n-Pentane 96 75 125 0.10 2.41 mg/kg-dry
Methyl tert-butyl ether (MTBE) 94 75 125 0.10 2.36 mg/kg-dry
Benzene 97 75 125 0.050 2.43 mg/kg-dry
Toluene 97 75 125 0.050 2.41 mg/kg-dry
Ethylbenzene 99 75 125 0.050 2.47 mg/kg-dry
m+p-Xylenes 102 75 125 0.050 5.08 mg/kg-dry
o-Xylene 100 75 125 0.050 2.50 mg/kg-dry
Naphthalene 81 75 125 0.10 2.03 mg/kg-dry
Surr: VPH Aromatics Surrogate 87 70 130 0.050
Surr: VPH Aliphatics Surrogate 93 70 130 0.050
Qualifiers:
RL - Analyte reporting limit. ND - Not detected at the reporting limit.
R - RPD exceeds advisory limit.
Page 7 of 21
Project: PDMC Site
Client: Allied Engineering Services Inc
Work Order: H14050122
QA/QC Summary Report
05/28/14 Report Date:
Analyte Result %REC RPD Low Limit High Limit RPDLimit RL Units Qual
Prepared by Helena, MT Branch
Method: SW8015M Batch: 24462
Lab ID: MB-24462 05/12/14 18:46 Method Blank Run: HHP_140512A
Total Extractable Hydrocarbons 10 ND mg/kg-dry
Surr: o-Terphenyl 79 40 140 0.17
Lab ID: LCS-24462 05/12/14 19:33 Laboratory Control Sample Run: HHP_140512A
Total Extractable Hydrocarbons 104 60 140 10 215 mg/kg-dry
Surr: o-Terphenyl 110 40 140 0.17
Lab ID: H14050155-008AMS 05/14/14 19:31 Sample Matrix Spike Run: HHP_140514A
Total Extractable Hydrocarbons 67 60 140 11 149 mg/kg-dry
Surr: o-Terphenyl 73 40 140 0.18
Lab ID: H14050155-008AMSD 05/14/14 20:18 Sample Matrix Spike Duplicate Run: HHP_140514A
Total Extractable Hydrocarbons 81 60 140 20 11 19 181 mg/kg-dry
Surr: o-Terphenyl 79 40 140 0.18
Qualifiers:
RL - Analyte reporting limit. ND - Not detected at the reporting limit.
Page 8 of 21
Project: PDMC Site
Client: Allied Engineering Services Inc
Work Order: H14050122
QA/QC Summary Report
05/28/14 Report Date:
Analyte Result %REC RPD Low Limit High Limit RPDLimit RL Units Qual
Prepared by Helena, MT Branch
Method: SW8015M Analytical Run: R97095
Lab ID: CCV_0512GC111r-S 05/12/14 18:00 Continuing Calibration Verification Standard
n-Nonane 99 75 125 6.61 mg/kg-dry
n-Decane 100 75 125 6.66 mg/kg-dry
n-Dodecane 97 75 125 6.46 mg/kg-dry
n-Tetradecane 101 75 125 6.70 mg/kg-dry
n-Hexadecane 97 75 125 6.50 mg/kg-dry
n-Octadecane 98 75 125 6.55 mg/kg-dry
n-Nonadecane 99 75 125 6.60 mg/kg-dry
n-Eicosane 97 75 125 6.50 mg/kg-dry
n-Docosane 99 75 125 6.57 mg/kg-dry
n-Tetracosane 99 75 125 6.57 mg/kg-dry
n-Hexacosane 99 75 125 6.62 mg/kg-dry
n-Octacosane 101 75 125 6.71 mg/kg-dry
n-Triacontane 100 75 125 6.66 mg/kg-dry
n-Hexatriacontane 101 75 125 6.74 mg/kg-dry
Surr: o-Terphenyl 105 75 125 0.17
Lab ID: CCV_0512GC122r-S 05/13/14 02:30 Continuing Calibration Verification Standard
n-Nonane 98 75 125 6.53 mg/kg-dry
n-Decane 100 75 125 6.66 mg/kg-dry
n-Dodecane 99 75 125 6.58 mg/kg-dry
n-Tetradecane 106 75 125 7.04 mg/kg-dry
n-Hexadecane 100 75 125 6.64 mg/kg-dry
n-Octadecane 100 75 125 6.68 mg/kg-dry
n-Nonadecane 101 75 125 6.73 mg/kg-dry
n-Eicosane 100 75 125 6.64 mg/kg-dry
n-Docosane 101 75 125 6.71 mg/kg-dry
n-Tetracosane 101 75 125 6.71 mg/kg-dry
n-Hexacosane 101 75 125 6.74 mg/kg-dry
n-Octacosane 103 75 125 6.84 mg/kg-dry
n-Triacontane 102 75 125 6.77 mg/kg-dry
n-Hexatriacontane 102 75 125 6.83 mg/kg-dry
Surr: o-Terphenyl 107 75 125 0.17
Qualifiers:
RL - Analyte reporting limit. ND - Not detected at the reporting limit.
Page 9 of 21
S2-B @ 2.0'-3.5'Batch ID: 24462
EXTRACTABLE PETROLEUM HYDROCARBONS (EPH) SCREENING ANALYSIS CHROMATOGRAM
Sample Name: H14050122-001A ;0512GC1 , $HC-EPH-SCRN-S, ,(2,2)
Raw File: G:\Org\1GC\DAT\1GC051214_b\0512GC1.0020.RAW
Date & Time Acquired: 5/13/2014 12:57:53 AM
Method File: G:\Org\1GC\Methods\GC1_2014Methods\05121419.MET
Calibration File: G:\Org\1GC\Cals\GC1_2014CALS\SC011314F.CAL
Sample Weight: 24.1 Dilution: 4 S.A.: 1
Mean RF for C9 to C18 Hydrocarbons: 1856.84
Mean RF for C19 to C36 Hydrocarbons: 1896.267
Mean RF for Total Extractable Hydrocarbons: 1876.554
Rt range for Diesel Range Organics: 6.85 to 17.16
Rt range for C9 to C18 Hydrocarbons: 5.87 to 12.72
Rt range for C19 to C36 Hydrocarbons: 12.77 to 20.13
SURROGATE COMPOUND RT ACTUAL MEASURED %REC
*o-Terphenyl_____________12.822 8.299 7.804 94.03 -
*1-Chloro-octadecane_____13.61 8.299 7.81 94.12 -
DRO Area:538158.8 DRO Amount: 47.5984
TEH Area:2546789 TEH Amount: 225.2552
C9-C18 Area:19433.75 C9-C18 Amount: 1.737101
C19-C36 Area:1825821 C19-C36 Amount: 159.8091
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G:\Org\1GC\DAT\1GC051214_b\0512GC1.0020.RAW H14050122-001A ;0512GC1 , $HC-EPH-SCRN-S, ,(2,2)
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Page 10 of 21
S3-B @ 2.0'-3.5'Batch ID: 24462
EXTRACTABLE PETROLEUM HYDROCARBONS (EPH) SCREENING ANALYSIS CHROMATOGRAM
Sample Name: H14050122-002A ;0512GC1 , $HC-EPH-SCRN-S,
Raw File: G:\Org\1GC\DAT\1GC051214_b\0512GC1.0021.RAW
Date & Time Acquired: 5/13/2014 1:44:13 AM
Method File: G:\Org\1GC\Methods\GC1_2014Methods\05121421.MET
Calibration File: G:\Org\1GC\Cals\GC1_2014CALS\SC011314F.CAL
Sample Weight: 23.1 Dilution: 2 S.A.: 1
Mean RF for C9 to C18 Hydrocarbons: 1856.84
Mean RF for C19 to C36 Hydrocarbons: 1896.267
Mean RF for Total Extractable Hydrocarbons: 1876.554
Rt range for Diesel Range Organics: 6.85 to 17.16
Rt range for C9 to C18 Hydrocarbons: 5.87 to 12.72
Rt range for C19 to C36 Hydrocarbons: 12.77 to 20.13
SURROGATE COMPOUND RT ACTUAL MEASURED %REC
*o-Terphenyl_____________12.826 8.658 9.475 109.44 -
*1-Chloro-octadecane_____13.612 8.658 10.556 121.92 -
DRO Area:7005869 DRO Amount: 323.2354
TEH Area:1.51941E+07 TEH Amount: 701.0225
C9-C18 Area:105561.4 C9-C18 Amount: 4.922079
C19-C36 Area:1.328907E+07C19-C36 Amount: 606.7545
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G:\Org\1GC\DAT\1GC051214_b\0512GC1.0021.RAW H14050122-002A ;0512GC1 , $HC-EPH-SCRN-S,
0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30
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Page 11 of 21
S5-B @ 2.0'-3.5'Batch ID: 24462
EXTRACTABLE PETROLEUM HYDROCARBONS (EPH) SCREENING ANALYSIS CHROMATOGRAM
Sample Name: H14050122-003A ;0512GC1 , $HC-EPH-SCRN-S,
Raw File: G:\Org\1GC\DAT\1GC051214_b\0512GC1.0023.RAW
Date & Time Acquired: 5/13/2014 3:17:24 AM
Method File: G:\Org\1GC\Methods\GC1_2014Methods\05121414.MET
Calibration File: G:\Org\1GC\Cals\GC1_2014CALS\SC011314F.CAL
Sample Weight: 25.4 Dilution: 2 S.A.: 1
Mean RF for C9 to C18 Hydrocarbons: 1856.84
Mean RF for C19 to C36 Hydrocarbons: 1896.267
Mean RF for Total Extractable Hydrocarbons: 1876.554
Rt range for Diesel Range Organics: 6.85 to 17.16
Rt range for C9 to C18 Hydrocarbons: 5.87 to 12.72
Rt range for C19 to C36 Hydrocarbons: 12.77 to 20.13
SURROGATE COMPOUND RT ACTUAL MEASURED %REC
*o-Terphenyl_____________12.826 7.874 8.952 113.69 -
*1-Chloro-octadecane_____13.61 7.874 9.094 115.49 -
DRO Area:2483585 DRO Amount: 104.2112
TEH Area:5514989 TEH Amount: 231.4088
C9-C18 Area:36154.11 C9-C18 Amount: 1.533132
C19-C36 Area:4613991 C19-C36 Amount: 191.5903
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G:\Org\1GC\DAT\1GC051214_b\0512GC1.0023.RAW H14050122-003A ;0512GC1 , $HC-EPH-SCRN-S,
0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30
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Page 12 of 21
S2-B @ 2.0'-3.5' Batch ID: 24472
VPH AROMATICS PHOTOIONIZATION DETECTOR CHROMATOGRAM REPORT
Sample Name: H14050122-001A ;0512GC2 , $HC-VPH-MA-S,
Raw File: G:\Org\2GC\DAT\2GC051214_b\0512GC2.0017.RAW
Date & Time Acquired: 5/12/2014 7:39:11 PM
Method File: G:\Org\2GC\Methods\lavar042214.MET
Calibration File: G:\Org\2GC\Cals\Vhn042214.cal
Sample Weight: 50 Dilution: 1.25 S.A.: 1.25
Mean RF for C9 to C10 Aromatic Hydrocarbons: 420.4557
Rt range for C9 to C10 Aromatics: 14.566 to 20.099
Aromatic Hydrocarbon Range Area and Quantitation:
C9-C10 Aromatics Area:2304.129 C9-C10 Aromatics Amount: 0.1370019
TARGET ANALYTES RT CAL RRT RRT AREA AMOUNT FLAG
MTBE_____________________. . . .125 U
Benzene__________________7.194 7.194 7.194 97 .063 U
Toluene__________________10.068 10.068 10.068 315 .063 U
Ethylbenzene_____________13.506 13.506 13.506 99 .063 U
m+p-Xylenes______________13.65 13.65 13.65 441 .125 U
o-Xylene_________________14.446 14.446 14.446 155 .063 U
124-Trimethylbenzene_____16.498 16.498 16.498 334 .063 U
Naphthalene______________20.183 20.183 20.183 175 .125 U
SURROGATE COMPOUND RT ACTUAL MEASURED %REC QC LIMITS
**TRIFLUOROTOLUENE_______7.95 3.125 2.653 84.89 70-130
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G:\Org\2GC\DAT\2GC051214_b\0512GC2.0017.RAW H14050122-001A ;0512GC2 , $HC-VPH-MA-S,
0 2 4 6 8 10 12 14 16 18 20 22 24
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Page 13 of 21
S2-B @ 2.0'-3.5' Batch ID: 24472
VPH ALIPHATICS FLAME IONIZATION DETECTOR CHROMATOGRAM REPORT
Sample Name: H14050122-001A ;0512GC2 , $HC-VPH-MA-S,
Raw File: G:\Org\2GC\DAT\2GC051214_b\0512GC2B.0017.RAW
Date & Time Acquired: 5/12/2014 7:39:11 PM
Method File: G:\Org\2GC\Methods\lavar042214B.MET
Calibration File: G:\Org\2GC\Cals\Vhn042214B.cal
Sample Weight: 50 Dilution: 1.25 S.A.: 1.25
Mean RF for C5 to C8 Aliphatic Hydrocarbons: 431.8487
Mean RF for C9 to C12 Aliphatic Hydrocarbons: 338.7009
Mean RF for all calibrated compounds: 473.2145
Rt range for Gasoline Range Organics: 4.391 to 15.614
Rt range for C5 to C8 Aliphatic Hydrocarbons: 3.524 to 13.01
Rt range for C9 to C12 Aliphatic Hydrocarbons: 13.06 to 20.133
SURROGATE COMPOUND RT ACTUAL MEASURED %REC
**TFT_______________7.955 3.125 2.559 81.9 -
GRO Area:3264.992 GRO Amount: 0.1724901
TPH Area:7764.117 TPH Amount: 0.4101796
Aliphatic Hydrocarbon Areas and Quantitations uncorrected for Aromatics:
C5-C8 Area:2057.344 C5-C8 Amount: 0.119101
C9-C12 Area:5118.551 C9-C12 Amount: 0.3778076
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G:\Org\2GC\DAT\2GC051214_b\0512GC2B.0017.RAW H14050122-001A ;0512GC2 , $HC-VPH-MA-S,
0 2 4 6 8 10 12 14 16 18 20 22 24
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Page 14 of 21
S3-B @ 2.0'-3.5' Batch ID: 24472
VPH AROMATICS PHOTOIONIZATION DETECTOR CHROMATOGRAM REPORT
Sample Name: H14050122-002A ;0512GC2 , $HC-VPH-MA-S,
Raw File: G:\Org\2GC\DAT\2GC051214_b\0512GC2.0019.RAW
Date & Time Acquired: 5/12/2014 8:47:14 PM
Method File: G:\Org\2GC\Methods\lavar042214.MET
Calibration File: G:\Org\2GC\Cals\Vhn042214.cal
Sample Weight: 50 Dilution: 1.3 S.A.: 1.3
Mean RF for C9 to C10 Aromatic Hydrocarbons: 420.4557
Rt range for C9 to C10 Aromatics: 14.566 to 20.099
Aromatic Hydrocarbon Range Area and Quantitation:
C9-C10 Aromatics Area:1762.329 C9-C10 Aromatics Amount: 0.1089783
TARGET ANALYTES RT CAL RRT RRT AREA AMOUNT FLAG
MTBE_____________________. . . .13 U
Benzene__________________7.191 7.191 7.191 130 .065 U
Toluene__________________10.07 10.07 10.07 364 .065 U
Ethylbenzene_____________13.492 13.492 13.492 134 .065 U
m+p-Xylenes______________13.639 13.639 13.639 445 .13 U
o-Xylene_________________14.441 14.441 14.441 255 .065 U
124-Trimethylbenzene_____16.487 16.487 16.487 256 .065 U
Naphthalene______________20.174 20.174 20.174 163 .13 U
SURROGATE COMPOUND RT ACTUAL MEASURED %REC QC LIMITS
**TRIFLUOROTOLUENE_______7.943 3.25 2.685 82.62 70-130
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G:\Org\2GC\DAT\2GC051214_b\0512GC2.0019.RAW H14050122-002A ;0512GC2 , $HC-VPH-MA-S,
0 2 4 6 8 10 12 14 16 18 20 22 24
-1.0
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Page 15 of 21
S3-B @ 2.0'-3.5' Batch ID: 24472
VPH ALIPHATICS FLAME IONIZATION DETECTOR CHROMATOGRAM REPORT
Sample Name: H14050122-002A ;0512GC2 , $HC-VPH-MA-S,
Raw File: G:\Org\2GC\DAT\2GC051214_b\0512GC2B.0019.RAW
Date & Time Acquired: 5/12/2014 8:47:14 PM
Method File: G:\Org\2GC\Methods\lavar042214B.MET
Calibration File: G:\Org\2GC\Cals\Vhn042214B.cal
Sample Weight: 50 Dilution: 1.3 S.A.: 1.3
Mean RF for C5 to C8 Aliphatic Hydrocarbons: 431.8487
Mean RF for C9 to C12 Aliphatic Hydrocarbons: 338.7009
Mean RF for all calibrated compounds: 473.2145
Rt range for Gasoline Range Organics: 4.391 to 15.614
Rt range for C5 to C8 Aliphatic Hydrocarbons: 3.524 to 13.01
Rt range for C9 to C12 Aliphatic Hydrocarbons: 13.06 to 20.133
SURROGATE COMPOUND RT ACTUAL MEASURED %REC
**TFT_______________7.948 3.25 2.596 79.89 -
GRO Area:6862.773 GRO Amount: 0.3770639
TPH Area:11363.23 TPH Amount: 0.6243344
Aliphatic Hydrocarbon Areas and Quantitations uncorrected for Aromatics:
C5-C8 Area:5398.816 C5-C8 Amount: 0.3250426
C9-C12 Area:4649.277 C9-C12 Amount: 0.3568967
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G:\Org\2GC\DAT\2GC051214_b\0512GC2B.0019.RAW H14050122-002A ;0512GC2 , $HC-VPH-MA-S,
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Page 16 of 21
S5-B @ 2.0'-3.5' Batch ID: 24472
VPH AROMATICS PHOTOIONIZATION DETECTOR CHROMATOGRAM REPORT
Sample Name: H14050122-003A ;0512GC2 , $HC-VPH-MA-S,
Raw File: G:\Org\2GC\DAT\2GC051214_b\0512GC2.0021.RAW
Date & Time Acquired: 5/12/2014 9:55:22 PM
Method File: G:\Org\2GC\Methods\05121421$nap.MET
Calibration File: G:\Org\2GC\Cals\Vhn042214.cal
Sample Weight: 50 Dilution: 1.18 S.A.: 1.18
Mean RF for C9 to C10 Aromatic Hydrocarbons: 420.4557
Rt range for C9 to C10 Aromatics: 14.566 to 20.099
Aromatic Hydrocarbon Range Area and Quantitation:
C9-C10 Aromatics Area:19957.98 C9-C10 Aromatics Amount: 1.120233
TARGET ANALYTES RT CAL RRT RRT AREA AMOUNT FLAG
MTBE_____________________. . . .118 U
Benzene__________________7.19 7.19 7.19 77 .059 U
Toluene__________________10.049 10.049 10.049 295 .059 U
Ethylbenzene_____________13.474 13.474 13.474 139 .059 U
m+p-Xylenes______________13.634 13.634 13.634 556 .118 U
o-Xylene_________________14.432 14.432 14.432 204 .059 U
124-Trimethylbenzene_____16.483 -8.55 -8.545 751 .04 J
Naphthalene______________20.167 20.167 20.167 311 .118 U
SURROGATE COMPOUND RT ACTUAL MEASURED %REC QC LIMITS
**TRIFLUOROTOLUENE_______7.938 2.95 2.463 83.49 70-130
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G:\Org\2GC\DAT\2GC051214_b\0512GC2.0021.RAW H14050122-003A ;0512GC2 , $HC-VPH-MA-S,
0 2 4 6 8 10 12 14 16 18 20 22 24
-1.0
-0.5
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Page 17 of 21
S5-B @ 2.0'-3.5' Batch ID: 24472
VPH AROMATICS PHOTOIONIZATION DETECTOR CHROMATOGRAM REPORT
Sample Name: H14050122-003A ;0512GC2 , $HC-VPH-MA-S,
Raw File: G:\Org\2GC\DAT\2GC051214_b\0512GC2.0021.RAW
Date & Time Acquired: 5/12/2014 9:55:22 PM
Method File: G:\Org\2GC\Methods\05121421.MET
Calibration File: G:\Org\2GC\Cals\Vhn042214.cal
Sample Weight: 50 Dilution: 1.18 S.A.: 1.18
Mean RF for C9 to C10 Aromatic Hydrocarbons: 420.4557
Rt range for C9 to C10 Aromatics: 14.566 to 20.099
Aromatic Hydrocarbon Range Area and Quantitation:
C9-C10 Aromatics Area:37406.8 C9-C10 Aromatics Amount: 2.099628
TARGET ANALYTES RT CAL RRT RRT AREA AMOUNT FLAG
MTBE_____________________. . . .118 U
Benzene__________________7.19 7.19 7.19 77 .059 U
Toluene__________________10.049 10.049 10.049 295 .059 U
Ethylbenzene_____________13.474 13.474 13.474 139 .059 U
m+p-Xylenes______________13.634 13.634 13.634 556 .118 U
o-Xylene_________________14.432 14.432 14.432 204 .059 U
124-Trimethylbenzene_____16.483 -8.55 -8.545 944 .051 J
Naphthalene______________20.167 -12.234 -12.229 1499 .129
SURROGATE COMPOUND RT ACTUAL MEASURED %REC QC LIMITS
**TRIFLUOROTOLUENE_______7.938 2.95 2.463 83.49 70-130
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G:\Org\2GC\DAT\2GC051214_b\0512GC2.0021.RAW H14050122-003A ;0512GC2 , $HC-VPH-MA-S,
0 2 4 6 8 10 12 14 16 18 20 22 24
-1.0
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Page 18 of 21
S5-B @ 2.0'-3.5' Batch ID: 24472
VPH ALIPHATICS FLAME IONIZATION DETECTOR CHROMATOGRAM REPORT
Sample Name: H14050122-003A ;0512GC2 , $HC-VPH-MA-S,
Raw File: G:\Org\2GC\DAT\2GC051214_b\0512GC2b.0021.RAW
Date & Time Acquired: 5/12/2014 9:55:22 PM
Method File: G:\Org\2GC\Methods\05121421B.MET
Calibration File: G:\Org\2GC\Cals\Vhn042214B.cal
Sample Weight: 50 Dilution: 1.18 S.A.: 1.18
Mean RF for C5 to C8 Aliphatic Hydrocarbons: 431.8487
Mean RF for C9 to C12 Aliphatic Hydrocarbons: 338.7009
Mean RF for all calibrated compounds: 473.2145
Rt range for Gasoline Range Organics: 4.391 to 15.614
Rt range for C5 to C8 Aliphatic Hydrocarbons: 3.524 to 13.01
Rt range for C9 to C12 Aliphatic Hydrocarbons: 13.06 to 20.133
SURROGATE COMPOUND RT ACTUAL MEASURED %REC
**TFT_______________7.944 2.95 2.391 81.05 -
GRO Area:7794.773 GRO Amount: 0.3887384
TPH Area:54000.45 TPH Amount: 2.693093
Aliphatic Hydrocarbon Areas and Quantitations uncorrected for Aromatics:
C5-C8 Area:3437.02 C5-C8 Amount: 0.1878289
C9-C12 Area:42083.72 C9-C12 Amount: 2.932309
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0 2 4 6 8 10 12 14 16 18 20 22 24
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Page 19 of 21
Shipping container/cooler in good condition?
Custody seals intact on all shipping container(s)/cooler(s)?
Custody seals intact on all sample bottles?
Chain of custody present?
Chain of custody signed when relinquished and received?
Chain of custody agrees with sample labels?
Samples in proper container/bottle?
Sample containers intact?
Sufficient sample volume for indicated test?
All samples received within holding time?
(Exclude analyses that are considered field parameters
such as pH, DO, Res Cl, Sulfite, Ferrous Iron, etc.)
Container/Temp Blank temperature:
Water - VOA vials have zero headspace?
Water - pH acceptable upon receipt?
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
Yes
No
No
No
No
No
No
No
No
No
No
No
No
Not Present
Not Present
Not Present
No VOA vials submitted
Not Applicable
20.0°C No Ice
5/7/2014 Wanda Johnson
FedEx Overnight
wjj
Date Received:
Received by:
Login completed by:
Carrier
name:
BL2000\sdull
5/20/2014
Reviewed by:
Reviewed Date:
Contact and Corrective Action Comments:
Samples received in a plastic container & past the recommended analysis time. Jon Hager spoke with Lee Evans
regarding sample past hold & improper container. No collection time on sample containers. Wj 5/7/14
Temp Blank received in all shipping container(s)/cooler(s)? Yes No Not Applicable
Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as
pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time.
Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected,
data units are typically noted as –dry. For agricultural and mining soil parameters/characteristics, all samples are dried
and ground prior to sample analysis.
Standard Reporting Procedures:
Workorder Receipt Checklist
Allied Engineering Services Inc H14050122
Page 20 of 21
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