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Home My WebLink AboutA3. Res 4594 VillasPage 1 of 24 P-14051,City Commission Staff Report for the Villas Growth Policy Amendment NOTE: UPDATES TO THIS STAFF REPORT THAT HAVE BEEN MADE SINCE ITS PRESENTATION TO THE ZONING COMMISSION ARE SHOWN IN RED. Public Hearing Date: Planning Board April 21, 2015 City Commission May 11, 2015 Project Description: A growth policy amendment to revise Figure 3-1, the future land use map from Parks, Recreation and Open Space to Residential on 6.49 acres. Project Location: Located east of Manley Road, north of Turtle Way adjacent to the East Gallatin Recreation Area. The property is legally described as Section 31, Township 1S, Range 6E, C.O.S 157, Remaining Tract GLR-1, Gallatin County, Montana. Recommendation: Approval with contingencies to complete processing Recommended Motion: Having reviewed and considered the application materials, public comment, and all the information presented, I hereby adopt the findings presented in the staff report for Resolution 4594 a resolution of intent to amend the growth policy per application P-14051 and move to approve the growth policy amendment with contingencies and subject to all applicable code provisions. Report Date: April 29, 2015 Staff Contact: Chris Saunders Agenda Item Type: Action - Legislative EXECUTIVE SUMMARY Unresolved Issues None Project Summary The application seeks to change the Future Land Use Designation from Parks, Open Space & Recreation to Residential on 6.49 acres. The change is preparatory to a potential annexation and development. There are four primary public interests in considering the change from Parks, Open Space and Recreation to Residential in addition to the specific review criteria. 166 P-14051, City Commission Staff Report for The Villas Growth Policy Map Amendment Page 2 of 24 1) Maintaining the existing legal and physical vehicle and pedestrian access to the East Gallatin Recreation Area. 2) Protecting any future development on the site from any exposures to potential hazards resulting from the adjacent former solid waste facility. 3) Maintaining additional open space to expand the present East Gallatin Recreation Area. 4) Character of the area. As described in Section 4 of the report, the public issues may be addressed with or without the change to the future land use map. Staff concludes there is not a strong reason to choose one land use designation over the other unless the Commission makes a finding that the designation of private land as Park was an error. Recommendation in favor of the application is reflective of the general City culture of allowing private development and land control unless there is a strong basis rooted in the planning principles for not doing so. Alternatives 1. Approve the application with the recommended contingencies; 2. Approve the application with modifications to the recommended contingencies; 3. Deny the application based on the Commission’s findings of non-compliance with the applicable criteria contained within the staff report; or 4. Open and continue the public hearing on the application, with specific direction to staff or the applicant to supply additional information or to address specific items. Planning Board Action The Planning Board held their public hearing on April 21, 2015. There was public testimony from three persons received at the public hearing and two written public comments, which is summarized in the “Public Comment” section of this report. The link to the video recording of this public hearing can be found here http://media.avcaptureall.com/session.html?sessionid=b5c84dc7-c9a8-4bb0-b968- 6441bcc5444d. The Villas discussion begins at minute mark 2:17:30 of the recording. The Planning Board vote on the motion to recommend approval was 1:5 and the motion failed. TABLE OF CONTENTS EXECUTIVE SUMMARY ...................................................................................................... 1 Unresolved Issues ............................................................................................................... 1 Project Summary ................................................................................................................. 1 167 P-14051, City Commission Staff Report for The Villas Growth Policy Map Amendment Page 3 of 24 Alternatives ......................................................................................................................... 2 SECTION 1 - MAP SERIES .................................................................................................... 4 SECTION 2- RECOMMENDED CONTINGENCIES OF APPROVAL ................................ 9 SECTION 3 - RECOMMENDATIONS AND FUTURE ACTIONS ...................................... 9 SECTION 4 - STAFF ANALYSIS AND FINDINGS ........................................................... 10 Section 17.4, Bozeman Community Plan Amendment Criteria. ...................................... 10 APPENDIX A –AFFECTED ZONING AND GROWTH POLICY PROVISIONS ............. 15 APPENDIX B – DETAILED PROJECT DESCRIPTION AND BACKGROUND.............. 17 APPENDIX C – NOTICING AND PUBLIC COMMENT ................................................... 23 APPENDIX D - OWNER INFORMATION AND REVIEWING STAFF............................ 24 FISCAL EFFECTS ................................................................................................................. 24 ATTACHMENTS ................................................................................................................... 24 168 P-14051, City Commission Staff Report for The Villas Growth Policy Map Amendment Page 4 of 24 SECTION 1 - MAP SERIES 169 P-14051, City Commission Staff Report for The Villas Growth Policy Map Amendment Page 5 of 24 170 P-14051, City Commission Staff Report for The Villas Growth Policy Map Amendment Page 6 of 24 171 P-14051, City Commission Staff Report for The Villas Growth Policy Map Amendment Page 7 of 24 172 P-14051, City Commission Staff Report for The Villas Growth Policy Map Amendment Page 8 of 24 173 P-14051, City Commission Staff Report for The Villas Growth Policy Map Amendment Page 9 of 24 SECTION 2- RECOMMENDED CONTINGENCIES OF APPROVAL If the City Commission approves the application the following contingencies are recommended. Please note that these contingencies are necessary for the City to complete the processing of the proposed amendment. Recommended Contingencies of Approval: 1) The applicant shall submit, within forty-five (45) days of approval by the City Commission, an 8½- x 11-inch or 8½- x 14-inch exhibit entitled “The Villas Growth Policy Amendment” to the Department of Community Development containing an accurate description of the property for which the growth policy designation is being amended. The exhibit must be acceptable to the Department of Community Development. 2) The resolution for the growth policy amendment shall not be drafted until the applicant provides an exhibit of the area to be re-designated, which will be utilized in the preparation of the resolution to officially amend the Future Land Use Map of the Bozeman Community Plan. SECTION 3 - RECOMMENDATIONS AND FUTURE ACTIONS Project Name: The Villas Growth Policy Map Amendment File: Z-14051 Having considered the criteria established for a growth policy map amendment, the Staff recommends approval with contingencies for the application as submitted. The Development Review Committee (DRC) considered the amendment on November 5, 12&19, 2014, February 25, 2015, and March 4, 2015. The DRC recommended approval of the application with awareness that there may be required restrictions on the use of the property at time of development due to potential site contamination. See the attached comments from the Engineering division. The Recreation and Parks Advisory Board review committee considered the application on March 6, 2015. They did not oppose approval of the application so long as specific concerns were addressed. Their comments are attached to this report The Planning Board held a public hearing on this GPA on April 21, 2015 and recommend 1:5 to the City Commission that the application not be approved. The hearing will be held at 121 N. Rouse Avenue, Bozeman. The meeting will begin at 7 p.m. The City Commission will hold a public hearing on the growth policy map amendment on May 11, 2015. The hearing will be held at 121 N. Rouse Avenue, Bozeman. The meeting will begin at 6 p.m. 174 P-14051, City Commission Staff Report for The Villas Growth Policy Map Amendment Page 10 of 24 SECTION 4 - STAFF ANALYSIS AND FINDINGS In considering applications for approval under this title, the advisory boards and City Commission shall consider the following criteria. As an amendment is a legislative action, the Commission has broad latitude to determine a policy direction. The burden of proof that the application should be approved lies with the applicant. Few proposals are uniformly positive or negative in their effects. Especially in a legislative policy arena such as a growth policy amendment the legislative body must balance competing priorities and issues. The following criteria give guidance in evaluating a proposal. To reach a favorable decision on the proposed application the City Commission must find that the application meets all of criteria 1-4 and that the positive outcomes of the amendment outweigh negative outcomes. In making these findings, they may identify that there are some negative elements within a specific criteria but that on balance other elements outweigh the negative. Section 17.4, Bozeman Community Plan Amendment Criteria. 1. The proposed amendment must cure a deficiency in the growth policy, or improve the growth policy, to better respond to the needs of the general community; The term “deficiency” is not defined in the growth policy. The Merriam-Webster dictionary defines it as: “a lack of something that is needed; the state of not having enough of something necessary : a problem in the way something is made or formed”. The applicant asserts in his submittal that the change in designation will enable residential development necessary to address the expected growth of the community. It is true that Bozeman is expected to grow in population and will need additional housing. However, there are significant areas available for residential development which are expected to be adequate to meet the need. It is true that the application site could serve a residential function but no explanation of why this site is better than another already designated as Residential is provided. Therefore, staff does not find that the arguments made by the applicant persuasive. As described in Appendix B, the property has been included in the City’s long range planning documents for many years and the designation has changed during that time. As described in Appendix B, staff has not found direct evidence that the property was deliberately changed to Parks, Open Space, and Recreation to achieve a specific purpose. If the property was redesignated by error then the change to Residential would be a correction of a deficiency. Staff has identified four public concerns relating to the potential change to Residential. 1) Maintaining the existing legal and physical vehicle and pedestrian access to the East Gallatin Recreation Area. 2) Protecting any future development on the site from any exposure to potential hazards resulting from the adjacent former solid waste facility. 175 P-14051, City Commission Staff Report for The Villas Growth Policy Map Amendment Page 11 of 24 3) Maintaining additional open space to expand the present East Gallatin Recreation Area. 4) Character of the area. Consideration: 1) The right of way for the access road is an easement of record with the Gallatin County Clerk and Recorder’s office on a Certificate of Survey. It will remain regardless of the designation of the property on the future land use map. It is 60 feet in width, the standard size for a local street. That is wide enough to provide for two-way traffic, parking, and sidewalks on both sides. If the site were subdivided the right of way would become a dedication to the public. Therefore, it appears that the designation does not affect this public concern and there is no deficiency or improvement to be addressed. 2) The site is adjacent to an area to the east which was formerly used for a solid waste facility. There is some concern that there might be contamination on the site or it could migrate to the site. The record to date shows that sampling has occurred on several occasions since 1970. Results of the testing have shown either very low levels of contaminants or have been inconclusive. The MT Department of Environmental Quality sent a letter to the applicant’s representative which is part of the attached material. A recent set of testing has also been completed and is attached. Comments on this item from the Engineering Division of the City are attached. The City just received a new testing report dated April 30th which generally correlates with the sampling conducted by the application. See attached documentation. Regardless of the actual level of hazard quantified there remains the concern about potential hazards. Development of the site could potentially take many forms. Development or redevelopment of contaminated sites is not uncommon in the U.S. and there are well established protocols to mitigate potential hazards. Institutional controls are one such option. They are described by the EPA as “Institutional controls are non-engineered instruments, such as administrative and legal controls, that help minimize the potential for human exposure to contamination and/or protect the integrity of the remedy…ICs are used when contamination is first discovered, when remedies are ongoing and when residual contamination remains onsite at a level that does not allow for unlimited use and unrestricted exposure after cleanup.” Source: http://www.epa.gov/superfund/policy/ic/. Designation of the site as Park, Open Space, and Recreation on the future land use map is one institutional control as it affects the use of the site. Others may include required ventilation systems installed with constructed buildings. Exactly what institutional control is adequate is beyond the scope of this report and would require considerable additional technical study. If a development is proposed it would be appropriate to establish controls based on the nature of the proposed development and level of risk. Institutional controls need to be evaluated and applied as appropriate at the land use development application stage which could include annexation, subdivision, or site plan. However, it appears that the 176 P-14051, City Commission Staff Report for The Villas Growth Policy Map Amendment Page 12 of 24 change in designation does not affect this public concern and there is no deficiency or improvement to be made in the growth policy by the proposed change. 3) The site is privately owned. Designation as Park, Open Space, and Recreation Lands on the future land use map does not create any public right of use to the property. The property is presently zoned as industrial land within Gallatin County’s zoning system. No park dedication would be required if the property were developed for industrial uses. If the site were developed as residential uses, state law and local ordinance would require parkland to be set aside. The City of Bozeman park dedication requirement is .03 acres (1,307 sq. ft.) per dwelling. The amount of land provided by a future development will depend on the number of dwellings proposed. It is the responsibility of the City Commission to determine how and where that land dedication is provided. Any land dedication could be coordinated with the adjacent state owned park to create a better and more functional overall space. As noted under public concern one above and Appendix B, the public already has right of access from Manley Road to the East Gallatin Recreation Area. Any additional land would be able to be developed as functional recreational space. Therefore, if there is a public benefit to obtaining additional land the change to the future land use map to Residential would be beneficial and an improvement to the growth policy. 4) The area is in transition to urban uses. Areas to the south and east are annexed, publicly held and used for open space which is unlikely to change. Sewer and water services are available to adjacent areas west and north. Development has occurred as industrial uses west of Manley Road. The subdivision is approaching full build out. Adjacent property was approved within the last ten years as a urban density residential subdivision. A growth policy amendment was approved to enable this development. The property to the north is large lot unannexed residential. It is zoned under County authority as Agricultural Suburban. Therefore, residential development at urban density is not in conflict with the character of the area. There is a surface water connection from the outlet of the Glen Lake (East Gallatin Recreation Area) which is adjacent to or crosses this property. Regulations are in place to protect the watercourse and associated wetlands. The regulations establish minimum setbacks, restrictions on use of land within those setbacks, control of stormwater, and other standards. These, along with required park dedication requirements, will limit the home density able to be achieved on this site and will protect open spaces associated with the park. With the diversity and transition of uses already underway and the limitations of the site due to environmental constraints staff does not find that a change to Residential would conflict with the character of the area; but neither does it correct a deficiency or make a material improvement in the growth policy. Either Residential or Parks, Open Space and Recreational Lands would be consistent with the diverse uses in the area. Staff concludes there is not a 177 P-14051, City Commission Staff Report for The Villas Growth Policy Map Amendment Page 13 of 24 strong reason to choose one land use designation over the other unless the Commission makes a finding that the designation of private land as Park, Open Space, and Recreational Lands was an error as analyzed in Appendix B. Recommendation in favor of the application is reflective of the general City culture of allowing private development and land control unless there is a strong basis rooted in the planning principles for not doing so. 2. The proposed amendment does not create inconsistencies within the growth policy, either between the goals and the maps or between different goals and objectives. The application is for 6.49 acres. Given the size and location of the parcel, the overall effect on the growth policy is small. The proposed change does not alter the basic future land use map principals established in the growth policy and contained on pages 3-3 through 3-6. Review of any proposed development on this site will need to carefully consider the elements of natural amenities, sense of place, and sustainability. The Residential land use designation description in Section 3.4 includes the statement: “In limited instances the strong presence of constraints and natural features such as floodplains may cause an area to be designated for development at a lower density than normally expected within this category. All residential housing should be arranged with consideration of compatibility with adjacent development, natural constraints such as watercourses or steep slopes, and in a fashion which advances the overall goals of the Bozeman growth policy.” As discussed above in Criterion 1, issue 4, the proposed amendment is in a transitional area. The application materials propose several benefits that may occur due to the change. Some of these may be possible under either the existing or proposed designation. Staff has reviewed all the goals and objectives of the growth policy. The conclusion is that it does not appear that the application creates inconsistencies. 3. The proposed amendment must be consistent with the overall intent of the growth policy; The proposed change will not materially alter the desired land use pattern. The intent of the growth policy as expressed in Sections 1.2, 2.1, and 3.2 does not appear to be in conflict with the application. There are goals and objectives addressing and encouraging both residential development and park development. A balance must be made between both. On page 3-5 the growth policy states: “Density of development must also be balanced against community character, parks and open spaces, and the housing choices of citizens.” On page 3-17 the growth policy states: “Continued development of the community brings change. These changes will bring mutual costs and benefits, as well as some detriments and benefits from the actions of others which are felt more individually. In preparing and executing implementation it is important to preserve fairness and reasonableness. Regulations may be 178 P-14051, City Commission Staff Report for The Villas Growth Policy Map Amendment Page 14 of 24 expected to seek mitigation of substantial actual impacts, not minor or only perceived impact on preferences which are not supported by evidence. The established review criteria are an effort to provide balance and consideration for all the affected parties in the evaluation of development impacts. The use of public facilities in conformance with the standards and programs adopted by the City is not an unreasonable or burdensome impact of development. The City’s standards, while respectful of the community values and diversity of interests, will not yield outcomes which satisfy every person in each situation.” As discussed under Criterion 1, the public interests have been addressed. Therefore, the application appears to be consistent with the overall intent of the growth policy. 4. The proposed amendment will not adversely affect the community as a whole or significant portion by: Significantly altering land use patterns and principles in a manner contrary to those established by this plan, The requested Growth Policy Amendment will not significantly alter land use patterns and principles. Further discussion related to this criterion is presented under the analysis of the criteria above. Requiring unmitigated larger or more expensive improvements to streets, water, sewer, or other public facilities or services, thereby impacting development of other lands, The area is already served with water and sewer services. Public right of way is in place although some additional right of way for Manley Road would be required with the development process to meet the standards of the long range transportation plan. Exact required improvements would be identified through the development review process as would occur elsewhere in the community. Development of the site does not appear to require unmitigated improvements. Adversely impact existing uses because of unmitigated greater than anticipated impacts on facilities and services, No extraordinary impacts have been identified at this time. Additional review would occur during site development and mitigation of impact will be required. Development as a residential use has well documented impact levels. Negatively affect the livability of the area or the health and safety of the residents. This criterion needs to be applied to two different groups, the existing residents of the area and those who would be future residents of the application site after development. For existing residents the change to Residential would over time likely increase the number of homes with associated increased use of municipal services. It appears that capacity exists to serve the area so there should be no negative impacts. There would be incremental traffic increase but Manley Road is designated as a collector street and would be able to accommodate the additional vehicle trips. Therefore, there appears to be no negative impact 179 P-14051, City Commission Staff Report for The Villas Growth Policy Map Amendment Page 15 of 24 to the health and safety of the existing residents. Although it would be pleasant for the adjacent owners to have the property left open there can be no expectation that property will remain unoccupied unless it is legally reserved from development. A growth policy is by state law a non-regulatory document. Any future residential development will be subject to the same standards as other neighborhoods in the City. Those standards have been found by the City Commission to be adequate to protect against negative impacts. Future residents share many of the same potential health and safety issues as existing residents. The City’s development standards are adequate to address issues relating to availability of water, sewer, and other municipal services. The one element that would be unique to future residents is the concern regarding potential migration of possible contamination from the eastern property. That concern may be adequately addressed with future development through engineering design and institutional controls as discussed above. Therefore, it appears this criterion has been satisfied for future residents. APPENDIX A –AFFECTED ZONING AND GROWTH POLICY PROVISIONS Zoning Designation and Land Uses: The property is presently not annexed. Under the Gallatin County zoning the property is designed M-1, Light Industrial. The property is presently used for pasturing animals and is crossed by an access road to the East Gallatin Recreation Area. Adopted Growth Policy Designation: The following designations are applicable to this application. (Proposed) Residential. This category designates places where the primary activity is urban density dwellings. Other uses which complement residences are also acceptable such as parks, low intensity home based occupations, fire stations, churches, and schools. High density residential areas should be established in close proximity to commercial centers to facilitate the provision of services and employment opportunities to persons without requiring the use of an automobile. Implementation of this category by residential zoning should provide for and coordinate intensive residential uses in proximity to commercial centers. The residential designation indicates that it is expected that development will occur within municipal boundaries, which may require annexation prior to development. The dwelling unit density expected within this classification varies between 6 and 32 dwellings per net acre. A higher density may be considered in some locations and circumstances. A variety of housing types can be blended to achieve the desired density. Large areas of single type housing are discouraged. In limited instances the strong presence of constraints and natural features such as floodplains may cause an area to be designated for development at a lower density than normally expected within this category. All residential 180 P-14051, City Commission Staff Report for The Villas Growth Policy Map Amendment Page 16 of 24 housing should be arranged with consideration of compatibility with adjacent development, natural constraints such as watercourses or steep slopes, and in a fashion which advances the overall goals of the Bozeman growth policy. The residential designation is intended to provide the primary locations for additional housing within the planning area. (Existing) Parks, Open Space, and Recreational Lands. All publicly owned recreational lands, including parks, are included within this category, as well as certain private lands. These areas are generally open in character and may or may not be developed for active recreational purposes. This category includes conservation easements which may not be open for public use. The following excerpt from the growth policy describes the future land use map. 3.5 Future Land Use Map Figure 3-1 (pocket in back) is the future land use map for the Bozeman Community Plan. It is a synthesis of many different ideas, public input, existing conditions, and existing and desired land use patterns for the future. The map is the visual representation of the land use patterns and ideas discussed in this chapter, and elsewhere throughout this document. The map shows in a very broad manner acceptable uses and locations throughout the community. It does not represent a commitment by the City to approve every development proposed within each category. Neither does a designation indicate that a property is free from constraints to development The map and other elements of this plan must be weighed and evaluated in conjunction with the specific details of a proposed project which are beyond the scope of this plan but will be addressed through the implementation tools discussed in Chapter 16 and Appendix I. The provisions of any intergovernmental agreement between the City and County regarding land use will influence the final development pattern with the defined planning area. The boundaries shown on the map are of necessity at a large scale. As a result some interpretation may be required in the future. It is the intent of the map to follow natural and visible boundaries such as streams or right-of-ways where possible. Within developed areas, boundaries generally follow parcel boundaries established by recorded plats or certificates of survey. Where such natural or legal boundaries do not exist, some minor flexibility in the interpretation of the boundary is allowed to the Director of the Department of Planning and Community Development so long as the exercise of that flexibility is not contrary to the intent, purposes, or goals of this plan and does not materially alter the desired land pattern in an area. If significant alterations or modifications are desired, an amendment to this plan must be undertaken. 181 P-14051, City Commission Staff Report for The Villas Growth Policy Map Amendment Page 17 of 24 This plan looks at a twenty-year horizon as well as the current situation, so it is to be expected that some areas which are not in conformance with the plan will be identified. This plan recognizes the presence of these uses without specifically mapping or otherwise identifying them. It is desired that these anomalies be resolved over the term of this plan so that the land use pattern identified herein may be completed. APPENDIX B – DETAILED PROJECT DESCRIPTION AND BACKGROUND Project Description A proposal to change the Future Land Use Map, Figure 3-1, of the Bozeman Community Plan from Parks, Open Space, and Recreational Lands to Residential on 6.49 acres. Project Background The property is located north of the East Gallatin Recreation Area and east of Manley Road. The property is privately owned and the application for the change is signed by the land owner. The purpose of the amendment is to enable sale of the property for future development. The present designation of the property for future park uses appears to have occurred during the development of the Bozeman Community Plan which was adopted in 2009. Previously, the 1990 Master Plan showed the property as being in a transition area between Industrial and Park uses. Given the scale of the 1990 map now available it is difficult to clearly show the parcel, especially as individual property lines were not reliably shown on the map. The orange line shows Manley Road and the red donut is the application site in maps to follow. 182 P-14051, City Commission Staff Report for The Villas Growth Policy Map Amendment Page 18 of 24 1990 Master Plan Future Land Use Map Excerpt – “8” is industrial, “1” is park 183 P-14051, City Commission Staff Report for The Villas Growth Policy Map Amendment Page 19 of 24 As shown on this excerpt from the Bozeman 2020 Community Plan, the road alignment for Gallatin Park Drive which is to the west of Manley Road is north of the access road into the East Gallatin Recreation Area. The line of the future land use boundary appears to either be on the roadway or on the adjacent property line to the south with the subject property left as Future Urban. Bozeman 2020 Community Plan Future Land Use Map Excerpt – Blue is Industrial, green is Park/open space, light yellow (north) is Future Urban, and light green (east) is Public Institutions A current air photo of the area shows the roadway as described above. See below for the image. A review of the mapping for the adopted 2009 update of the growth policy shows the present boundary line for all versions of the map. Staff has reviewed minutes of the Planning Board meetings during the preparation of the plan and cannot find discussion of why this change was made. The present map is shown in Section 1 of this report. 184 P-14051, City Commission Staff Report for The Villas Growth Policy Map Amendment Page 20 of 24 Designation on a future land use map, as shown in growth policy excerpt Section 3.5 above, may reflect either existing uses or aspirations for use. At this time Staff has not been able to identify any specific Planning Board or City Commission discussion regarding the adoption of the future land use map in 2009 that would indicate whether the designation of the property was a deliberate act, a translation of the old difficult to read 1990 map which picked up an adjacent property, or an assumption that the subject property was supposed to be included with the larger open space tracts to the south and east. County designation Between the adoption of the 1990 and 2001 future land use maps the City-County planning program was dissolved. All non-annexed property transitioned to the sole control of Gallatin County for planning and zoning. Gallatin County largely retained the 1990 Master Plan for the county areas and readopted the associated zoning. This property with the new County zoning was designated as M-1. The following excerpt is from the 1999 zoning map which was adopted by the City prior to the dissolution of the joint planning area. The property boundaries are not clear. As before the general area of the application is identified with a red donut and Manley Road by an orange line. As shown here the former City zoning map indicates an M-2, Heavy Industry zone had been established on the property. The County did not change the zoning after the City adopted the 2009 growth policy. 185 P-14051, City Commission Staff Report for The Villas Growth Policy Map Amendment Page 21 of 24 The current future land use map is shown on page 4 of this report. Vicinity Land Use The property to the east is owned by the City of Bozeman. A solid waste disposal facility was operated there per the MT Department of Environmental Quality between 1962 and 1970. Use of the site is currently as open space supportive of the East Gallatin Recreation Area and providing a connection between the recreation area and the Bridger Creek Subdivision trail system. The site is approximately 47 acres and was leased to the MT Department of Fish, Wildlife, and Parks in 1985. The state was obligated to perform certain monitoring of the site as set forth in the lease. The application materials include a letter dated November 18, 2014 forwarding a report dated April 4, 1996 from the MT Department of Environmental Quality regarding monitoring and site improvement efforts that had been taken to that point. An updated site monitoring report was provided by the applicant dated January 13, 2015 prepared by Resource Technologies, Inc. Copies of both items are included in the application materials attached to this report. 186 P-14051, City Commission Staff Report for The Villas Growth Policy Map Amendment Page 22 of 24 The property to the south is a former gravel pit redeveloped into a pond and recreational area. The property is owned by the MT Fish, Wildlife, and Parks and was purchased in 1984. A 60 foot road easement to access the site passes from Manley Road through the application site and to the East Gallatin Recreation Area. This easement was a part of the purchase agreement between the State and landowner as is to the benefit of the specific parcel and is shown on Certificate of Survey 1221. Both Gallatin County and the City of Bozeman find that this easement is a public right of way for a street and not simply a driveway. The property containing the lack and recreation area was leased to the City of Bozeman by the State for recreational uses in 1991. A tract to the SW of the subject parcel also was the subject of a growth policy amendment in 2004 as application P-04044. The revised area was 1.84 acres in size and was located at 780 Manley Road. The request was also to change from the future land use designation of Park, Open Space and Recreational Lands to Residential. The application was considered by the City Commission on October 18, 2004 and was approved on a vote of 4-1. The minutes of that meeting are available through the City’s laserfiche archive. The property was later annexed, zoned as R-1, and developed as Minor Subdivision 385 into five residential lots. All lots are now built on. Turtle Way connects to Manley Road and provides access to the five lots. No parkland was dedicated with the development as minor subdivisions are not required to dedicate parkland. The property to the west has been annexed and is zoned M-1, Light Industrial and has been developed as the Gallatin Park subdivision. There are 30 lots and most have buildings on them. There is a pedestrian trail which passes through the subdivision to the Cherry Creek open space to the northwest. East Gallatin Recreation Area The most distinguishing feature of the East Gallatin Recreation Area is the 15.6 acre lake. The lake is supplied by ground water with a surface outlet on the north. The outlet flows to the north and around the adjacent subdivision and connects to a stream north of the right of way which divides the parcel. The outlet has both a manual control and an overflow control to enable management of the water level in the lake. Wetland and potential flooding areas are present but need to be formally delineated on the site. There are water setbacks and water quality standards which will apply to any future development of the site. Exact locations and nature of the setbacks and water quality improvements will be dependent on the delineation of the water courses, wetlands, and design of the site. 187 P-14051, City Commission Staff Report for The Villas Growth Policy Map Amendment Page 23 of 24 The 60 foot public right of way by easement which divides the application site provides the primary access to the East Gallatin Recreation Area. Both Gallatin County and the City of Bozeman find that the right of way is a public street subject to typical zoning setbacks and constructions standards. Any future development of the site will require the right of way to be upgraded to public road standards for both vehicles and pedestrians. Any future development of the site will also require provision of additional right of way for Manley Road which is a designated collector street in the long range transportation plan. There are four primary public interests in considering the change from Parks, Open Space and Recreation to Residential in addition to the specific review criteria. 1) Maintaining the existing legal and physical vehicle and pedestrian access to the East Gallatin Recreation Area. 2) Protecting any future development on the site from any exposures to potential hazards resulting from the adjacent former solid waste facility. 3) Maintaining additional open space to expand the present East Gallatin Recreation Area. 4) Character of the area. APPENDIX C – NOTICING AND PUBLIC COMMENT Notice of the public hearings before the Planning Board and City Commission was given by first class US mail to all property owners within 200 feet of the site. The site was posted with a copy of the notice. The notice was also published in the Bozeman Daily Chronicle at least 15 days and not more than 45 days prior to the public hearings. Public comment received as of the writing of this report: September 9, 2014 – letter regarding contamination concerns April 20, 2015 – letter regarding contamination concerns, park access, park experience. Public speakers at the public hearing testified regarding the character of the area, affect on the East Gallatin Recreation Area, traffic spill over, wildlife, affect on adjacent properties by the amendment, and potential of hazards due to proximity to a former landfill. Public testimony began at minute mark 2:31:00 of the recording available at http://media.avcaptureall.com/session.html?sessionid=b5c84dc7-c9a8-4bb0-b968- 6441bcc5444d. 188 P-14051, City Commission Staff Report for The Villas Growth Policy Map Amendment Page 24 of 24 APPENDIX D - OWNER INFORMATION AND REVIEWING STAFF Owner: Patricia Hash, and Bill Beyl c/o Beyl Trust 1520 Alder Court, Bozeman, MT 59715 Applicant: Andy Ebbighausen, PO Box 930, Manhattan, MT 59741 Representative: C&H Engineering & Surveying, Inc., 1091 Stoneridge Drive, Bozeman MT 59718 Report By: Chris Saunders, Policy and Planning Manager FISCAL EFFECTS No unusual fiscal effects have been identified. No presently budgeted funds will be changed by this growth policy amendment. ATTACHMENTS The full application and file of record can be viewed at the Community Development Department at 20 E. Olive Street, Bozeman, MT 59715. Commission Resolution 4594 Planning Board resolution Application materials Memo from Brian Heaston to DRC Recreation and Parks Advisory Board comments Public Comment to date Testing Report by Hydrometrics 189 Resolution No. 4594, Intent to revise Growth Policy, The Villas Page 1 of 2 RESOLUTION NO. 4594 A RESOLUTION OF THE CITY COMMISSION OF THE CITY OF BOZEMAN, MONTANA, STATING THE INTENT OF THE CITY COMMISSION TO CONSIDER AN AMENDMENT TO FIGURE 3-1 OF THE BOZEMAN COMMUNITY PLAN. WHEREAS, the City of Bozeman has had a comprehensive plan (growth policy) since 1958, and WHEREAS, the City of Bozeman adopted its growth policy known as the Bozeman Community Plan (BCP) through Resolution 4163 on June 1, 2009, and WHEREAS, the City of Bozeman adopted its most recent amendments to the growth policy known as the Bozeman Community Plan (BCP) through Resolution 4195 on August 3, 2009, and WHEREAS, the Bozeman City Commission establishes criteria for the amending of the document, and WHEREAS, an application has been received to amend Figure 3-1 the future land use map of the growth policy, and WHEREAS, the City of Bozeman Planning Board conducted a public hearing on the application on April 21, 2015, and WHEREAS, in accordance with 76-1-602, MCA, the City Commission must conduct a public hearing prior to taking any action to adopt or revise a growth policy, NOW, THEREFORE, BE IT RESOLVED by the City Commission of the City of Bozeman, Montana, that: Section 1 190 Resolution No. 4594, Intent to revise Growth Policy, The Villas Page 2 of 2 In accordance with the requirements of Section 76-1-604 MCA, the intent to consider the application for amendment and possible corresponding revisions to the growth policy is hereby stated. Section 2 That a public hearing was set and advertised for the purpose of receiving public testimony on P-14051, The Villas growth policy amendment, a possible revision to Figure 3-1 of the Bozeman Community Plan on property legally described as Section 31, Township 1S, Range 6E, C.O.S 157, Remaining Tract GLR-1, Gallatin County, Montana.. Section 3 PASSED AND APPROVED by the City Commission of the City of Bozeman, Montana, at a regular session thereof held on the 11th day of May 2015. DATED this 11th day of May, 2015. ___________________________________ JEFFREY K. KRAUSS Mayor ATTEST: ________________________________________ STACY ULMEN, CMC City Clerk APPROVED AS TO FORM: ___________________________________ GREG SULLIVAN City Attorney 191 The Villas Growth Policy Future Land Use Map Amendment 1 RESOLUTION #P14051 RESOLUTION OF THE CITY OF BOZEMAN PLANNING BOARD REGARDING A GROWTH POLICY AMENDMENT TO REVISE FIGURE 3-1, THE FUTURE LAND USE MAP FROM PARKS, RECREATION AND OPEN SPACE TO RESIDENTIAL ON 6.49 ACRES LOCATED EAST OF MANLEY ROAD, NORTH OF TURTLE WAY ADJACENT TO THE EAST GALLATIN RECREATION AREA. THE PROPERTY IS LEGALLY DESCRIBED AS SECTION 31, TOWNSHIP 1S, RANGE 6E, C.O.S 157, REMAINING TRACT GLR-1, GALLATIN COUNTY, MONTANA. WHEREAS, the City of Bozeman has adopted a growth policy pursuant to Section 76-1- 601, M.C.A.; and WHEREAS, the City of Bozeman Planning Board has been created by Resolution of the Bozeman City Commission as provided for in Title 76-1-101, M.C.A.; and WHEREAS, the property owner Patricia Hash, and Bill Beyl c/o Beyl Trust, 1520 Alder Court, Bozeman, MT 59715, applicant Andy Ebbighausen, PO Box 930, Manhattan, MT 59741, represented by C&H Engineering and Surveying, Inc., 1091 Stoneridge Drive, Bozeman, MT 59718 submitted a growth policy amendment to revise Figure 3-1, Future Land Use Map; and WHEREAS, the proposed growth policy amendment has been properly submitted, reviewed, and advertised in accordance with the procedures of Section 38.03 of the Bozeman Unified Development Code; and WHEREAS, the City of Bozeman Planning Board held a public hearing on Tuesday, April 21, 2015, to review the application and any written public testimony on the request for said growth policy amendment application; and WHEREAS, two written comments and three items of oral testimony by the general public concerning the growth policy amendment were received; and WHEREAS, members of the City of Bozeman Planning Board discussed the proposed growth policy amendment in regards to the character of the area, affect on the East Gallatin Recreation Area, traffic spill over, wildlife, affect on adjacent properties by the amendment, potential of hazards due to proximity to a former landfill, whether there was an error in the designation of the property on the future land use map; and the criteria for amendment; and WHEREAS, the City of Bozeman Planning Board moved to recommend approval of the preliminary plat application with the recommended contingencies provided in the staff report; and NOW, THEREFORE, BE IT RESOLVED, that the City of Bozeman Planning Board, having heard and considered public comment, adopted the findings presented in the staff report for P14051 and voted 1:5 to recommended to of growth policy amendment with the contingencies as outlined in the staff report: 1) The applicant shall submit, within forty-five (45) days of approval by the City 192 The Villas Growth Policy Future Land Use Map Amendment 2 Commission, an 8½- x 11-inch or 8½- x 14-inch exhibit entitled “The Villas Growth Policy Amendment” to the Department of Community Development containing an accurate description of the property for which the growth policy designation is being amended. The exhibit must be acceptable to the Department of Community Development. 2) The resolution for the growth policy amendment shall not be drafted until the applicant provides an exhibit of the area to be re-designated, which will be utilized in the preparation of the resolution to officially amend the Future Land Use Map of the Bozeman Community Plan. DATED THIS DAY OF , 2015 Resolution #P14051 _____________________________ ____________________________ Chris Saunders Erik Garberg, Chairperson Department of Community Development City of Bozeman Planning Board Video begins at 2:17.5 minutes into the recorded video. 193 194 195 196 197 198 199 200 201 202 203 204 205 Resource Technologies, Inc. 1050 East Main Street Suite 4, Bozeman, Montana 59715 Voice: (406) 585-8005 • Fax: (406) 585-0069 • e-mail: rti @ montana.net January 13, 2015 Mr. Andy Ebbighausen P.O. Box 930 Manhattan, MT 59741 Subject: Environmental Sampling Report; Manley Drive Property; Bozeman, Montana Dear Mr. Ebbighausen: Resource Technologies, Inc. (RTI) has completed environmental sampling at the property located east of Manley Road and north of the Bozeman Ponds Recreation Area in Bozeman, Montana. Environmental sampling was completed to assess potential environmental impacts associated with the former Bozeman City Landfill that was situated southeast of the subject property. Sampling activities were not designed nor intended to identify potential on-site sources of contamination. Work tasks included installing two groundwater monitoring wells and two soil vapor probes at the property and collection of soil, groundwater, and soil vapor samples. One monitoring well and soil vapor probe were placed along the southern boundary of the site and one monitoring well and soil vapor probe were placed along the eastern margin of the site (Figure 1). Sampling locations were selected to establish environmental conditions at the up-hydraulic gradient boundaries of the subject property. Groundwater at these locations is expected to be flowing onto the subject property from the south and/or east. As such, contaminants identified at these locations (particularly in groundwater and soil vapor) would presumably be attributable to an off-site source. Sampling methods and results are discussed below. Monitoring Well Installation On December 16, 2014, RTI installed two monitoring wells (MW-1 and MW-2) at the locations shown in Figure 1 using direct push methods. Stantec of Butte, Montana provided soil-boring services. Soil samples were collected continuously by driving a four-foot core barrel with an acetate liner into undisturbed soil. Samples collected above the water table were field screened for the presence of volatile organic compounds (VOCs) using a photoionization detector (PID) and heated headspace methods. One soil sample from each borehole collected above the soil/groundwater interface was retained and submitted to Energy Laboratories in Billings for extractable petroleum hydrocarbons (EPH) screen and VOCs (Method 8260 Extended List) analyses. The analyte list for soil samples is included as Table 1A. Soil laboratory analytical reports are included as Appendix A. 206 Mr. Andy Ebbighausen Page 2 January 13, 2015 Resource Technologies, Inc. Soil boreholes were advanced to depths of 12 feet and were completed as groundwater monitoring wells with 1-inch diameter polyvinyl chloride (PVC) well casing and eight foot lengths of 0.010 inch slotted well screen positioned from 4 to 12 feet below ground surface. A washed sand filter pack was emplaced around the well screen and the remaining annular space was backfilled with granular bentonite. Since the monitoring wells are expected to be temporary installations, no protective cover was installed over the wellheads. Soil borehole logs are included as Appendix B. Monitoring wells were developed by surging and pumping until the wells yielded visibly non-turbid water. Soil Vapor Probe Installation On December 16, 2014, RTI installed two soil vapor probes (VW-1 and VW-2) at the location shown in Figure 1 using direct push methods. A six-inch stainless steel GeotechTM soil vapor probe was installed at a depth of 3 to 3.5 feet at each location. Teflon tubing was attached to the probe and the tubing extended to several feet above ground surface to facilitate soil vapor sampling. Washed sand was emplaced around the probe and the remaining annular space was backfilled with granular bentonite. Groundwater Sampling Groundwater samples were collected from the two monitoring wells on December 22, 2014 using disposable polyethylene bailers and nylon string. Prior to sample collection, a minimum of three casing volumes of water were purged from the well. During purging, stabilization parameters including temperature, pH, conductivity, dissolved oxygen, and oxidation reduction potential were monitored. When readings of these parameters stabilized, groundwater samples were collected. Samples were transferred to laboratory provided containers and were submitted to Energy Laboratories for EPH screen and VOCs analyses. The analyte list for groundwater samples is included as Table 1A. Groundwater analytical results for detected compounds only are included in Table 1B and laboratory analytical reports are included as Appendix C. Soil Vapor Sampling Soil vapor samples were collected from the two soil vapor probes on December 22, 2014. Six-liter SUMMA canisters with flow controllers calibrated to collect a sample over an interval of one hour were connected to the vapor-probe tubing. Sampling was initiated by opening the SUMMA canister valve at the start of sampling and monitoring the flow controller vacuum. When the vacuum reading on the flow controller decreased to no less than (5) inches mercury, sampling was terminated by closing the SUMMA canister valve. Following sampling, a protective cap was then tightened onto the SUMMA canister intake fitting. The SUMMA canisters were submitted to ALS Laboratories of Salt Lake City, Utah for VOCs analysis by Method TO-15. The analytical laboratory supplied the certified SUMMA canister, flow controller, and vacuum gauge. The SUMMA canisters were returned to the laboratory along with the flow controllers in the same packaging in which they arrived. The analyte list for soil 207 Mr. Andy Ebbighausen Page 3 January 13, 2015 Resource Technologies, Inc. vapor samples is included as Table 2A. Analytical results for detected compounds only are summarized in Table 2B and laboratory analytical reports are included as Appendix D. Results Soil Analytes detected in soil samples were limited to total extractable hydrocarbons (TEH) detected via EPH analysis in sample MW-1 3-4 at a concentration of 59 milligrams per kilogram (mg/kg). TEH represents the aliphatic and aromatic hydrocarbon compounds that comprise diesel fuel and waste oil; however, the laboratory indicated that the analytical profile of TEH detected in sample MW-1 3-4 was typical of naturally occurring hydrocarbons in soil. Groundwater Analytes detected in groundwater samples included the VOCs toluene, chloroethane, and vinyl chloride. VOCs detected in sample MW-1 were limited to toluene at an estimated concentration of 0.14 micrograms per liter (g/l). The result was “J” qualified by the laboratory since the compound was detected at a concentration below the laboratory reporting limit. VOCs detected in sample MW-2 included chloroethane reported at a “J” qualified concentration of 0.11 g/l, toluene reported at a “J” qualified concentration of 0.19 g/l, and vinyl chloride reported at a “J” qualified concentration of 0.52 g/l. TEH was not detected in either groundwater sample. Soil Vapor Analytical results for soil-vapor sample VW-1 indicated a total VOCs concentration of 220 micrograms per cubic meter (g/m3). The majority of the VOCs detected in this sample were unidentified compounds that are not VOCs on the TO-15 analyte list. Identified compounds included freon 11 reported at a “J” qualified concentration of 0.87 g/m3 and tetrachloroethene (PCE) reported at a concentration of 51 g/m3. Analytical results for soil-vapor sample VW-2 indicated a total VOCs concentration of 410 micrograms per cubic meter g/m3. Just under 50% of the VOCs detected in this sample were unidentified compounds that are not VOCs on the TO-15 analyte list. Identified compounds included freon 11 reported at a “J” qualified concentration of 0.87 g/m3, acetone reported at 100 g/m3, 2-butanone reported at g/m3, chloroform reported at g/m3, tetrahydrofuran reported at 10 g/m3, toluene reported at 6.5 g/m3, PCE reported at 1.1 g/m3, ethylbenzene reported at 3.4 g/m3, total xylenes reported at 23.1 g/m3, 4-ethyl toluene reported at 3.6 g/m3, 1,3,5 trimethylbenzene reported at 7.2 g/m3, and 1,2,4 trimethylbenzene reported at 20 g/m3. Discussion Groundwater and soil vapor along the eastern and southern boundaries of the property appear to be impacted with a variety of VOCs that are not naturally occurring. Impacts 208 Mr. Andy Ebbighausen Page 4 January 13, 2015 Resource Technologies, Inc. appear to be more substantial along the eastern site boundary. With the exception of TEH, no target analytes were detected in either soil sample collected at the site. The reported TEH concentration was well below the most conservative soil RBSLs and the laboratory report indicated that detected TEH may have been naturally occurring. VOCs detected in groundwater included toluene and vinyl chloride at concentrations below the laboratory reporting limit. The laboratory reporting limit is the level at which the concentration of a compound can be quantified with statistical confidence. These compounds were positively identified; however, the concentrations were too low to be quantified with statistical confidence, thus the reported values are estimates. The estimated concentrations of toluene are well below human health standards for groundwater. The estimated vinyl chloride concentration (0.52 g/l) exceeds the human health standard for groundwater of 0.2 g/l. Vinyl chloride is the final breakdown product of PCE. Numerous VOCs were detected in soil vapor samples (Table 2B). There are no established regulatory screening levels for VOCs in soil vapor. Conclusions VOCs that are not naturally occurring were detected in groundwater and soil vapor along the southern and eastern margins of the subject property. Sampling points were chosen to assess potential environmental impacts originating off site. Sample points MW-1 and VW-1 were positioned to detect contaminants potentially entering the site from the south and sample points MW-2 and VW-2 were positioned to detect contaminants potentially entering the site from the east. It is unknown if any of the sampling data represents worst case conditions. Only one applicable regulatory screening level was exceeded by detected compounds. The groundwater human health standard for vinyl chloride was exceeded in sample MW-2, although the reported concentration was “J” qualified for being below the laboratory reporting limit. Limitations Sampling conducted at the subject property was intended to assess the potential for impacts by contaminants associated with the former Bozeman City Landfill. The data indicate that groundwater and soil vapor at the presumed upgradient margins of the subject property are impacted by VOCs; however, the data are not definitive as to the contaminant source or to the extent and magnitude of impacts on site. In addition, sampling was not intended to assess environmental conditions across the entire property, only at the specific locations chosen for sampling. 209 210 Figures 211 Resource Technologies Inc. MW-1 MW-2 VW-2 VW-1 MW-1 VP-1 Existing 1-inch groundwater monitoring well Existing soil vapor probe Figure 1. Site Photo and Sample Locations Manley road Property Bozeman, Montana Proposed 1-inch groundwater monitoring well 212 Tables 213 Table 1A. Soil and Groundwater Sampling Target Compounds; December 22, 2014; Ebbighausen; Bozeman, Montana EPH Screen Target Analytes 1,1,1-Trichloroethane Chlorobenzene Total Extractable Hydrocarbons (TEH) 1,1,1,2-Tetrachloroethane Chlorodibromomethane 1,1,2,2-Tetrachloroethane Chloroethane 1,1,2-Trichloroethane Chloroform 1,1-Dichloroethane Chloromethane 1,1-Dichloroethene cis-1,2-Dichloroethene 1,1-Dichloropropene cis-1,3-Dichloropropene 1,2,3-Trichloropropane Dibromomethane 1,2-Dibromoethane Dichlorodifluoromethane 1,2-Dichlorobenzene Ethyl benzene 1,2-Dichloroethane m,p-Xylene 1,2-Dichloropropane Methyl ethyl ketone (2-Butanone) 1,3-Dichlorobenzene Methyl t-butyl ether 1,3 Dichloropropane Methylene chloride 1,4-Dichlorobenzene o-Xylene 2-Chlorotoluene Styrene 2,2 Dichloropropane Tetrachloroethene Benzene Toluene Bromobenzene trans-1,2-Dichloroethene Bromochloromethane trans-1,3-Dichloropropene Bromodichloromethane Trichloroethene Bromoform Trichlorofluormethane Bromomethane Vinyl chloride Carbon tetrachloride Method 8260 (VOCs) Target Analytes 214 Table 1B. Groundwater Sampling Results; Detected Compounds; December 22, 2014; Ebbighausen, Bozeman, Montana VOCs by 8260 DEQ Human Health Standard for Groundwater Chloroethane ND 0.11 J NA Toluene 0.14 J 0.19 J 1,000 Vinyl chloride ND 0.52 J 0.2 Notes: Q = Qualifier ND = Not detected. NA = Not applicable. µg/l Q Analyte J = Qualifier Indicates that the analyte value is between the MDL and the Reporting Limit (RL). It is also used to indicate an estimated value for tentatively identified compounds in mass µg/l = micrograms per liter MW-1 MW-2 µg/l Q µg/l Z:\Projects\ESAs\Ebbighausen Bozeman Ponds\Data\Table 1B Groundwater Sample Results 12.2014 1 of 1 215 Tentatively Identified Compounds* 1,1,1-Trichloroethane Chloromethane Ethanol 1,1,2,2-Tetrachloroethane cis-1,2-Dichloroethene Decane 1,1,2-Trichloroethane cis-1,3-Dichloropropene 4-methyl-Decane 1,1-Dichloroethane Cyclohexane 1,1-Dichloroethene Dibromochloromethane 1,2,4-Trichlorobenzene Dichlorodifluoromethane 1,2,4-Trimethylbenzene Ethyl acetate1,2-Dibromoethane Ethyl benzene 1,2-Dichlorobenzene Freon 11 1,2-Dichloroethane Freon 113 1,2-Dichloropropane Freon 114 1,3,5-Trimethylbenzene Heptane1,3-Butadiene Hexane 1,3-Dichlorobenzene Hexachlorobutadiene 1,4-Dichlorobenzene m,p-Xylene 2-Hexanone Methyl ethyl ketone (2-Butanone) 4-Ethyl Toluene Methyl t-butyl ether 4-Methyl-2-pentanone Methylene chloride Acetone o-Xylene Benzene Styrene Benzyl chloride Tetrachloroethene Bromodichloromethane Tetrahydrofuran Bromoform Toluene Bromomethane Total Volatile Organics Carbon disulfide trans-1,2-Dichloroethene Carbon tetrachloride trans-1,3-Dichloropropene Chlorobenzene Trichloroethene Chloroethane Vinyl acetate Chloroform Vinyl chloride Table 2A. Soil Vapor Sampling Target Compounds; December 22, 2014; Ebbighausen; Bozeman, Montana TO-15 Analytes Z:\Projects\ESAs\Ebbighausen Bozeman Ponds\Data\Table 2B Air Sample Results 12.2014 1 of 1216 Table 2B. Soil Vapor Sampling Results; Detected Compounds; December 22, 2014; Ebbighausen, Bozeman, Montana VOCs by TO-15 1,2,4-Trimethylbenzene ND U <0.74 U 4.0 20 1,3,5-Trimethylbenzene ND U <0.74 U 1.5 7.2 4-Ethyl Toluene ND U <0.74 U 0.73 3.6 Acetone ND U <0.71 U 43 E 100 E Chloroform ND U <0.73 U 0.41 J 2.0 J Ethyl benzene ND U <0.65 U 0.79 3.4 Freon 11 0.16 J 0.87 J 0.15 J 0.87 J m,p-Xylene ND U <0.65 U 4.0 18 Methyl ethyl ketone (2-Butanone)ND U <0.44 U 3.5 10 o-Xylene ND U <0.65 U 1.2 5.1 Tetrachloroethene 7.5 51 0.16 J 1.1 J Tetrahydrofuran ND U <0.44 U 3.5 10 Toluene ND U <0.57 U 1.7 6.5 Total Volatile Organics 53 J 220 J 100 410 Tentatively Identified Compounds* Decane 5.8 J Ethanol 21 J 4-methyl-Decane 2.7 J Notes: Q = Qualifier * Compounds not on the TO-15 analyte list Sample ID VW-1 QQ b - EPA commercial air screening level (EPA, 2014) VW-2 a - EPA residential air screening level (EPA, 2014) ppb v/v ND = Not detected. NA = Not applicable. µg/m3 Q U = Qualifier indicates that the analyte was not detected above the Method Detection Limit (MDL). E = Qualifier indicates that the analyte result exceeds calibration range. ppb v/v Analyte J = Qualifier Indicates that the analyte value is between the MDL and the Reporting Limit (RL). It is also used to indicate an estimated value for tentatively identified compounds in mass spectrometry where a 1:1 response is assumed. µg/m3 µg/m3 = micrograms per cubic meter ppb v/v = parts per billion volume Q Z:\Projects\ESAs\Ebbighausen Bozeman Ponds\Data\Table 2B Air Sample Results 12.2014 1 of 1 217 APPENDIX A Laboratory Analytical Reports - Soil 218 ANALYTICAL SUMMARY REPORTANALYTICAL SUMMARY REPORTANALYTICAL SUMMARY REPORTANALYTICAL SUMMARY REPORT The analyses presented in this report were performed by Energy Laboratories, Inc., 1120 S 27th St., Billings, MT 59101, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Lab ID Client Sample ID Collect Date Receive Date Matrix Test Report Approved By: B14121551-001 MW-1 3-4 12/16/14 10:00 12/17/14 Soil EPH-Ultrasonic Extraction Hydrocarbons, Extractable Petroleum-Scrn Moisture Moisture Prep Percent Moisture Volatile Organics, Methanol Extraction 8260-Volatile Organic Compounds- Extended List B14121551-002 MW-2 5-6 12/16/14 10:15 12/17/14 Soil Same As Above Resource Technologies Inc Project Name: Ebbighausen Work Order: B14121551 1050 E Main St Ste 4 Bozeman, MT 59715 December 30, 2014 Energy Laboratories Inc Billings MT received the following 2 samples for Resource Technologies Inc on 12/17/2014 for analysis. Page 1 of 19219 LABORATORY ANALYTICAL REPORT Client:Resource Technologies Inc Project:Ebbighausen Lab ID:B14121551-001 Client Sample ID:MW-1 3-4 Collection Date:12/16/14 10:00 Matrix:Soil Report Date:12/24/14 DateReceived:12/17/14 Revised Date:12/30/14Prepared by Billings, MT Branch Analyses Result Units Analysis Date / ByRLMethod MCL/ QCLQualifiers PHYSICAL CHARACTERISTICS 12/19/14 08:24 / amn0.2wt%17Moisture SW3550A VOLATILE ORGANIC COMPOUNDS 12/19/14 14:13 / jrj4.0mg/kg-dryNDAcetone SW8260B 12/19/14 14:13 / jrj4.0mg/kg-dryNDAcetonitrile SW8260B 12/19/14 14:13 / jrj4.0mg/kg-dryNDAcrolein SW8260B 12/19/14 14:13 / jrj4.0mg/kg-dryNDAcrylonitrile SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDBenzene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDBromobenzene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDBromochloromethane SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDBromodichloromethane SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDBromoform SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDBromomethane SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDn-Butylbenzene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDsec-Butylbenzene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDtert-Butylbenzene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDCarbon disulfide SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDCarbon tetrachloride SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDChlorobenzene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDChlorodibromomethane SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDChloroethane SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryND2-Chloroethyl vinyl ether SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDChloroform SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDChloromethane SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryND2-Chlorotoluene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryND4-Chlorotoluene SW8260B 12/19/14 14:13 / jrj0.24mg/kg-dryND1,2-Dibromo-3-chloropropane SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryND1,2-Dibromoethane SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDDibromomethane SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryND1,2-Dichlorobenzene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryND1,3-Dichlorobenzene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryND1,4-Dichlorobenzene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDDichlorodifluoromethane SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryND1,1-Dichloroethane SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryND1,2-Dichloroethane SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryND1,1-Dichloroethene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDcis-1,2-Dichloroethene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDtrans-1,2-Dichloroethene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryND1,2-Dichloropropane SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryND1,3-Dichloropropane SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryND2,2-Dichloropropane SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryND1,1-Dichloropropene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDcis-1,3-Dichloropropene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDtrans-1,3-Dichloropropene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDEthylbenzene SW8260B Report Definitions: RL - Analyte reporting limit.MCL - Maximum contaminant level. QCL - Quality control limit.ND - Not detected at the reporting limit. Page 2 of 19220 LABORATORY ANALYTICAL REPORT Client:Resource Technologies Inc Project:Ebbighausen Lab ID:B14121551-001 Client Sample ID:MW-1 3-4 Collection Date:12/16/14 10:00 Matrix:Soil Report Date:12/24/14 DateReceived:12/17/14 Revised Date:12/30/14Prepared by Billings, MT Branch Analyses Result Units Analysis Date / ByRLMethod MCL/ QCLQualifiers VOLATILE ORGANIC COMPOUNDS 12/19/14 14:13 / jrj0.20mg/kg-dryNDHexachlorobutadiene SW8260B 12/19/14 14:13 / jrj4.0mg/kg-dryND2-Hexanone SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDIodomethane SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDIsopropylbenzene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDp-Isopropyltoluene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDMethyl tert-butyl ether (MTBE)SW8260B 12/19/14 14:13 / jrj4.0mg/kg-dryNDMethyl ethyl ketone SW8260B 12/19/14 14:13 / jrj4.0mg/kg-dryNDMethyl isobutyl ketone SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDMethylene chloride SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDNaphthalene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDn-Propylbenzene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDStyrene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryND1,1,1,2-Tetrachloroethane SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryND1,1,2,2-Tetrachloroethane SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDTetrachloroethene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDToluene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryND1,2,3-Trichlorobenzene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryND1,2,4-Trichlorobenzene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryND1,1,1-Trichloroethane SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryND1,1,2-Trichloroethane SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDTrichloroethene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDTrichlorofluoromethane SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryND1,2,3-Trichloropropane SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryND1,2,4-Trimethylbenzene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryND1,3,5-Trimethylbenzene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDVinyl acetate SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDVinyl chloride SW8260B 12/19/14 14:13 / jrj0.24mg/kg-dryNDm+p-Xylenes SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDo-Xylene SW8260B 12/19/14 14:13 / jrj0.20mg/kg-dryNDXylenes, Total SW8260B 12/19/14 14:13 / jrj60-136%REC90.0 Surr: 1,2-Dichloroethane-d4 SW8260B 12/19/14 14:13 / jrj70-132%REC90.0 Surr: Dibromofluoromethane SW8260B 12/19/14 14:13 / jrj78-160%REC98.0 Surr: p-Bromofluorobenzene SW8260B 12/19/14 14:13 / jrj75-138%REC96.0 Surr: Toluene-d8 SW8260B EXTRACTABLE PETROLEUM HYDROCARBONS-SCREEN 12/29/14 14:18 / amn12mg/kg-dry13Total Extractable Hydrocarbons (SGT)SW8015M200 12/19/14 23:22 / amn12mg/kg-dry59Total Extractable Hydrocarbons SW8015M200 12/29/14 14:18 / amn40-140%REC76.0 Surr: o-Terphenyl (SGT)SW8015M 12/19/14 23:22 / amn40-140%REC79.0 Surr: o-Terphenyl SW8015M - Note: Total Extractable Hydrocarbons are defined as the total hydrocarbon responses regardless of elution time. - Results for both the Silca Gel Treatment (SGT) and the untreated solvent extract are reported. Silica gel treatment removes polar non-petroleum hydrcarbons. The hydrocarbon profile was typical of natural occuring hydrocarbons in soil. Report Definitions: RL - Analyte reporting limit.MCL - Maximum contaminant level. QCL - Quality control limit.ND - Not detected at the reporting limit. Page 3 of 19221 LABORATORY ANALYTICAL REPORT Client:Resource Technologies Inc Project:Ebbighausen Lab ID:B14121551-002 Client Sample ID:MW-2 5-6 Collection Date:12/16/14 10:15 Matrix:Soil Report Date:12/24/14 DateReceived:12/17/14 Revised Date:12/30/14Prepared by Billings, MT Branch Analyses Result Units Analysis Date / ByRLMethod MCL/ QCLQualifiers PHYSICAL CHARACTERISTICS 12/19/14 08:27 / amn0.2wt%20Moisture SW3550A VOLATILE ORGANIC COMPOUNDS 12/19/14 14:42 / jrj4.0mg/kg-dryNDAcetone SW8260B 12/19/14 14:42 / jrj4.0mg/kg-dryNDAcetonitrile SW8260B 12/19/14 14:42 / jrj4.0mg/kg-dryNDAcrolein SW8260B 12/19/14 14:42 / jrj4.0mg/kg-dryNDAcrylonitrile SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDBenzene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDBromobenzene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDBromochloromethane SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDBromodichloromethane SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDBromoform SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDBromomethane SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDn-Butylbenzene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDsec-Butylbenzene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDtert-Butylbenzene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDCarbon disulfide SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDCarbon tetrachloride SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDChlorobenzene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDChlorodibromomethane SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDChloroethane SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryND2-Chloroethyl vinyl ether SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDChloroform SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDChloromethane SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryND2-Chlorotoluene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryND4-Chlorotoluene SW8260B 12/19/14 14:42 / jrj0.25mg/kg-dryND1,2-Dibromo-3-chloropropane SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryND1,2-Dibromoethane SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDDibromomethane SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryND1,2-Dichlorobenzene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryND1,3-Dichlorobenzene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryND1,4-Dichlorobenzene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDDichlorodifluoromethane SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryND1,1-Dichloroethane SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryND1,2-Dichloroethane SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryND1,1-Dichloroethene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDcis-1,2-Dichloroethene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDtrans-1,2-Dichloroethene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryND1,2-Dichloropropane SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryND1,3-Dichloropropane SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryND2,2-Dichloropropane SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryND1,1-Dichloropropene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDcis-1,3-Dichloropropene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDtrans-1,3-Dichloropropene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDEthylbenzene SW8260B Report Definitions: RL - Analyte reporting limit.MCL - Maximum contaminant level. QCL - Quality control limit.ND - Not detected at the reporting limit. Page 4 of 19222 LABORATORY ANALYTICAL REPORT Client:Resource Technologies Inc Project:Ebbighausen Lab ID:B14121551-002 Client Sample ID:MW-2 5-6 Collection Date:12/16/14 10:15 Matrix:Soil Report Date:12/24/14 DateReceived:12/17/14 Revised Date:12/30/14Prepared by Billings, MT Branch Analyses Result Units Analysis Date / ByRLMethod MCL/ QCLQualifiers VOLATILE ORGANIC COMPOUNDS 12/19/14 14:42 / jrj0.20mg/kg-dryNDHexachlorobutadiene SW8260B 12/19/14 14:42 / jrj4.0mg/kg-dryND2-Hexanone SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDIodomethane SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDIsopropylbenzene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDp-Isopropyltoluene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDMethyl tert-butyl ether (MTBE)SW8260B 12/19/14 14:42 / jrj4.0mg/kg-dryNDMethyl ethyl ketone SW8260B 12/19/14 14:42 / jrj4.0mg/kg-dryNDMethyl isobutyl ketone SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDMethylene chloride SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDNaphthalene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDn-Propylbenzene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDStyrene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryND1,1,1,2-Tetrachloroethane SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryND1,1,2,2-Tetrachloroethane SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDTetrachloroethene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDToluene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryND1,2,3-Trichlorobenzene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryND1,2,4-Trichlorobenzene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryND1,1,1-Trichloroethane SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryND1,1,2-Trichloroethane SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDTrichloroethene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDTrichlorofluoromethane SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryND1,2,3-Trichloropropane SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryND1,2,4-Trimethylbenzene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryND1,3,5-Trimethylbenzene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDVinyl acetate SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDVinyl chloride SW8260B 12/19/14 14:42 / jrj0.25mg/kg-dryNDm+p-Xylenes SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDo-Xylene SW8260B 12/19/14 14:42 / jrj0.20mg/kg-dryNDXylenes, Total SW8260B 12/19/14 14:42 / jrj60-136%REC82.0 Surr: 1,2-Dichloroethane-d4 SW8260B 12/19/14 14:42 / jrj70-132%REC83.0 Surr: Dibromofluoromethane SW8260B 12/19/14 14:42 / jrj78-160%REC89.0 Surr: p-Bromofluorobenzene SW8260B 12/19/14 14:42 / jrj75-138%REC86.0 Surr: Toluene-d8 SW8260B EXTRACTABLE PETROLEUM HYDROCARBONS-SCREEN 12/19/14 22:30 / amn13mg/kg-dryNDTotal Extractable Hydrocarbons SW8015M200 12/19/14 22:30 / amn40-140%REC87.0 Surr: o-Terphenyl SW8015M - Note: Total Extractable Hydrocarbons are defined as the total hydrocarbon responses regardless of elution time. Report Definitions: RL - Analyte reporting limit.MCL - Maximum contaminant level. QCL - Quality control limit.ND - Not detected at the reporting limit. Page 5 of 19223 Project:Ebbighausen Client:Resource Technologies Inc Work Order:B14121551 QA/QC Summary Report 12/24/14Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits Qual Prepared by Billings, MT Branch Method: SW8260B Batch: 85641 Lab ID: lcs-85641 12/19/14 11:45Laboratory Control Sample Run: 5971A.I_141219A Acetone 107 49 1454.010.7 mg/kg Acetonitrile 82 60 1304.08.24 mg/kg Acrolein 85 20 1974.08.48 mg/kg Acrylonitrile 86 45 1464.08.56 mg/kg Benzene 99 70 1270.200.992 mg/kg Bromobenzene 101 70 1350.201.01 mg/kg Bromochloromethane 110 60 1300.201.10 mg/kg Bromodichloromethane 100 56 1360.201.00 mg/kg Bromoform 85 59 1320.200.848 mg/kg Bromomethane 36 18 1340.200.362 mg/kg n-Butylbenzene 108 71 1340.201.08 mg/kg sec-Butylbenzene 103 67 1320.201.03 mg/kg tert-Butylbenzene 102 68 1340.201.02 mg/kg Carbon disulfide 90 32 1410.200.896 mg/kg Carbon tetrachloride 109 60 1400.201.09 mg/kg Chlorobenzene 98 75 1320.200.976 mg/kg Chlorodibromomethane 86 62 1330.200.856 mg/kg Chloroethane 27 45 1390.200.270 mg/kg S Chloroform 104 62 1320.201.04 mg/kg Chloromethane 95 41 1380.200.952 mg/kg 2-Chloroethyl vinyl ether 100 41 1490.201.00 mg/kg 1,2-Dibromo-3-chloropropane 89 57 1230.200.888 mg/kg 1,2-Dibromoethane 95 60 1350.200.952 mg/kg 2-Chlorotoluene 98 74 1350.200.976 mg/kg Dibromomethane 110 60 1350.201.10 mg/kg 1,2-Dichlorobenzene 98 70 1300.200.976 mg/kg 4-Chlorotoluene 102 75 1360.201.02 mg/kg 1,3-Dichlorobenzene 98 71 1320.200.976 mg/kg 1,4-Dichlorobenzene 108 71 1310.201.08 mg/kg Dichlorodifluoromethane 85 31 1230.200.848 mg/kg 1,1-Dichloroethane 104 66 1300.201.04 mg/kg 1,2-Dichloroethane 97 51 1400.200.968 mg/kg 1,1-Dichloroethene 106 64 1330.201.06 mg/kg cis-1,2-Dichloroethene 96 63 1310.200.960 mg/kg trans-1,2-Dichloroethene 100 66 1330.201.00 mg/kg 1,2-Dichloropropane 96 60 1300.200.960 mg/kg 1,3-Dichloropropane 95 59 1350.200.952 mg/kg 2,2-Dichloropropane 107 39 1570.201.07 mg/kg 1,1-Dichloropropene 103 65 1320.201.03 mg/kg cis-1,3-Dichloropropene 93 55 1340.200.928 mg/kg trans-1,3-Dichloropropene 95 58 1460.200.952 mg/kg Ethylbenzene 103 74 1360.201.03 mg/kg Hexachlorobutadiene 95 52 1330.200.952 mg/kg Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. S - Spike recovery outside of advisory limits. Page 6 of 19224 Project:Ebbighausen Client:Resource Technologies Inc Work Order:B14121551 QA/QC Summary Report 12/24/14Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits Qual Prepared by Billings, MT Branch Method: SW8260B Batch: 85641 Lab ID: lcs-85641 12/19/14 11:45Laboratory Control Sample Run: 5971A.I_141219A 2-Hexanone 100 54 1294.010.0 mg/kg Iodomethane 111 53 1280.201.11 mg/kg Isopropylbenzene 99 70 1330.200.992 mg/kg p-Isopropyltoluene 114 70 1310.201.14 mg/kg Methyl tert-butyl ether (MTBE)86 43 1520.200.864 mg/kg Methyl ethyl ketone 96 43 1484.09.60 mg/kg Methyl isobutyl ketone 91 54 1274.09.12 mg/kg Methylene chloride 90 51 1340.200.904 mg/kg Naphthalene 81 15 1710.200.808 mg/kg n-Propylbenzene 98 72 1340.200.976 mg/kg Styrene 102 70 1350.201.02 mg/kg 1,1,1,2-Tetrachloroethane 99 35 1560.200.992 mg/kg 1,1,2,2-Tetrachloroethane 96 59 1350.200.960 mg/kg Tetrachloroethene 112 64 1390.201.12 mg/kg Toluene 99 73 1370.200.992 mg/kg 1,2,3-Trichlorobenzene 84 24 1530.200.840 mg/kg 1,2,4-Trichlorobenzene 84 34 1500.200.840 mg/kg 1,1,1-Trichloroethane 107 63 1340.201.07 mg/kg 1,1,2-Trichloroethane 90 56 1360.200.904 mg/kg Trichloroethene 98 65 1340.200.976 mg/kg Trichlorofluoromethane 92 48 1400.200.920 mg/kg 1,2,3-Trichloropropane 93 56 1420.200.928 mg/kg 1,2,4-Trimethylbenzene 98 67 1250.200.984 mg/kg 1,3,5-Trimethylbenzene 101 71 1310.201.01 mg/kg Vinyl acetate 88 28 1230.200.880 mg/kg Vinyl chloride 97 32 1360.200.968 mg/kg m+p-Xylenes 99 75 1360.201.98 mg/kg o-Xylene 96 72 1340.200.960 mg/kg Surr: 1,2-Dichloroethane-d4 86 60 1360.20 Surr: Dibromofluoromethane 85 70 1320.20 Surr: p-Bromofluorobenzene 95 78 1600.20 Surr: Toluene-d8 92 75 1380.20 Lab ID: mb-85641 12/19/14 13:14Method Blank Run: 5971A.I_141219A Acetone 4.0ND mg/kg Acetonitrile 4.0ND mg/kg Acrolein 4.0ND mg/kg Acrylonitrile 4.0ND mg/kg Benzene 0.20ND mg/kg Bromobenzene 0.20ND mg/kg Bromochloromethane 0.20ND mg/kg Bromodichloromethane 0.20ND mg/kg Bromoform 0.20ND mg/kg Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 7 of 19225 Project:Ebbighausen Client:Resource Technologies Inc Work Order:B14121551 QA/QC Summary Report 12/24/14Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits Qual Prepared by Billings, MT Branch Method: SW8260B Batch: 85641 Lab ID: mb-85641 12/19/14 13:14Method Blank Run: 5971A.I_141219A Bromomethane 0.20ND mg/kg n-Butylbenzene 0.20ND mg/kg sec-Butylbenzene 0.20ND mg/kg tert-Butylbenzene 0.20ND mg/kg Carbon disulfide 0.20ND mg/kg Carbon tetrachloride 0.20ND mg/kg Chlorobenzene 0.20ND mg/kg Chlorodibromomethane 0.20ND mg/kg Chloroethane 0.20ND mg/kg Chloroform 0.20ND mg/kg Chloromethane 0.20ND mg/kg 2-Chloroethyl vinyl ether 0.20ND mg/kg 1,2-Dibromo-3-chloropropane 0.20ND mg/kg 1,2-Dibromoethane 0.20ND mg/kg 2-Chlorotoluene 0.20ND mg/kg Dibromomethane 0.20ND mg/kg 1,2-Dichlorobenzene 0.20ND mg/kg 4-Chlorotoluene 0.20ND mg/kg 1,3-Dichlorobenzene 0.20ND mg/kg 1,4-Dichlorobenzene 0.20ND mg/kg Dichlorodifluoromethane 0.20ND mg/kg 1,1-Dichloroethane 0.20ND mg/kg 1,2-Dichloroethane 0.20ND mg/kg 1,1-Dichloroethene 0.20ND mg/kg cis-1,2-Dichloroethene 0.20ND mg/kg trans-1,2-Dichloroethene 0.20ND mg/kg 1,2-Dichloropropane 0.20ND mg/kg 1,3-Dichloropropane 0.20ND mg/kg 2,2-Dichloropropane 0.20ND mg/kg 1,1-Dichloropropene 0.20ND mg/kg cis-1,3-Dichloropropene 0.20ND mg/kg trans-1,3-Dichloropropene 0.20ND mg/kg Ethylbenzene 0.20ND mg/kg Hexachlorobutadiene 0.20ND mg/kg 2-Hexanone 4.0ND mg/kg Iodomethane 0.20ND mg/kg Isopropylbenzene 0.20ND mg/kg p-Isopropyltoluene 0.20ND mg/kg Methyl tert-butyl ether (MTBE)0.20ND mg/kg Methyl ethyl ketone 4.0ND mg/kg Methyl isobutyl ketone 4.0ND mg/kg Methylene chloride 0.20ND mg/kg Naphthalene 0.20ND mg/kg Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 8 of 19226 Project:Ebbighausen Client:Resource Technologies Inc Work Order:B14121551 QA/QC Summary Report 12/24/14Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits Qual Prepared by Billings, MT Branch Method: SW8260B Batch: 85641 Lab ID: mb-85641 12/19/14 13:14Method Blank Run: 5971A.I_141219A n-Propylbenzene 0.20ND mg/kg Styrene 0.20ND mg/kg 1,1,1,2-Tetrachloroethane 0.20ND mg/kg 1,1,2,2-Tetrachloroethane 0.20ND mg/kg Tetrachloroethene 0.20ND mg/kg Toluene 0.20ND mg/kg 1,2,3-Trichlorobenzene 0.20ND mg/kg 1,2,4-Trichlorobenzene 0.20ND mg/kg 1,1,1-Trichloroethane 0.20ND mg/kg 1,1,2-Trichloroethane 0.20ND mg/kg Trichloroethene 0.20ND mg/kg Trichlorofluoromethane 0.20ND mg/kg 1,2,3-Trichloropropane 0.20ND mg/kg 1,2,4-Trimethylbenzene 0.20ND mg/kg 1,3,5-Trimethylbenzene 0.20ND mg/kg Vinyl acetate 0.20ND mg/kg Vinyl chloride 0.20ND mg/kg m+p-Xylenes 0.20ND mg/kg o-Xylene 0.20ND mg/kg Xylenes, Total 0.20ND mg/kg Surr: 1,2-Dichloroethane-d4 92 60 1360.20 Surr: Dibromofluoromethane 94 70 1320.20 Surr: p-Bromofluorobenzene 107 78 1600.20 Surr: Toluene-d8 99 75 1380.20 Lab ID: b14121551-001ams 12/19/14 15:12Sample Matrix Spike Run: 5971A.I_141219A Acetone 107 49 1454.012.9 mg/kg-dry Acetonitrile 86 60 1304.010.3 mg/kg-dry Acrolein 94 19 1974.011.2 mg/kg-dry Acrylonitrile 92 45 1464.011.1 mg/kg-dry Benzene 96 70 1270.201.15 mg/kg-dry Bromobenzene 95 70 1350.201.14 mg/kg-dry Bromochloromethane 110 60 1300.201.32 mg/kg-dry Bromodichloromethane 97 56 1360.201.16 mg/kg-dry Bromoform 83 59 1320.201.000 mg/kg-dry Bromomethane 31 18 1340.200.373 mg/kg-dry n-Butylbenzene 94 71 1340.201.13 mg/kg-dry sec-Butylbenzene 95 67 1320.201.14 mg/kg-dry tert-Butylbenzene 93 68 1340.201.12 mg/kg-dry Carbon disulfide 93 32 1410.201.12 mg/kg-dry Carbon tetrachloride 104 60 1400.201.25 mg/kg-dry Chlorobenzene 95 75 1320.201.14 mg/kg-dry Chlorodibromomethane 86 62 1330.201.03 mg/kg-dry Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 9 of 19227 Project:Ebbighausen Client:Resource Technologies Inc Work Order:B14121551 QA/QC Summary Report 12/24/14Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits Qual Prepared by Billings, MT Branch Method: SW8260B Batch: 85641 Lab ID: b14121551-001ams 12/19/14 15:12Sample Matrix Spike Run: 5971A.I_141219A Chloroethane 30 45 1390.200.360 mg/kg-dry S Chloroform 102 62 1320.201.22 mg/kg-dry Chloromethane 95 41 1380.201.14 mg/kg-dry 2-Chloroethyl vinyl ether 112 41 1490.201.35 mg/kg-dry 1,2-Dibromo-3-chloropropane 77 57 1230.240.924 mg/kg-dry 1,2-Dibromoethane 95 60 1350.201.14 mg/kg-dry 2-Chlorotoluene 85 74 1350.201.02 mg/kg-dry Dibromomethane 108 60 1350.201.30 mg/kg-dry 1,2-Dichlorobenzene 90 70 1300.201.09 mg/kg-dry 4-Chlorotoluene 94 75 1360.201.13 mg/kg-dry 1,3-Dichlorobenzene 88 71 1320.201.06 mg/kg-dry 1,4-Dichlorobenzene 98 71 1310.201.17 mg/kg-dry Dichlorodifluoromethane 67 31 1230.200.800 mg/kg-dry 1,1-Dichloroethane 104 66 1300.201.25 mg/kg-dry 1,2-Dichloroethane 94 51 1400.201.12 mg/kg-dry 1,1-Dichloroethene 96 64 1330.201.15 mg/kg-dry cis-1,2-Dichloroethene 95 63 1310.201.14 mg/kg-dry trans-1,2-Dichloroethene 98 66 1330.201.17 mg/kg-dry 1,2-Dichloropropane 94 60 1300.201.13 mg/kg-dry 1,3-Dichloropropane 96 59 1350.201.15 mg/kg-dry 2,2-Dichloropropane 102 39 1570.201.23 mg/kg-dry 1,1-Dichloropropene 99 65 1320.201.19 mg/kg-dry cis-1,3-Dichloropropene 95 55 1340.201.14 mg/kg-dry trans-1,3-Dichloropropene 94 58 1460.201.13 mg/kg-dry Ethylbenzene 99 74 1360.201.19 mg/kg-dry Hexachlorobutadiene 77 52 1330.200.926 mg/kg-dry 2-Hexanone 107 54 1294.012.9 mg/kg-dry Iodomethane 114 53 1280.201.37 mg/kg-dry Isopropylbenzene 90 70 1330.201.09 mg/kg-dry p-Isopropyltoluene 100 69 1310.201.20 mg/kg-dry Methyl tert-butyl ether (MTBE)91 43 1520.201.10 mg/kg-dry Methyl ethyl ketone 106 43 1484.012.7 mg/kg-dry Methyl isobutyl ketone 102 54 1274.012.2 mg/kg-dry Methylene chloride 91 51 1340.201.10 mg/kg-dry Naphthalene 82 15 1710.200.990 mg/kg-dry n-Propylbenzene 86 72 1340.201.03 mg/kg-dry Styrene 96 70 1350.201.15 mg/kg-dry 1,1,1,2-Tetrachloroethane 93 35 1560.201.12 mg/kg-dry 1,1,2,2-Tetrachloroethane 94 59 1350.201.13 mg/kg-dry Tetrachloroethene 105 64 1390.201.26 mg/kg-dry Toluene 96 73 1370.201.15 mg/kg-dry 1,2,3-Trichlorobenzene 76 24 1530.200.911 mg/kg-dry 1,2,4-Trichlorobenzene 76 34 1500.200.910 mg/kg-dry Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. S - Spike recovery outside of advisory limits. Page 10 of 19228 Project:Ebbighausen Client:Resource Technologies Inc Work Order:B14121551 QA/QC Summary Report 12/24/14Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits Qual Prepared by Billings, MT Branch Method: SW8260B Batch: 85641 Lab ID: b14121551-001ams 12/19/14 15:12Sample Matrix Spike Run: 5971A.I_141219A 1,1,1-Trichloroethane 106 63 1340.201.27 mg/kg-dry 1,1,2-Trichloroethane 94 56 1360.201.12 mg/kg-dry Trichloroethene 96 65 1340.201.15 mg/kg-dry Trichlorofluoromethane 95 48 1400.201.14 mg/kg-dry 1,2,3-Trichloropropane 90 56 1420.201.09 mg/kg-dry 1,2,4-Trimethylbenzene 89 67 1250.201.07 mg/kg-dry 1,3,5-Trimethylbenzene 94 71 1300.201.12 mg/kg-dry Vinyl acetate 99 28 1230.201.19 mg/kg-dry Vinyl chloride 96 32 1360.201.15 mg/kg-dry m+p-Xylenes 96 75 1360.242.32 mg/kg-dry o-Xylene 93 72 1340.201.12 mg/kg-dry Surr: 1,2-Dichloroethane-d4 84 60 1360.20 Surr: Dibromofluoromethane 87 70 1320.20 Surr: p-Bromofluorobenzene 90 78 1600.20 Surr: Toluene-d8 88 75 1380.20 Lab ID: b14121551-001amsd 12/19/14 15:41Sample Matrix Spike Duplicate Run: 5971A.I_141219A Acetone 113 49 145 204.0 5.113.6 mg/kg-dry Acetonitrile 86 60 130 204.0 0.910.4 mg/kg-dry Acrolein 86 19 197 204.0 8.010.4 mg/kg-dry Acrylonitrile 90 45 146 204.0 1.810.9 mg/kg-dry Benzene 95 70 127 200.20 0.81.14 mg/kg-dry Bromobenzene 92 70 135 200.20 3.41.11 mg/kg-dry Bromochloromethane 109 60 130 200.20 0.71.31 mg/kg-dry Bromodichloromethane 99 56 136 200.20 2.41.19 mg/kg-dry Bromoform 85 59 132 200.20 1.91.02 mg/kg-dry Bromomethane 36 18 134 200.20 150.432 mg/kg-dry n-Butylbenzene 94 71 134 200.20 0.91.12 mg/kg-dry sec-Butylbenzene 92 67 132 200.20 3.41.11 mg/kg-dry tert-Butylbenzene 93 68 134 200.20 0.01.12 mg/kg-dry Carbon disulfide 91 32 141 200.20 1.71.10 mg/kg-dry Carbon tetrachloride 106 60 140 200.20 1.51.27 mg/kg-dry Chlorobenzene 94 75 132 200.20 1.71.12 mg/kg-dry Chlorodibromomethane 83 62 133 200.20 2.81.000 mg/kg-dry Chloroethane 29 45 139 200.20 2.20.352 mg/kg-dry S Chloroform 102 62 132 200.20 0.81.23 mg/kg-dry Chloromethane 86 41 138 200.20 111.03 mg/kg-dry 2-Chloroethyl vinyl ether 110 41 149 200.20 2.21.32 mg/kg-dry 1,2-Dibromo-3-chloropropane 87 57 123 200.24 131.05 mg/kg-dry 1,2-Dibromoethane 98 60 135 200.20 2.51.17 mg/kg-dry 2-Chlorotoluene 86 74 135 200.20 0.91.03 mg/kg-dry Dibromomethane 106 60 135 200.20 1.51.28 mg/kg-dry 1,2-Dichlorobenzene 94 70 130 200.20 3.51.12 mg/kg-dry Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. S - Spike recovery outside of advisory limits. Page 11 of 19229 Project:Ebbighausen Client:Resource Technologies Inc Work Order:B14121551 QA/QC Summary Report 12/24/14Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits Qual Prepared by Billings, MT Branch Method: SW8260B Batch: 85641 Lab ID: b14121551-001amsd 12/19/14 15:41Sample Matrix Spike Duplicate Run: 5971A.I_141219A 4-Chlorotoluene 96 75 136 200.20 1.71.15 mg/kg-dry 1,3-Dichlorobenzene 89 71 132 200.20 0.91.07 mg/kg-dry 1,4-Dichlorobenzene 100 71 131 200.20 2.41.20 mg/kg-dry Dichlorodifluoromethane 63 31 123 200.20 5.70.756 mg/kg-dry 1,1-Dichloroethane 106 66 130 200.20 2.31.28 mg/kg-dry 1,2-Dichloroethane 95 51 140 200.20 1.71.14 mg/kg-dry 1,1-Dichloroethene 101 64 133 200.20 4.91.21 mg/kg-dry cis-1,2-Dichloroethene 100 63 131 200.20 4.91.20 mg/kg-dry trans-1,2-Dichloroethene 98 66 133 200.20 0.01.17 mg/kg-dry 1,2-Dichloropropane 96 60 130 200.20 1.71.15 mg/kg-dry 1,3-Dichloropropane 98 59 135 200.20 2.51.18 mg/kg-dry 2,2-Dichloropropane 106 39 157 200.20 3.11.27 mg/kg-dry 1,1-Dichloropropene 100 65 132 200.20 0.81.20 mg/kg-dry cis-1,3-Dichloropropene 94 55 134 200.20 0.81.13 mg/kg-dry trans-1,3-Dichloropropene 92 58 146 200.20 2.61.11 mg/kg-dry Ethylbenzene 101 74 136 200.20 1.61.21 mg/kg-dry Hexachlorobutadiene 83 52 133 200.20 7.71.000 mg/kg-dry 2-Hexanone 110 54 129 204.0 2.913.3 mg/kg-dry Iodomethane 113 53 128 200.20 0.71.36 mg/kg-dry Isopropylbenzene 90 70 133 200.20 0.91.08 mg/kg-dry p-Isopropyltoluene 100 69 131 200.20 0.01.20 mg/kg-dry Methyl tert-butyl ether (MTBE)90 43 152 200.20 1.81.08 mg/kg-dry Methyl ethyl ketone 110 43 148 204.0 4.413.3 mg/kg-dry Methyl isobutyl ketone 101 54 127 204.0 0.812.1 mg/kg-dry Methylene chloride 93 51 134 200.20 1.71.12 mg/kg-dry Naphthalene 98 15 171 200.20 171.17 mg/kg-dry n-Propylbenzene 85 72 134 200.20 0.91.02 mg/kg-dry Styrene 96 70 135 200.20 0.01.15 mg/kg-dry 1,1,1,2-Tetrachloroethane 95 35 156 200.20 2.61.14 mg/kg-dry 1,1,2,2-Tetrachloroethane 96 59 135 200.20 1.71.15 mg/kg-dry Tetrachloroethene 104 64 139 200.20 0.81.25 mg/kg-dry Toluene 96 73 137 200.20 0.01.15 mg/kg-dry 1,2,3-Trichlorobenzene 95 24 153 200.20 231.14 mg/kg-dry R 1,2,4-Trichlorobenzene 87 34 150 200.20 141.05 mg/kg-dry 1,1,1-Trichloroethane 105 63 134 200.20 0.81.26 mg/kg-dry 1,1,2-Trichloroethane 94 56 136 200.20 0.91.13 mg/kg-dry Trichloroethene 90 65 134 200.20 6.91.08 mg/kg-dry Trichlorofluoromethane 86 48 140 200.20 111.03 mg/kg-dry 1,2,3-Trichloropropane 90 56 142 200.20 0.91.08 mg/kg-dry 1,2,4-Trimethylbenzene 88 67 125 200.20 0.91.06 mg/kg-dry 1,3,5-Trimethylbenzene 95 71 130 200.20 1.71.14 mg/kg-dry Vinyl acetate 97 28 123 200.20 2.41.16 mg/kg-dry Vinyl chloride 89 32 136 200.20 7.81.07 mg/kg-dry Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. R - RPD exceeds advisory limit. Page 12 of 19230 Project:Ebbighausen Client:Resource Technologies Inc Work Order:B14121551 QA/QC Summary Report 12/24/14Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits Qual Prepared by Billings, MT Branch Method: SW8260B Batch: 85641 Lab ID: b14121551-001amsd 12/19/14 15:41Sample Matrix Spike Duplicate Run: 5971A.I_141219A m+p-Xylenes 98 75 136 200.24 1.22.35 mg/kg-dry o-Xylene 94 72 134 200.20 1.71.13 mg/kg-dry Surr: 1,2-Dichloroethane-d4 84 60 1360.20 Surr: Dibromofluoromethane 84 70 1320.20 Surr: p-Bromofluorobenzene 86 78 1600.20 Surr: Toluene-d8 84 75 1380.20 Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 13 of 19231 Project:Ebbighausen Client:Resource Technologies Inc Work Order:B14121551 QA/QC Summary Report 12/24/14Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits Qual Prepared by Billings, MT Branch Method: SW8015M Batch: 85666 Lab ID: LCS-85666 12/19/14 15:48Laboratory Control Sample Run: GCFID-HP2-B_141218C Total Extractable Hydrocarbons 84 60 14010174 mg/kg Surr: o-Terphenyl 84 40 1400.17 Lab ID: MB-85666 12/19/14 16:32Method Blank Run: GCFID-HP2-B_141218C Total Extractable Hydrocarbons 10ND mg/kg Surr: o-Terphenyl 89 40 1400.17 Lab ID: B14121514-002AMS 12/19/14 18:05Sample Matrix Spike Run: GCFID-HP2-B_141218C Total Extractable Hydrocarbons 86 60 14013269 mg/kg-dry Surr: o-Terphenyl 80 40 1400.22 Lab ID: B14121514-002AMSD 12/19/14 18:49Sample Matrix Spike Duplicate Run: GCFID-HP2-B_141218C Total Extractable Hydrocarbons 86 60 140 20130.4270 mg/kg-dry Surr: o-Terphenyl 78 40 1400.22 Method: SW8015M Analytical Run: R235698 Lab ID: CCV_1218HP234r-S 12/19/14 14:21Continuing Calibration Verification Standard n-Nonane 95 75 1256.33 mg/kg n-Decane 98 75 1256.54 mg/kg n-Dodecane 101 75 1256.70 mg/kg n-Tetradecane 104 75 1256.92 mg/kg n-Hexadecane 106 75 1257.06 mg/kg n-Octadecane 106 75 1257.05 mg/kg n-Nonadecane 108 75 1257.21 mg/kg n-Eicosane 108 75 1257.17 mg/kg n-Docosane 108 75 1257.22 mg/kg n-Tetracosane 111 75 1257.40 mg/kg n-Hexacosane 111 75 1257.42 mg/kg n-Octacosane 112 75 1257.46 mg/kg n-Triacontane 111 75 1257.42 mg/kg n-Hexatriacontane 102 75 1256.79 mg/kg Surr: o-Terphenyl 101 75 1250.17 Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 14 of 19232 MW-1 3-4 Batch ID: 85666 EXTRACTABLE PETROLEUM HYDROCARBONS (EPH) SCREENING ANALYSIS CHROMATOGRAM Sample Name: B14121551-001A ;1218HP2 , $HC-EPH-SCRN-S, V46 Raw File: G:\org\HP2\DAT\HP2121814_b\1218HP2.0046.RAW Date & Time Acquired: 12/19/2014 11:22:53 PM Method File: g:\org\HP2\Methods\S3_SCN-WE-L%.met Calibration File: G:\Org\HP2\Cals\SC110829WE.CAL Sample Weight: 30 Dilution: 2 S.A.: 1 Mean RF for C9 to C18 Hydrocarbons: 27187.9 Mean RF for C19 to C36 Hydrocarbons: 27480.28 Mean RF for Total Extractable Hydrocarbons: 27334.08 Rt range for Diesel Range Organics: 5.924 to 16.075 Rt range for C9 to C18 Hydrocarbons: 4.894 to 11.675 Rt range for C19 to C36 Hydrocarbons: 11.71 to 18.044 SURROGATE COMPOUND RT ACTUAL MEASURED %REC *o-Terphenyl_____________11.743 6.667 5.322 79.83 - *1-Chloro-octadecane_____12.581 6.667 5.593 83.9 - DRO Area:3281863 DRO Amount: 8.004323 TEH Area:2.027716E+07 TEH Amount: 49.45514 C9-C18 Area:178217.9 C9-C18 Amount: 0.4370029 C19-C36 Area:1.117761E+07C19-C36 Amount: 27.11669 3.54 4.23 4.43 4.55 4.66 4.71 4.77 4.98 5.01 5.15 5.31 5.49 5.52 5.59 6.12 6.23 6.99 7.08 7.27 7.67 7.73 8.14 8.18 8.27 8.34 8.41 8.47 8.64 8.70 8.82 8.98 9.06 9.19 9.34 9.43 9.57 9.77 9.87 9.94 10.04 10.15 10.19 10.40 10.49 10.58 10.65 10.71 10.84 11.01 11.20 11.25 11.33 11.43 11.52 11.62 11.74 11.91 11.99 12.11 12.17 12.28 12.41 12.48 12.58 12.84 12.90 13.06 13.19 13.29 13.39 13.48 13.61 13.75 13.89 14.02 14.21 14.27 14.41 14.54 14.65 14.78 14.93 15.02 15.14 15.27 15.36 15.50 15.71 16.03 16.08 16.17 16.37 16.56 16.64 16.72 16.80 16.94 17.02 17.17 17.34 17.47 17.56 17.64 17.79 17.89 17.98 18.12 18.38 18.54 18.86 19.16 19.74 19.86 19.92 20.62 21.01 21.10 21.28 21.37 21.42 21.62 22.09 22.14 22.19 22.24 22.61 22.66 22.70 23.14 23.18 23.28 23.43 23.55 23.59 23.62 23.66 23.71 24.03 24.06 24.57 24.64 24.73 24.80 24.84 24.92 24.96 25.07 25.10 25.13 25.20 25.25 25.34 25.40 25.52 25.59 25.65 26.08 26.24 26.37 26.49 26.70 26.75 26.82 26.93 27.42 27.47 28.11 28.17 28.36 28.41 28.48 28.52 28.59 28.66 28.81 28.86 29.00 29.13 29.16 29.28 29.61 n-Nonane n-Decane n-Dodecane n-Tetradecane n-Hexadecane n-Octadecane n-Nonadecane *o-Terphenyl n-Eicosane *1-Chloro-octadecane n-Docosane n-Tetracosane n-Hexacosane n-Octacosane n-Triacontane n-Hexatriacontane G:\org\HP2\DAT\HP2121814_b\1218HP2.0046.RAW B14121551-001A ;1218HP2 , $HC-EPH-SCRN-S, V46 0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 0 500 1000 1500 2000 2500 3000 Page 15 of 19233 MW-2 5-6 Batch ID: 85666 EXTRACTABLE PETROLEUM HYDROCARBONS (EPH) SCREENING ANALYSIS CHROMATOGRAM Sample Name: B14121551-002A ;1218HP2 , $HC-EPH-SCRN-S, V45 Raw File: G:\org\HP2\DAT\HP2121814_b\1218HP2.0045.RAW Date & Time Acquired: 12/19/2014 10:30:33 PM Method File: g:\org\HP2\Methods\SR_SCN-WE-L%.met Calibration File: G:\Org\HP2\Cals\SC110829WE.CAL Sample Weight: 30 Dilution: 2 S.A.: 1 Mean RF for C9 to C18 Hydrocarbons: 27187.9 Mean RF for C19 to C36 Hydrocarbons: 27480.28 Mean RF for Total Extractable Hydrocarbons: 27334.08 Rt range for Diesel Range Organics: 5.924 to 16.075 Rt range for C9 to C18 Hydrocarbons: 4.894 to 11.675 Rt range for C19 to C36 Hydrocarbons: 11.71 to 18.044 SURROGATE COMPOUND RT ACTUAL MEASURED %REC *o-Terphenyl_____________11.747 6.667 5.778 86.67 - *1-Chloro-octadecane_____12.586 6.667 6.16 92.4 - DRO Area:241938.5 DRO Amount: 0.5900777 TEH Area:367310.5 TEH Amount: 0.8958547 C9-C18 Area:145740.2 C9-C18 Amount: 0.3573654 C19-C36 Area:181022 C19-C36 Amount: 0.4391562 3.50 3.59 4.24 4.55 4.65 4.71 4.79 4.94 5.02 5.15 5.33 5.44 5.53 5.93 6.01 6.12 6.23 6.32 6.37 6.48 6.67 6.83 6.98 7.23 7.27 7.61 7.68 7.72 7.76 7.89 8.09 8.14 8.19 8.23 8.30 8.37 8.48 8.64 8.72 8.85 8.94 8.97 9.07 9.34 9.45 9.54 9.82 9.92 10.17 10.43 10.50 10.69 11.04 11.20 11.34 11.38 11.57 11.63 11.75 11.96 12.12 12.18 12.29 12.33 12.59 13.06 13.20 13.30 13.35 13.40 13.48 13.76 13.89 14.28 14.50 14.66 15.02 15.35 15.44 15.50 15.70 15.75 15.95 16.08 16.18 16.35 16.42 16.57 16.81 16.95 17.03 17.18 17.57 17.80 18.01 18.14 18.68 20.00 24.09 26.46 n-Nonane n-Decane n-Dodecane n-Tetradecane n-Hexadecane n-Octadecane n-Nonadecane *o-Terphenyl n-Eicosane *1-Chloro-octadecane n-Docosane n-Tetracosane n-Hexacosane n-Octacosane n-Triacontane n-Hexatriacontane G:\org\HP2\DAT\HP2121814_b\1218HP2.0045.RAW B14121551-002A ;1218HP2 , $HC-EPH-SCRN-S, V45 0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 0 500 1000 1500 2000 2500 3000 Page 16 of 19234 MW-1 3-4 (Silica Gel Treatment)Batch ID: 85666 EXTRACTABLE PETROLEUM HYDROCARBONS (EPH) SCREENING ANALYSIS CHROMATOGRAM Sample Name: B14121551-001A ;1229HP2 , $HC-EPH-SCRN-S, SGT-V06 Raw File: G:\org\HP2\DAT\HP2122914_b\1229HP2.0006.RAW Date & Time Acquired: 12/29/2014 2:18:11 PM Method File: g:\org\HP2\Methods\SR_SCN-122906-WF-L%.met Calibration File: G:\Org\HP2\Cals\SC110829WF.CAL Sample Weight: 30 Dilution: 2 S.A.: 1 Mean RF for C9 to C18 Hydrocarbons: 27187.9 Mean RF for C19 to C36 Hydrocarbons: 27480.28 Mean RF for Total Extractable Hydrocarbons: 27334.08 Rt range for Diesel Range Organics: 6.09 to 16.2 Rt range for C9 to C18 Hydrocarbons: 5.1 to 11.82 Rt range for C19 to C36 Hydrocarbons: 11.855 to 18.23 SURROGATE COMPOUND RT ACTUAL MEASURED %REC *o-Terphenyl_____________11.866 6.667 5.069 76.04 - *1-Chloro-octadecane_____12.696 6.667 5.486 82.29 - DRO Area:1528382 DRO Amount: 3.727659 TEH Area:4501137 TEH Amount: 10.97808 C9-C18 Area:629612.8 C9-C18 Amount: 1.543855 C19-C36 Area:2922362 C19-C36 Amount: 7.089598 4.05 4.16 4.27 4.37 4.42 4.50 4.56 4.65 4.77 4.91 4.97 5.10 5.16 5.19 5.36 5.48 5.60 5.67 5.92 5.96 6.15 6.30 6.38 6.44 6.48 6.84 6.95 7.11 7.14 7.26 7.32 7.42 7.57 7.82 7.87 7.97 8.17 8.32 8.40 8.47 8.61 8.70 8.78 8.84 8.94 9.11 9.32 9.46 9.56 9.69 9.91 10.02 10.09 10.26 10.53 10.62 10.72 10.82 11.02 11.13 11.32 11.43 11.53 11.63 11.67 11.74 11.87 12.23 12.28 12.41 12.57 12.70 13.03 13.18 13.31 13.43 13.51 13.59 13.73 14.00 14.13 14.24 14.38 14.52 14.61 14.76 14.90 15.12 15.26 15.37 15.47 15.61 15.80 15.95 16.06 16.13 16.28 16.45 16.60 16.76 16.91 17.05 17.15 17.22 17.31 17.44 17.55 17.71 17.83 17.93 18.10 18.22 18.34 18.56 18.76 18.93 19.08 19.12 19.33 19.47 19.53 19.60 19.73 19.86 19.91 19.95 19.99 20.04 20.24 20.47 21.06 21.55 21.61 21.75 22.09 22.62 22.69 22.73 23.26 24.00 24.08 24.30 24.67 25.72 26.10 26.31 26.36 26.97 27.19 27.32 27.39 27.51 27.67 28.30 28.87 28.99 29.08 n-Nonane n-Decane n-Dodecane n-Tetradecane n-Hexadecane n-Octadecane n-Nonadecane *o-Terphenyl n-Eicosane *1-Chloro-octadecane n-Docosane n-Tetracosane n-Hexacosane n-Octacosane n-Triacontane n-Hexatriacontane G:\org\HP2\DAT\HP2122914_b\1229HP2.0006.RAW B14121551-001A ;1229HP2 , $HC-EPH-SCRN-S, SGT-V06 0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 0 500 1000 1500 2000 2500 3000 Page 17 of 19235 Shipping container/cooler in good condition? Custody seals intact on all shipping container(s)/cooler(s)? Custody seals intact on all sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res Cl, Sulfite, Ferrous Iron, etc.) Container/Temp Blank temperature: Water - VOA vials have zero headspace? Water - pH acceptable upon receipt? Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes No No No No No No No No No No No No Not Present Not Present Not Present No VOA vials submitted Not Applicable 2.4°C On Ice 12/17/2014Leslie S. Cadreau Return-UPS Ground lg Date Received: Received by: Login completed by: Carrier name: BL2000\jmueller 12/17/2014 Reviewed by: Reviewed Date: Contact and Corrective Action Comments: None Temp Blank received in all shipping container(s)/cooler(s)? Yes No Not Applicable Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as –dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Standard Reporting Procedures: Workorder Receipt Checklist Resource Technologies Inc B14121551 Page 18 of 19236 Page 19 of 19237 APPENDIX B Soil Borehole Logs 238 239 240 APPENDIX C Laboratory Analytical Reports - Groundwater 241 ANALYTICAL SUMMARY REPORTANALYTICAL SUMMARY REPORTANALYTICAL SUMMARY REPORTANALYTICAL SUMMARY REPORT The analyses presented in this report were performed by Energy Laboratories, Inc., 1120 S 27th St., Billings, MT 59101, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Lab ID Client Sample ID Collect Date Receive Date Matrix Test Report Approved By: B14121909-001 MW-1 12/22/14 13:16 12/23/14 Aqueous EPH-Liquid-Liquid Extraction Hydrocarbons, Extractable Petroleum Screen 8260-Volatile Organic Compounds- Short List B14121909-002 MW-2 12/22/14 12:30 12/23/14 Aqueous Same As Above Resource Technologies Inc Project Name: Ebbighausen Work Order: B14121909 1050 E Main St Ste 4 Bozeman, MT 59715 January 05, 2015 Energy Laboratories Inc Billings MT received the following 2 samples for Resource Technologies Inc on 12/23/2014 for analysis. Page 1 of 16242 LABORATORY ANALYTICAL REPORT Client:Resource Technologies Inc Project:Ebbighausen Lab ID:B14121909-001 Client Sample ID:MW-1 Collection Date:12/22/14 13:16 Matrix:Aqueous Report Date:01/05/15 DateReceived:12/23/14 Prepared by Billings, MT Branch Analyses Result Units Analysis Date / ByRLMethod MCL/ QCLQualifiers VOLATILE ORGANIC COMPOUNDS 12/24/14 10:29 / nl1.0ug/LNDBenzene SW8260B 12/24/14 10:29 / nl1.0ug/LNDBromobenzene SW8260B 12/24/14 10:29 / nl1.0ug/LNDBromochloromethane SW8260B 12/24/14 10:29 / nl1.0ug/LNDBromodichloromethane SW8260B 12/24/14 10:29 / nl1.0ug/LNDBromoform SW8260B 12/24/14 10:29 / nl1.0ug/LNDBromomethane SW8260B 12/24/14 10:29 / nl1.0ug/LNDCarbon tetrachloride SW8260B 12/24/14 10:29 / nl1.0ug/LNDChlorobenzene SW8260B 12/24/14 10:29 / nl1.0ug/LNDChlorodibromomethane SW8260B 12/24/14 10:29 / nl1.0ug/LNDChloroethane SW8260B 12/24/14 10:29 / nl1.0ug/LNDChloroform SW8260B 12/24/14 10:29 / nl1.0ug/LNDChloromethane SW8260B 12/24/14 10:29 / nl1.0ug/LND1,2-Dibromoethane SW8260B 12/24/14 10:29 / nl1.0ug/LND2-Chlorotoluene SW8260B 12/24/14 10:29 / nl1.0ug/LND4-Chlorotoluene SW8260B 12/24/14 10:29 / nl1.0ug/LNDDibromomethane SW8260B 12/24/14 10:29 / nl1.0ug/LND1,2-Dichlorobenzene SW8260B 12/24/14 10:29 / nl1.0ug/LND1,3-Dichlorobenzene SW8260B 12/24/14 10:29 / nl1.0ug/LND1,4-Dichlorobenzene SW8260B 12/24/14 10:29 / nl1.0ug/LNDDichlorodifluoromethane SW8260B 12/24/14 10:29 / nl1.0ug/LND1,1-Dichloroethane SW8260B 12/24/14 10:29 / nl1.0ug/LND1,2-Dichloroethane SW8260B 12/24/14 10:29 / nl1.0ug/LND1,1-Dichloroethene SW8260B 12/24/14 10:29 / nl1.0ug/LNDcis-1,2-Dichloroethene SW8260B 12/24/14 10:29 / nl1.0ug/LNDtrans-1,2-Dichloroethene SW8260B 12/24/14 10:29 / nl1.0ug/LND1,2-Dichloropropane SW8260B 12/24/14 10:29 / nl1.0ug/LND1,3-Dichloropropane SW8260B 12/24/14 10:29 / nl1.0ug/LND2,2-Dichloropropane SW8260B 12/24/14 10:29 / nl1.0ug/LND1,1-Dichloropropene SW8260B 12/24/14 10:29 / nl1.0ug/LNDcis-1,3-Dichloropropene SW8260B 12/24/14 10:29 / nl1.0ug/LNDtrans-1,3-Dichloropropene SW8260B 12/24/14 10:29 / nl1.0ug/LNDEthylbenzene SW8260B 12/24/14 10:29 / nl20ug/LNDMethyl ethyl ketone SW8260B 12/24/14 10:29 / nl1.0ug/LNDMethyl tert-butyl ether (MTBE)SW8260B 12/24/14 10:29 / nl1.0ug/LNDMethylene chloride SW8260B 12/24/14 10:29 / nl1.0ug/LNDStyrene SW8260B 12/24/14 10:29 / nl1.0ug/LND1,1,1,2-Tetrachloroethane SW8260B 12/24/14 10:29 / nl1.0ug/LND1,1,2,2-Tetrachloroethane SW8260B 12/24/14 10:29 / nl1.0ug/LNDTetrachloroethene SW8260B J 12/24/14 10:29 / nl1.0ug/L0.14Toluene SW8260B 12/24/14 10:29 / nl1.0ug/LND1,1,1-Trichloroethane SW8260B 12/24/14 10:29 / nl1.0ug/LND1,1,2-Trichloroethane SW8260B 12/24/14 10:29 / nl1.0ug/LNDTrichloroethene SW8260B Report Definitions: RL - Analyte reporting limit.MCL - Maximum contaminant level. QCL - Quality control limit.ND - Not detected at the reporting limit. J - Estimated value. The analyte was present but less than the reporting limit. Page 2 of 16243 LABORATORY ANALYTICAL REPORT Client:Resource Technologies Inc Project:Ebbighausen Lab ID:B14121909-001 Client Sample ID:MW-1 Collection Date:12/22/14 13:16 Matrix:Aqueous Report Date:01/05/15 DateReceived:12/23/14 Prepared by Billings, MT Branch Analyses Result Units Analysis Date / ByRLMethod MCL/ QCLQualifiers VOLATILE ORGANIC COMPOUNDS 12/24/14 10:29 / nl1.0ug/LNDTrichlorofluoromethane SW8260B 12/24/14 10:29 / nl1.0ug/LND1,2,3-Trichloropropane SW8260B 12/24/14 10:29 / nl1.0ug/LNDVinyl chloride SW8260B 12/24/14 10:29 / nl1.0ug/LNDm+p-Xylenes SW8260B 12/24/14 10:29 / nl1.0ug/LNDo-Xylene SW8260B 12/24/14 10:29 / nl1.0ug/LNDXylenes, Total SW8260B 12/24/14 10:29 / nl77-126%REC106 Surr: Dibromofluoromethane SW8260B 12/24/14 10:29 / nl70-130%REC101 Surr: 1,2-Dichloroethane-d4 SW8260B 12/24/14 10:29 / nl79-122%REC114 Surr: Toluene-d8 SW8260B 12/24/14 10:29 / nl76-127%REC116 Surr: p-Bromofluorobenzene SW8260B EXTRACTABLE PETROLEUM HYDROCARBONS-SCREEN 01/03/15 18:49 / tmc309ug/LNDTotal Extractable Hydrocarbons SW8015M1000 01/03/15 18:49 / tmc40-140%REC50.0 Surr: o-Terphenyl SW8015M - Note: Total Extractable Hydrocarbons are defined as the total hydrocarbon responses regardless of elution time. Report Definitions: RL - Analyte reporting limit.MCL - Maximum contaminant level. QCL - Quality control limit.ND - Not detected at the reporting limit. Page 3 of 16244 LABORATORY ANALYTICAL REPORT Client:Resource Technologies Inc Project:Ebbighausen Lab ID:B14121909-002 Client Sample ID:MW-2 Collection Date:12/22/14 12:30 Matrix:Aqueous Report Date:01/05/15 DateReceived:12/23/14 Prepared by Billings, MT Branch Analyses Result Units Analysis Date / ByRLMethod MCL/ QCLQualifiers VOLATILE ORGANIC COMPOUNDS 12/24/14 10:57 / nl1.0ug/LNDBenzene SW8260B 12/24/14 10:57 / nl1.0ug/LNDBromobenzene SW8260B 12/24/14 10:57 / nl1.0ug/LNDBromochloromethane SW8260B 12/24/14 10:57 / nl1.0ug/LNDBromodichloromethane SW8260B 12/24/14 10:57 / nl1.0ug/LNDBromoform SW8260B 12/24/14 10:57 / nl1.0ug/LNDBromomethane SW8260B 12/24/14 10:57 / nl1.0ug/LNDCarbon tetrachloride SW8260B 12/24/14 10:57 / nl1.0ug/LNDChlorobenzene SW8260B 12/24/14 10:57 / nl1.0ug/LNDChlorodibromomethane SW8260B J 12/24/14 10:57 / nl1.0ug/L0.11Chloroethane SW8260B 12/24/14 10:57 / nl1.0ug/LNDChloroform SW8260B 12/24/14 10:57 / nl1.0ug/LNDChloromethane SW8260B 12/24/14 10:57 / nl1.0ug/LND1,2-Dibromoethane SW8260B 12/24/14 10:57 / nl1.0ug/LND2-Chlorotoluene SW8260B 12/24/14 10:57 / nl1.0ug/LND4-Chlorotoluene SW8260B 12/24/14 10:57 / nl1.0ug/LNDDibromomethane SW8260B 12/24/14 10:57 / nl1.0ug/LND1,2-Dichlorobenzene SW8260B 12/24/14 10:57 / nl1.0ug/LND1,3-Dichlorobenzene SW8260B 12/24/14 10:57 / nl1.0ug/LND1,4-Dichlorobenzene SW8260B 12/24/14 10:57 / nl1.0ug/LNDDichlorodifluoromethane SW8260B 12/24/14 10:57 / nl1.0ug/LND1,1-Dichloroethane SW8260B 12/24/14 10:57 / nl1.0ug/LND1,2-Dichloroethane SW8260B 12/24/14 10:57 / nl1.0ug/LND1,1-Dichloroethene SW8260B 12/24/14 10:57 / nl1.0ug/LNDcis-1,2-Dichloroethene SW8260B 12/24/14 10:57 / nl1.0ug/LNDtrans-1,2-Dichloroethene SW8260B 12/24/14 10:57 / nl1.0ug/LND1,2-Dichloropropane SW8260B 12/24/14 10:57 / nl1.0ug/LND1,3-Dichloropropane SW8260B 12/24/14 10:57 / nl1.0ug/LND2,2-Dichloropropane SW8260B 12/24/14 10:57 / nl1.0ug/LND1,1-Dichloropropene SW8260B 12/24/14 10:57 / nl1.0ug/LNDcis-1,3-Dichloropropene SW8260B 12/24/14 10:57 / nl1.0ug/LNDtrans-1,3-Dichloropropene SW8260B 12/24/14 10:57 / nl1.0ug/LNDEthylbenzene SW8260B 12/24/14 10:57 / nl20ug/LNDMethyl ethyl ketone SW8260B 12/24/14 10:57 / nl1.0ug/LNDMethyl tert-butyl ether (MTBE)SW8260B 12/24/14 10:57 / nl1.0ug/LNDMethylene chloride SW8260B 12/24/14 10:57 / nl1.0ug/LNDStyrene SW8260B 12/24/14 10:57 / nl1.0ug/LND1,1,1,2-Tetrachloroethane SW8260B 12/24/14 10:57 / nl1.0ug/LND1,1,2,2-Tetrachloroethane SW8260B 12/24/14 10:57 / nl1.0ug/LNDTetrachloroethene SW8260B J 12/24/14 10:57 / nl1.0ug/L0.19Toluene SW8260B 12/24/14 10:57 / nl1.0ug/LND1,1,1-Trichloroethane SW8260B 12/24/14 10:57 / nl1.0ug/LND1,1,2-Trichloroethane SW8260B 12/24/14 10:57 / nl1.0ug/LNDTrichloroethene SW8260B Report Definitions: RL - Analyte reporting limit.MCL - Maximum contaminant level. QCL - Quality control limit.ND - Not detected at the reporting limit. J - Estimated value. The analyte was present but less than the reporting limit. Page 4 of 16245 LABORATORY ANALYTICAL REPORT Client:Resource Technologies Inc Project:Ebbighausen Lab ID:B14121909-002 Client Sample ID:MW-2 Collection Date:12/22/14 12:30 Matrix:Aqueous Report Date:01/05/15 DateReceived:12/23/14 Prepared by Billings, MT Branch Analyses Result Units Analysis Date / ByRLMethod MCL/ QCLQualifiers VOLATILE ORGANIC COMPOUNDS 12/24/14 10:57 / nl1.0ug/LNDTrichlorofluoromethane SW8260B 12/24/14 10:57 / nl1.0ug/LND1,2,3-Trichloropropane SW8260B J 12/24/14 10:57 / nl1.0ug/L0.52Vinyl chloride SW8260B 12/24/14 10:57 / nl1.0ug/LNDm+p-Xylenes SW8260B 12/24/14 10:57 / nl1.0ug/LNDo-Xylene SW8260B 12/24/14 10:57 / nl1.0ug/LNDXylenes, Total SW8260B 12/24/14 10:57 / nl77-126%REC106 Surr: Dibromofluoromethane SW8260B 12/24/14 10:57 / nl70-130%REC103 Surr: 1,2-Dichloroethane-d4 SW8260B 12/24/14 10:57 / nl79-122%REC113 Surr: Toluene-d8 SW8260B 12/24/14 10:57 / nl76-127%REC117 Surr: p-Bromofluorobenzene SW8260B EXTRACTABLE PETROLEUM HYDROCARBONS-SCREEN 01/03/15 21:43 / tmc316ug/LNDTotal Extractable Hydrocarbons SW8015M1000 01/03/15 21:43 / tmc40-140%REC52.0 Surr: o-Terphenyl SW8015M - Note: Total Extractable Hydrocarbons are defined as the total hydrocarbon responses regardless of elution time. Report Definitions: RL - Analyte reporting limit.MCL - Maximum contaminant level. QCL - Quality control limit.ND - Not detected at the reporting limit. J - Estimated value. The analyte was present but less than the reporting limit. Page 5 of 16246 Project:Ebbighausen Client:Resource Technologies Inc Work Order:B14121909 QA/QC Summary Report 01/05/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits Qual Prepared by Billings, MT Branch Method: SW8260B Batch: R235880 Lab ID: LCS_122414 12/24/14 09:03Laboratory Control Sample Run: SV5972.I_141224A Benzene 99 71 1331.04.96 ug/L Bromobenzene 109 78 1331.05.44 ug/L Bromochloromethane 111 68 1311.05.56 ug/L Bromodichloromethane 104 67 1381.05.20 ug/L Bromoform 113 64 1361.05.64 ug/L Bromomethane 104 60 1381.05.20 ug/L Carbon tetrachloride 85 61 1441.04.24 ug/L Chlorobenzene 100 78 1361.05.00 ug/L Chlorodibromomethane 104 72 1361.05.20 ug/L Chloroethane 94 64 1361.04.68 ug/L Chloroform 107 69 1331.05.36 ug/L Chloromethane 89 63 1491.04.44 ug/L 1,2-Dibromoethane 105 75 1311.05.24 ug/L 2-Chlorotoluene 100 74 1351.05.00 ug/L Dibromomethane 111 72 1331.05.56 ug/L 1,2-Dichlorobenzene 105 78 1291.05.24 ug/L 4-Chlorotoluene 105 79 1351.05.24 ug/L 1,3-Dichlorobenzene 105 79 1321.05.24 ug/L 1,4-Dichlorobenzene 106 78 1311.05.28 ug/L Dichlorodifluoromethane 82 55 1411.04.08 ug/L 1,1-Dichloroethane 113 72 1301.05.64 ug/L 1,2-Dichloroethane 98 57 1461.04.92 ug/L 1,1-Dichloroethene 102 66 1421.05.12 ug/L cis-1,2-Dichloroethene 107 74 1331.05.36 ug/L trans-1,2-Dichloroethene 97 76 1381.04.84 ug/L 1,2-Dichloropropane 102 72 1351.05.12 ug/L 1,3-Dichloropropane 98 75 1341.04.92 ug/L 2,2-Dichloropropane 120 42 1671.06.00 ug/L 1,1-Dichloropropene 103 72 1401.05.16 ug/L cis-1,3-Dichloropropene 105 75 1321.05.24 ug/L trans-1,3-Dichloropropene 114 77 1451.05.72 ug/L Ethylbenzene 108 78 1311.05.40 ug/L Methyl tert-butyl ether (MTBE)82 58 1511.04.12 ug/L Methyl ethyl ketone 106 55 1452052.8 ug/L Methylene chloride 90 73 1261.04.48 ug/L Styrene 110 76 1341.05.52 ug/L 1,1,1,2-Tetrachloroethane 104 75 1351.05.20 ug/L 1,1,2,2-Tetrachloroethane 101 72 1321.05.04 ug/L Tetrachloroethene 115 78 1371.05.76 ug/L Toluene 108 78 1341.05.40 ug/L 1,1,1-Trichloroethane 110 64 1411.05.52 ug/L 1,1,2-Trichloroethane 99 72 1331.04.96 ug/L Trichloroethene 105 75 1381.05.24 ug/L Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 6 of 16247 Project:Ebbighausen Client:Resource Technologies Inc Work Order:B14121909 QA/QC Summary Report 01/05/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits Qual Prepared by Billings, MT Branch Method: SW8260B Batch: R235880 Lab ID: LCS_122414 12/24/14 09:03Laboratory Control Sample Run: SV5972.I_141224A Trichlorofluoromethane 81 58 1391.04.04 ug/L 1,2,3-Trichloropropane 98 67 1331.04.92 ug/L Vinyl chloride 82 66 1401.04.08 ug/L m+p-Xylenes 108 78 1331.010.8 ug/L o-Xylene 105 79 1361.05.24 ug/L Xylenes, Total 107 78 1361.016.0 ug/L Surr: 1,2-Dichloroethane-d4 101 70 1301.0 Surr: Dibromofluoromethane 105 77 1261.0 Surr: p-Bromofluorobenzene 108 76 1271.0 Surr: Toluene-d8 114 79 1221.0 Lab ID: BLK_122414 12/24/14 10:00Method Blank Run: SV5972.I_141224A Benzene 0.50ND ug/L Bromobenzene 0.50ND ug/L Bromochloromethane 0.50ND ug/L Bromodichloromethane 0.50ND ug/L Bromoform 0.50ND ug/L Bromomethane 0.50ND ug/L Carbon tetrachloride 0.50ND ug/L Chlorobenzene 0.50ND ug/L Chlorodibromomethane 0.50ND ug/L Chloroethane 0.50ND ug/L Chloroform 0.50ND ug/L Chloromethane 0.50ND ug/L 1,2-Dibromoethane 0.50ND ug/L 2-Chlorotoluene 0.50ND ug/L Dibromomethane 0.50ND ug/L 1,2-Dichlorobenzene 0.50ND ug/L 4-Chlorotoluene 0.50ND ug/L 1,3-Dichlorobenzene 0.50ND ug/L 1,4-Dichlorobenzene 0.50ND ug/L Dichlorodifluoromethane 0.50ND ug/L 1,1-Dichloroethane 0.50ND ug/L 1,2-Dichloroethane 0.50ND ug/L 1,1-Dichloroethene 0.50ND ug/L cis-1,2-Dichloroethene 0.50ND ug/L trans-1,2-Dichloroethene 0.50ND ug/L 1,2-Dichloropropane 0.50ND ug/L 1,3-Dichloropropane 0.50ND ug/L 2,2-Dichloropropane 0.50ND ug/L 1,1-Dichloropropene 0.50ND ug/L cis-1,3-Dichloropropene 0.50ND ug/L trans-1,3-Dichloropropene 0.50ND ug/L Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 7 of 16248 Project:Ebbighausen Client:Resource Technologies Inc Work Order:B14121909 QA/QC Summary Report 01/05/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits Qual Prepared by Billings, MT Branch Method: SW8260B Batch: R235880 Lab ID: BLK_122414 12/24/14 10:00Method Blank Run: SV5972.I_141224A Ethylbenzene 0.50ND ug/L Methyl tert-butyl ether (MTBE)0.50ND ug/L Methyl ethyl ketone 10ND ug/L Methylene chloride 0.50ND ug/L Styrene 0.50ND ug/L 1,1,1,2-Tetrachloroethane 0.50ND ug/L 1,1,2,2-Tetrachloroethane 0.50ND ug/L Tetrachloroethene 0.50ND ug/L Toluene 0.50ND ug/L 1,1,1-Trichloroethane 0.50ND ug/L 1,1,2-Trichloroethane 0.50ND ug/L Trichloroethene 0.50ND ug/L Trichlorofluoromethane 0.50ND ug/L 1,2,3-Trichloropropane 0.50ND ug/L Vinyl chloride 0.50ND ug/L m+p-Xylenes 0.50ND ug/L o-Xylene 0.50ND ug/L Xylenes, Total 0.50ND ug/L Surr: 1,2-Dichloroethane-d4 100 70 1301.0 Surr: Dibromofluoromethane 104 77 1261.0 Surr: p-Bromofluorobenzene 118 76 1271.0 Surr: Toluene-d8 114 79 1221.0 Lab ID: B14121909-001B_MS 12/24/14 14:43Sample Matrix Spike Run: SV5972.I_141224A Benzene 101 71 1331.05.04 ug/L Bromobenzene 107 78 1331.05.36 ug/L Bromochloromethane 115 68 1311.05.76 ug/L Bromodichloromethane 110 67 1381.05.48 ug/L Bromoform 131 64 1361.06.56 ug/L Bromomethane 104 60 1381.05.20 ug/L Carbon tetrachloride 94 61 1441.04.68 ug/L Chlorobenzene 100 78 1361.05.00 ug/L Chlorodibromomethane 117 72 1361.05.84 ug/L Chloroethane 88 64 1361.04.40 ug/L Chloroform 107 69 1331.05.36 ug/L Chloromethane 94 63 1491.04.72 ug/L 1,2-Dibromoethane 108 75 1311.05.40 ug/L 2-Chlorotoluene 100 74 1351.05.00 ug/L Dibromomethane 114 72 1331.05.72 ug/L 1,2-Dichlorobenzene 102 78 1291.05.08 ug/L 4-Chlorotoluene 102 79 1351.05.12 ug/L 1,3-Dichlorobenzene 100 79 1321.05.00 ug/L 1,4-Dichlorobenzene 100 78 1311.05.00 ug/L Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 8 of 16249 Project:Ebbighausen Client:Resource Technologies Inc Work Order:B14121909 QA/QC Summary Report 01/05/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits Qual Prepared by Billings, MT Branch Method: SW8260B Batch: R235880 Lab ID: B14121909-001B_MS 12/24/14 14:43Sample Matrix Spike Run: SV5972.I_141224A Dichlorodifluoromethane 81 55 1411.04.04 ug/L 1,1-Dichloroethane 114 72 1301.05.68 ug/L 1,2-Dichloroethane 101 57 1461.05.04 ug/L 1,1-Dichloroethene 103 66 1421.05.16 ug/L cis-1,2-Dichloroethene 106 74 1331.05.32 ug/L trans-1,2-Dichloroethene 94 76 1381.04.72 ug/L 1,2-Dichloropropane 102 72 1351.05.08 ug/L 1,3-Dichloropropane 101 75 1341.05.04 ug/L 2,2-Dichloropropane 113 42 1671.05.64 ug/L 1,1-Dichloropropene 103 72 1401.05.16 ug/L cis-1,3-Dichloropropene 106 75 1321.05.28 ug/L trans-1,3-Dichloropropene 118 77 1451.05.92 ug/L Ethylbenzene 108 78 1311.05.40 ug/L Methyl tert-butyl ether (MTBE)82 58 1511.04.12 ug/L Methyl ethyl ketone 98 55 1452048.8 ug/L Methylene chloride 91 73 1261.04.56 ug/L Styrene 109 76 1341.05.44 ug/L 1,1,1,2-Tetrachloroethane 107 75 1351.05.36 ug/L 1,1,2,2-Tetrachloroethane 106 72 1321.05.32 ug/L Tetrachloroethene 116 78 1371.05.80 ug/L Toluene 108 78 1341.05.56 ug/L 1,1,1-Trichloroethane 114 64 1411.05.68 ug/L 1,1,2-Trichloroethane 102 72 1331.05.12 ug/L Trichloroethene 104 75 1381.05.20 ug/L Trichlorofluoromethane 84 58 1391.04.20 ug/L 1,2,3-Trichloropropane 105 67 1331.05.24 ug/L Vinyl chloride 86 66 1401.04.32 ug/L m+p-Xylenes 106 78 1331.010.6 ug/L o-Xylene 105 79 1361.05.24 ug/L Xylenes, Total 106 78 1361.015.9 ug/L Surr: 1,2-Dichloroethane-d4 105 70 1301.0 Surr: Dibromofluoromethane 109 77 1261.0 Surr: p-Bromofluorobenzene 112 76 1271.0 Surr: Toluene-d8 115 79 1221.0 Lab ID: B14121909-001B_MSD 12/24/14 15:11Sample Matrix Spike Duplicate Run: SV5972.I_141224A Benzene 102 71 133 201.0 1.65.12 ug/L Bromobenzene 110 78 133 201.0 2.95.52 ug/L Bromochloromethane 115 68 131 201.0 0.05.76 ug/L Bromodichloromethane 110 67 138 201.0 0.75.52 ug/L Bromoform 134 64 136 201.0 1.86.68 ug/L Bromomethane 103 60 138 201.0 0.85.16 ug/L Carbon tetrachloride 93 61 144 201.0 0.94.64 ug/L Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 9 of 16250 Project:Ebbighausen Client:Resource Technologies Inc Work Order:B14121909 QA/QC Summary Report 01/05/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits Qual Prepared by Billings, MT Branch Method: SW8260B Batch: R235880 Lab ID: B14121909-001B_MSD 12/24/14 15:11Sample Matrix Spike Duplicate Run: SV5972.I_141224A Chlorobenzene 102 78 136 201.0 2.45.12 ug/L Chlorodibromomethane 117 72 136 201.0 0.05.84 ug/L Chloroethane 90 64 136 201.0 2.74.52 ug/L Chloroform 110 69 133 201.0 2.95.52 ug/L Chloromethane 91 63 149 201.0 3.44.56 ug/L 1,2-Dibromoethane 109 75 131 201.0 0.75.44 ug/L 2-Chlorotoluene 101 74 135 201.0 0.85.04 ug/L Dibromomethane 116 72 133 201.0 1.45.80 ug/L 1,2-Dichlorobenzene 106 78 129 201.0 4.65.32 ug/L 4-Chlorotoluene 107 79 135 201.0 4.65.36 ug/L 1,3-Dichlorobenzene 106 79 132 201.0 5.45.28 ug/L 1,4-Dichlorobenzene 106 78 131 201.0 5.45.28 ug/L Dichlorodifluoromethane 79 55 141 201.0 2.83.93 ug/L 1,1-Dichloroethane 114 72 130 201.0 0.75.72 ug/L 1,2-Dichloroethane 102 57 146 201.0 1.65.12 ug/L 1,1-Dichloroethene 104 66 142 201.0 0.85.20 ug/L cis-1,2-Dichloroethene 108 74 133 201.0 1.55.40 ug/L trans-1,2-Dichloroethene 97 76 138 201.0 2.54.84 ug/L 1,2-Dichloropropane 104 72 135 201.0 2.35.20 ug/L 1,3-Dichloropropane 102 75 134 201.0 1.65.12 ug/L 2,2-Dichloropropane 112 42 167 201.0 0.75.60 ug/L 1,1-Dichloropropene 104 72 140 201.0 0.85.20 ug/L cis-1,3-Dichloropropene 104 75 132 201.0 1.55.20 ug/L trans-1,3-Dichloropropene 114 77 145 201.0 4.15.68 ug/L Ethylbenzene 110 78 131 201.0 2.25.52 ug/L Methyl tert-butyl ether (MTBE)84 58 151 201.0 1.94.20 ug/L Methyl ethyl ketone 104 55 145 20206.352.0 ug/L Methylene chloride 92 73 126 201.0 0.94.60 ug/L Styrene 110 76 134 201.0 1.55.52 ug/L 1,1,1,2-Tetrachloroethane 109 75 135 201.0 1.55.44 ug/L 1,1,2,2-Tetrachloroethane 110 72 132 201.0 3.05.48 ug/L Tetrachloroethene 119 78 137 201.0 2.75.96 ug/L Toluene 111 78 134 201.0 2.15.68 ug/L 1,1,1-Trichloroethane 114 64 141 201.0 0.75.72 ug/L 1,1,2-Trichloroethane 102 72 133 201.0 0.05.12 ug/L Trichloroethene 106 75 138 201.0 1.55.28 ug/L Trichlorofluoromethane 82 58 139 201.0 2.94.08 ug/L 1,2,3-Trichloropropane 106 67 133 201.0 1.55.32 ug/L Vinyl chloride 84 66 140 201.0 2.84.20 ug/L m+p-Xylenes 108 78 133 201.0 1.510.8 ug/L o-Xylene 106 79 136 201.0 0.85.28 ug/L Xylenes, Total 107 78 1361.016.1 ug/L Surr: 1,2-Dichloroethane-d4 106 70 1301.0 Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 10 of 16251 Project:Ebbighausen Client:Resource Technologies Inc Work Order:B14121909 QA/QC Summary Report 01/05/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits Qual Prepared by Billings, MT Branch Method: SW8260B Batch: R235880 Lab ID: B14121909-001B_MSD 12/24/14 15:11Sample Matrix Spike Duplicate Run: SV5972.I_141224A Surr: Dibromofluoromethane 110 77 1261.0 Surr: p-Bromofluorobenzene 112 76 1271.0 Surr: Toluene-d8 115 79 1221.0 Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 11 of 16252 Project:Ebbighausen Client:Resource Technologies Inc Work Order:B14121909 QA/QC Summary Report 01/05/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits Qual Prepared by Billings, MT Branch Method: SW8015M Batch: 85897 Lab ID: LCS-85897 01/03/15 17:22Laboratory Control Sample Run: GCFID-HP3-B_150102B Total Extractable Hydrocarbons 106 60 1403006560 ug/L Surr: o-Terphenyl 96 40 140 Lab ID: MB-85897 01/03/15 18:06Method Blank Run: GCFID-HP3-B_150102B Total Extractable Hydrocarbons 300ND ug/L Surr: o-Terphenyl 94 40 140 Lab ID: B14121909-001AMS 01/03/15 19:33Sample Matrix Spike Run: GCFID-HP3-B_150102B Total Extractable Hydrocarbons 107 60 14060013300 ug/L Surr: o-Terphenyl 74 40 140 Lab ID: B14121909-001AMSD 01/03/15 20:16Sample Matrix Spike Duplicate Run: GCFID-HP3-B_150102B Total Extractable Hydrocarbons 110 60 140 206002.513600 ug/L Surr: o-Terphenyl 74 40 140 Method: SW8015M Analytical Run: R236224 Lab ID: CCV_0102HP333r-W 01/03/15 15:55Continuing Calibration Verification Standard n-Nonane 104 75 125208 ug/L n-Decane 104 75 125208 ug/L n-Dodecane 107 75 125214 ug/L n-Tetradecane 105 75 125210 ug/L n-Hexadecane 107 75 125214 ug/L n-Octadecane 107 75 125215 ug/L n-Nonadecane 108 75 125215 ug/L n-Eicosane 108 75 125215 ug/L n-Docosane 108 75 125215 ug/L n-Tetracosane 108 75 125216 ug/L n-Hexacosane 108 75 125216 ug/L n-Octacosane 108 75 125216 ug/L n-Triacontane 109 75 125217 ug/L n-Hexatriacontane 108 75 125216 ug/L Surr: o-Terphenyl 109 75 125 Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 12 of 16253 MW-1 Batch ID: 85897 EXTRACTABLE PETROLEUM HYDROCARBONS (EPH) SCREENING ANALYSIS CHROMATOGRAM Sample Name: B14121909-001A ;0102HP3 , $HC-EPH-SCRN-W, RR-V37 Raw File: G:\org\HP3\DAT\HP3010215_b\0102HP3.0037.RAW Date & Time Acquired: 1/3/2015 6:49:40 PM Method File: g:\org\HP3\Methods\SR_SCN-LI-L%.met Calibration File: G:\Org\HP3\Cals\SC140226LI.CAL Sample Weight: 0.97 Dilution: 2 S.A.: 1 Mean RF for C9 to C18 Hydrocarbons: 30979.57 Mean RF for C19 to C36 Hydrocarbons: 30994.75 Mean RF for Total Extractable Hydrocarbons: 30987.16 Rt range for Diesel Range Organics: 6.313 to 16.684 Rt range for C9 to C18 Hydrocarbons: 5.273 to 12.239 Rt range for C19 to C36 Hydrocarbons: 12.274 to 19.076 SURROGATE COMPOUND RT ACTUAL MEASURED %REC *o-Terphenyl_____________12.282 206.186 104.002 50.44 - *1-Chloro-octadecane_____13.12 206.186 75.556 36.64 - DRO Area:942938.4 DRO Amount: 62.74221 TEH Area:1152155 TEH Amount: 76.66328 C9-C18 Area:750547.9 C9-C18 Amount: 49.95296 C19-C36 Area:346567.7 C19-C36 Amount: 23.05463 4.36 4.64 5.06 5.15 5.29 5.37 5.47 5.56 5.68 5.78 5.89 5.99 6.10 6.30 6.39 6.52 6.60 7.20 7.45 7.64 7.70 7.92 8.00 8.09 8.15 8.21 8.28 8.34 8.41 8.46 8.85 8.93 9.18 9.31 9.42 9.53 9.66 9.83 9.90 9.95 10.03 10.13 10.24 10.32 10.41 10.59 10.65 10.93 11.00 11.08 11.19 11.31 11.34 11.45 11.52 11.67 11.71 11.76 11.89 12.02 12.10 12.15 12.21 12.28 12.38 12.51 12.70 12.77 12.89 12.99 13.12 13.35 13.44 13.61 13.77 13.88 13.96 14.03 14.21 14.34 14.39 14.44 14.55 14.63 14.83 14.94 15.00 15.06 15.22 15.37 15.50 15.59 15.81 15.85 15.92 16.07 16.28 16.36 16.46 16.60 16.77 16.94 17.03 17.18 17.24 17.42 17.59 17.65 17.74 17.91 17.96 18.10 18.33 18.42 18.53 18.68 18.90 19.03 19.53 19.89 20.25 20.76 21.68 22.05 22.26 23.25 27.00 n-Nonane n-Decane n-Dodecane n-Tetradecane n-Hexadecane n-Octadecane n-Nonadecane *o-Terphenyl n-Eicosane *1-Chloro-octadecane n-Docosane n-Tetracosane n-Hexacosane n-Octacosane n-Triacontane n-Hexatriacontane G:\org\HP3\DAT\HP3010215_b\0102HP3.0037.RAW B14121909-001A ;0102HP3 , $HC-EPH-SCRN-W, RR-V37 0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 0 500 1000 1500 2000 2500 3000 Page 13 of 16254 MW-2 Batch ID: 85897 EXTRACTABLE PETROLEUM HYDROCARBONS (EPH) SCREENING ANALYSIS CHROMATOGRAM Sample Name: B14121909-002A ;0102HP3 , $HC-EPH-SCRN-W, V41 Raw File: G:\org\HP3\DAT\HP3010215_b\0102HP3.0041.RAW Date & Time Acquired: 1/3/2015 9:43:42 PM Method File: g:\org\HP3\Methods\SR_SCN-LI-L%.met Calibration File: G:\Org\HP3\Cals\SC140226LI.CAL Sample Weight: 0.95 Dilution: 2 S.A.: 1 Mean RF for C9 to C18 Hydrocarbons: 30979.57 Mean RF for C19 to C36 Hydrocarbons: 30994.75 Mean RF for Total Extractable Hydrocarbons: 30987.16 Rt range for Diesel Range Organics: 6.313 to 16.684 Rt range for C9 to C18 Hydrocarbons: 5.273 to 12.239 Rt range for C19 to C36 Hydrocarbons: 12.274 to 19.076 SURROGATE COMPOUND RT ACTUAL MEASURED %REC *o-Terphenyl_____________12.281 210.526 110.504 52.49 - *1-Chloro-octadecane_____13.119 210.526 87.071 41.36 - DRO Area:930191.3 DRO Amount: 63.19706 TEH Area:1189115 TEH Amount: 80.78831 C9-C18 Area:676762.7 C9-C18 Amount: 45.99042 C19-C36 Area:401008 C19-C36 Amount: 27.23776 4.50 4.57 4.64 5.00 5.14 5.28 5.34 5.37 5.48 5.56 5.69 5.79 5.90 6.00 6.10 6.40 6.54 6.60 7.48 7.66 7.71 8.06 8.21 8.46 8.86 9.18 9.27 9.31 9.42 9.53 9.67 9.82 9.91 9.95 10.05 10.13 10.42 10.65 10.93 11.05 11.10 11.21 11.28 11.31 11.34 11.43 11.52 11.71 11.76 11.87 11.94 12.03 12.10 12.15 12.22 12.28 12.42 12.51 12.70 12.77 12.81 12.89 12.99 13.05 13.12 13.35 13.44 13.61 13.78 13.88 13.95 14.03 14.23 14.33 14.40 14.44 14.55 14.62 14.73 14.84 14.94 15.00 15.06 15.22 15.35 15.50 15.58 15.79 15.91 16.07 16.29 16.46 16.60 16.94 17.10 17.17 17.24 17.42 17.59 17.65 17.78 17.96 18.10 18.42 18.68 18.92 19.03 19.52 19.90 20.23 21.58 22.05 23.24 23.93 27.00 28.34 n-Nonane n-Decane n-Dodecane n-Tetradecane n-Hexadecane n-Octadecane n-Nonadecane *o-Terphenyl n-Eicosane *1-Chloro-octadecane n-Docosane n-Tetracosane n-Hexacosane n-Octacosane n-Triacontane n-Hexatriacontane G:\org\HP3\DAT\HP3010215_b\0102HP3.0041.RAW B14121909-002A ;0102HP3 , $HC-EPH-SCRN-W, V41 0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 0 500 1000 1500 2000 2500 3000 Page 14 of 16255 Shipping container/cooler in good condition? Custody seals intact on all shipping container(s)/cooler(s)? Custody seals intact on all sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res Cl, Sulfite, Ferrous Iron, etc.) Container/Temp Blank temperature: Water - VOA vials have zero headspace? Water - pH acceptable upon receipt? Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes No No No No No No No No No No No No Not Present Not Present Not Present No VOA vials submitted Not Applicable 2.7°C On Ice 12/23/2014Randa Nees Hand Del lg Date Received: Received by: Login completed by: Carrier name: BL2000\lcadreau 12/23/2014 Reviewed by: Reviewed Date: Contact and Corrective Action Comments: None Temp Blank received in all shipping container(s)/cooler(s)? Yes No Not Applicable Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as –dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Standard Reporting Procedures: Workorder Receipt Checklist Resource Technologies Inc B14121909 Page 15 of 16256 Page 16 of 16257 ANALYTICAL SUMMARY REPORTANALYTICAL SUMMARY REPORTANALYTICAL SUMMARY REPORTANALYTICAL SUMMARY REPORT The analyses presented in this report were performed by Energy Laboratories, Inc., 1120 S 27th St., Billings, MT 59101, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Lab ID Client Sample ID Collect Date Receive Date Matrix Test Report Approved By: B15011740-001 MW-1 01/27/15 15:25 01/28/15 Aqueous 8260-Volatile Organic Compounds- Short List B15011740-002 MW-2 01/27/15 15:10 01/28/15 Aqueous Same As Above B15011740-003 Trip Blank Lot#112514 4526 01/27/15 15:10 01/28/15 Trip Blank Same As Above Resource Technologies Inc Project Name:Ebbinghausen Work Order:B15011740 1050 E Main St Ste 4 Bozeman, MT 59715 February 05, 2015 Energy Laboratories Inc Billings MT received the following 3 samples for Resource Technologies Inc on 1/28/2015 for analysis. Page 1 of 15258 LABORATORY ANALYTICAL REPORT Client:Resource Technologies Inc Project:Ebbinghausen Lab ID:B15011740-001 Client Sample ID:MW-1 Collection Date:01/27/15 15:25 Matrix:Aqueous Report Date:02/05/15 DateReceived:01/28/15 Prepared by Billings, MT Branch Analyses Result Units Analysis Date / ByRLMethod MCL/ QCLQualifiers VOLATILE ORGANIC COMPOUNDS 02/02/15 22:39 / nl1.0ug/LNDBenzene SW8260B 02/02/15 22:39 / nl1.0ug/LNDBromobenzene SW8260B 02/02/15 22:39 / nl1.0ug/LNDBromochloromethane SW8260B 02/02/15 22:39 / nl1.0ug/LNDBromodichloromethane SW8260B 02/02/15 22:39 / nl1.0ug/LNDBromoform SW8260B 02/02/15 22:39 / nl1.0ug/LNDBromomethane SW8260B 02/02/15 22:39 / nl1.0ug/LNDCarbon tetrachloride SW8260B 02/02/15 22:39 / nl1.0ug/LNDChlorobenzene SW8260B 02/02/15 22:39 / nl1.0ug/LNDChlorodibromomethane SW8260B 02/02/15 22:39 / nl1.0ug/LNDChloroethane SW8260B 02/02/15 22:39 / nl1.0ug/LNDChloroform SW8260B 02/02/15 22:39 / nl1.0ug/LNDChloromethane SW8260B 02/02/15 22:39 / nl1.0ug/LND1,2-Dibromoethane SW8260B 02/02/15 22:39 / nl1.0ug/LND2-Chlorotoluene SW8260B 02/02/15 22:39 / nl1.0ug/LND4-Chlorotoluene SW8260B 02/02/15 22:39 / nl1.0ug/LNDDibromomethane SW8260B 02/02/15 22:39 / nl1.0ug/LND1,2-Dichlorobenzene SW8260B 02/02/15 22:39 / nl1.0ug/LND1,3-Dichlorobenzene SW8260B 02/02/15 22:39 / nl1.0ug/LND1,4-Dichlorobenzene SW8260B 02/02/15 22:39 / nl1.0ug/LNDDichlorodifluoromethane SW8260B 02/02/15 22:39 / nl1.0ug/LND1,1-Dichloroethane SW8260B 02/02/15 22:39 / nl1.0ug/LND1,2-Dichloroethane SW8260B 02/02/15 22:39 / nl1.0ug/LND1,1-Dichloroethene SW8260B 02/02/15 22:39 / nl1.0ug/LNDcis-1,2-Dichloroethene SW8260B 02/02/15 22:39 / nl1.0ug/LNDtrans-1,2-Dichloroethene SW8260B 02/02/15 22:39 / nl1.0ug/LND1,2-Dichloropropane SW8260B 02/02/15 22:39 / nl1.0ug/LND1,3-Dichloropropane SW8260B 02/02/15 22:39 / nl1.0ug/LND2,2-Dichloropropane SW8260B 02/02/15 22:39 / nl1.0ug/LND1,1-Dichloropropene SW8260B 02/02/15 22:39 / nl1.0ug/LNDcis-1,3-Dichloropropene SW8260B 02/02/15 22:39 / nl1.0ug/LNDtrans-1,3-Dichloropropene SW8260B 02/02/15 22:39 / nl1.0ug/LNDEthylbenzene SW8260B 02/02/15 22:39 / nl20ug/LNDMethyl ethyl ketone SW8260B 02/02/15 22:39 / nl1.0ug/LNDMethyl tert-butyl ether (MTBE)SW8260B 02/02/15 22:39 / nl1.0ug/LNDMethylene chloride SW8260B 02/02/15 22:39 / nl1.0ug/LNDStyrene SW8260B 02/02/15 22:39 / nl1.0ug/LND1,1,1,2-Tetrachloroethane SW8260B 02/02/15 22:39 / nl1.0ug/LND1,1,2,2-Tetrachloroethane SW8260B 02/02/15 22:39 / nl1.0ug/LNDTetrachloroethene SW8260B 02/02/15 22:39 / nl1.0ug/LNDToluene SW8260B 02/02/15 22:39 / nl1.0ug/LND1,1,1-Trichloroethane SW8260B 02/02/15 22:39 / nl1.0ug/LND1,1,2-Trichloroethane SW8260B Report Definitions: RL - Analyte reporting limit.MCL - Maximum contaminant level. QCL - Quality control limit.ND - Not detected at the reporting limit. Page 2 of 15259 LABORATORY ANALYTICAL REPORT Client:Resource Technologies Inc Project:Ebbinghausen Lab ID:B15011740-001 Client Sample ID:MW-1 Collection Date:01/27/15 15:25 Matrix:Aqueous Report Date:02/05/15 DateReceived:01/28/15 Prepared by Billings, MT Branch Analyses Result Units Analysis Date / ByRLMethod MCL/ QCLQualifiers VOLATILE ORGANIC COMPOUNDS 02/02/15 22:39 / nl1.0ug/LNDTrichloroethene SW8260B 02/02/15 22:39 / nl1.0ug/LNDTrichlorofluoromethane SW8260B 02/02/15 22:39 / nl1.0ug/LND1,2,3-Trichloropropane SW8260B 02/02/15 22:39 / nl0.50ug/LNDVinyl chloride SW8260B 02/02/15 22:39 / nl1.0ug/LNDm+p-Xylenes SW8260B 02/02/15 22:39 / nl1.0ug/LNDo-Xylene SW8260B 02/02/15 22:39 / nl1.0ug/LNDXylenes, Total SW8260B 02/02/15 22:39 / nl77-126%REC109 Surr: Dibromofluoromethane SW8260B 02/02/15 22:39 / nl70-130%REC107 Surr: 1,2-Dichloroethane-d4 SW8260B 02/02/15 22:39 / nl79-122%REC100 Surr: Toluene-d8 SW8260B 02/02/15 22:39 / nl76-127%REC100 Surr: p-Bromofluorobenzene SW8260B Report Definitions: RL - Analyte reporting limit.MCL - Maximum contaminant level. QCL - Quality control limit.ND - Not detected at the reporting limit. Page 3 of 15260 LABORATORY ANALYTICAL REPORT Client:Resource Technologies Inc Project:Ebbinghausen Lab ID:B15011740-002 Client Sample ID:MW-2 Collection Date:01/27/15 15:10 Matrix:Aqueous Report Date:02/05/15 DateReceived:01/28/15 Prepared by Billings, MT Branch Analyses Result Units Analysis Date / ByRLMethod MCL/ QCLQualifiers VOLATILE ORGANIC COMPOUNDS 02/02/15 22:11 / nl1.0ug/LNDBenzene SW8260B 02/02/15 22:11 / nl1.0ug/LNDBromobenzene SW8260B 02/02/15 22:11 / nl1.0ug/LNDBromochloromethane SW8260B 02/02/15 22:11 / nl1.0ug/LNDBromodichloromethane SW8260B 02/02/15 22:11 / nl1.0ug/LNDBromoform SW8260B 02/02/15 22:11 / nl1.0ug/LNDBromomethane SW8260B 02/02/15 22:11 / nl1.0ug/LNDCarbon tetrachloride SW8260B 02/02/15 22:11 / nl1.0ug/LNDChlorobenzene SW8260B 02/02/15 22:11 / nl1.0ug/LNDChlorodibromomethane SW8260B J 02/02/15 22:11 / nl1.0ug/L0.13Chloroethane SW8260B 02/02/15 22:11 / nl1.0ug/LNDChloroform SW8260B 02/02/15 22:11 / nl1.0ug/LNDChloromethane SW8260B 02/02/15 22:11 / nl1.0ug/LND1,2-Dibromoethane SW8260B 02/02/15 22:11 / nl1.0ug/LND2-Chlorotoluene SW8260B 02/02/15 22:11 / nl1.0ug/LND4-Chlorotoluene SW8260B 02/02/15 22:11 / nl1.0ug/LNDDibromomethane SW8260B 02/02/15 22:11 / nl1.0ug/LND1,2-Dichlorobenzene SW8260B 02/02/15 22:11 / nl1.0ug/LND1,3-Dichlorobenzene SW8260B 02/02/15 22:11 / nl1.0ug/LND1,4-Dichlorobenzene SW8260B 02/02/15 22:11 / nl1.0ug/LNDDichlorodifluoromethane SW8260B 02/02/15 22:11 / nl1.0ug/LND1,1-Dichloroethane SW8260B 02/02/15 22:11 / nl1.0ug/LND1,2-Dichloroethane SW8260B 02/02/15 22:11 / nl1.0ug/LND1,1-Dichloroethene SW8260B 02/02/15 22:11 / nl1.0ug/LNDcis-1,2-Dichloroethene SW8260B 02/02/15 22:11 / nl1.0ug/LNDtrans-1,2-Dichloroethene SW8260B 02/02/15 22:11 / nl1.0ug/LND1,2-Dichloropropane SW8260B 02/02/15 22:11 / nl1.0ug/LND1,3-Dichloropropane SW8260B 02/02/15 22:11 / nl1.0ug/LND2,2-Dichloropropane SW8260B 02/02/15 22:11 / nl1.0ug/LND1,1-Dichloropropene SW8260B 02/02/15 22:11 / nl1.0ug/LNDcis-1,3-Dichloropropene SW8260B 02/02/15 22:11 / nl1.0ug/LNDtrans-1,3-Dichloropropene SW8260B 02/02/15 22:11 / nl1.0ug/LNDEthylbenzene SW8260B 02/02/15 22:11 / nl20ug/LNDMethyl ethyl ketone SW8260B 02/02/15 22:11 / nl1.0ug/LNDMethyl tert-butyl ether (MTBE)SW8260B 02/02/15 22:11 / nl1.0ug/LNDMethylene chloride SW8260B 02/02/15 22:11 / nl1.0ug/LNDStyrene SW8260B 02/02/15 22:11 / nl1.0ug/LND1,1,1,2-Tetrachloroethane SW8260B 02/02/15 22:11 / nl1.0ug/LND1,1,2,2-Tetrachloroethane SW8260B 02/02/15 22:11 / nl1.0ug/LNDTetrachloroethene SW8260B 02/02/15 22:11 / nl1.0ug/LNDToluene SW8260B 02/02/15 22:11 / nl1.0ug/LND1,1,1-Trichloroethane SW8260B 02/02/15 22:11 / nl1.0ug/LND1,1,2-Trichloroethane SW8260B Report Definitions: RL - Analyte reporting limit.MCL - Maximum contaminant level. QCL - Quality control limit.ND - Not detected at the reporting limit. J - Estimated value. The analyte was present but less than the reporting limit. Page 4 of 15261 LABORATORY ANALYTICAL REPORT Client:Resource Technologies Inc Project:Ebbinghausen Lab ID:B15011740-002 Client Sample ID:MW-2 Collection Date:01/27/15 15:10 Matrix:Aqueous Report Date:02/05/15 DateReceived:01/28/15 Prepared by Billings, MT Branch Analyses Result Units Analysis Date / ByRLMethod MCL/ QCLQualifiers VOLATILE ORGANIC COMPOUNDS 02/02/15 22:11 / nl1.0ug/LNDTrichloroethene SW8260B 02/02/15 22:11 / nl1.0ug/LNDTrichlorofluoromethane SW8260B 02/02/15 22:11 / nl1.0ug/LND1,2,3-Trichloropropane SW8260B 02/02/15 22:11 / nl0.50ug/L0.58Vinyl chloride SW8260B 02/02/15 22:11 / nl1.0ug/LNDm+p-Xylenes SW8260B 02/02/15 22:11 / nl1.0ug/LNDo-Xylene SW8260B 02/02/15 22:11 / nl1.0ug/LNDXylenes, Total SW8260B 02/02/15 22:11 / nl77-126%REC108 Surr: Dibromofluoromethane SW8260B 02/02/15 22:11 / nl70-130%REC105 Surr: 1,2-Dichloroethane-d4 SW8260B 02/02/15 22:11 / nl79-122%REC100 Surr: Toluene-d8 SW8260B 02/02/15 22:11 / nl76-127%REC104 Surr: p-Bromofluorobenzene SW8260B Report Definitions: RL - Analyte reporting limit.MCL - Maximum contaminant level. QCL - Quality control limit.ND - Not detected at the reporting limit. Page 5 of 15262 LABORATORY ANALYTICAL REPORT Client:Resource Technologies Inc Project:Ebbinghausen Lab ID:B15011740-003 Client Sample ID:Trip Blank Lot#112514 4526 Collection Date:01/27/15 15:10 Matrix:Trip Blank Report Date:02/05/15 DateReceived:01/28/15 Prepared by Billings, MT Branch Analyses Result Units Analysis Date / ByRLMethod MCL/ QCLQualifiers VOLATILE ORGANIC COMPOUNDS 02/02/15 21:42 / nl1.0ug/LNDBenzene SW8260B 02/02/15 21:42 / nl1.0ug/LNDBromobenzene SW8260B 02/02/15 21:42 / nl1.0ug/LNDBromochloromethane SW8260B 02/02/15 21:42 / nl1.0ug/LNDBromodichloromethane SW8260B 02/02/15 21:42 / nl1.0ug/LNDBromoform SW8260B 02/02/15 21:42 / nl1.0ug/LNDBromomethane SW8260B 02/02/15 21:42 / nl1.0ug/LNDCarbon tetrachloride SW8260B 02/02/15 21:42 / nl1.0ug/LNDChlorobenzene SW8260B 02/02/15 21:42 / nl1.0ug/LNDChlorodibromomethane SW8260B 02/02/15 21:42 / nl1.0ug/LNDChloroethane SW8260B 02/02/15 21:42 / nl1.0ug/LNDChloroform SW8260B 02/02/15 21:42 / nl1.0ug/LNDChloromethane SW8260B 02/02/15 21:42 / nl1.0ug/LND1,2-Dibromoethane SW8260B 02/02/15 21:42 / nl1.0ug/LND2-Chlorotoluene SW8260B 02/02/15 21:42 / nl1.0ug/LND4-Chlorotoluene SW8260B 02/02/15 21:42 / nl1.0ug/LNDDibromomethane SW8260B 02/02/15 21:42 / nl1.0ug/LND1,2-Dichlorobenzene SW8260B 02/02/15 21:42 / nl1.0ug/LND1,3-Dichlorobenzene SW8260B 02/02/15 21:42 / nl1.0ug/LND1,4-Dichlorobenzene SW8260B 02/02/15 21:42 / nl1.0ug/LNDDichlorodifluoromethane SW8260B 02/02/15 21:42 / nl1.0ug/LND1,1-Dichloroethane SW8260B 02/02/15 21:42 / nl1.0ug/LND1,2-Dichloroethane SW8260B 02/02/15 21:42 / nl1.0ug/LND1,1-Dichloroethene SW8260B 02/02/15 21:42 / nl1.0ug/LNDcis-1,2-Dichloroethene SW8260B 02/02/15 21:42 / nl1.0ug/LNDtrans-1,2-Dichloroethene SW8260B 02/02/15 21:42 / nl1.0ug/LND1,2-Dichloropropane SW8260B 02/02/15 21:42 / nl1.0ug/LND1,3-Dichloropropane SW8260B 02/02/15 21:42 / nl1.0ug/LND2,2-Dichloropropane SW8260B 02/02/15 21:42 / nl1.0ug/LND1,1-Dichloropropene SW8260B 02/02/15 21:42 / nl1.0ug/LNDcis-1,3-Dichloropropene SW8260B 02/02/15 21:42 / nl1.0ug/LNDtrans-1,3-Dichloropropene SW8260B 02/02/15 21:42 / nl1.0ug/LNDEthylbenzene SW8260B 02/02/15 21:42 / nl20ug/LNDMethyl ethyl ketone SW8260B 02/02/15 21:42 / nl1.0ug/LNDMethyl tert-butyl ether (MTBE)SW8260B 02/02/15 21:42 / nl1.0ug/LNDMethylene chloride SW8260B 02/02/15 21:42 / nl1.0ug/LNDStyrene SW8260B 02/02/15 21:42 / nl1.0ug/LND1,1,1,2-Tetrachloroethane SW8260B 02/02/15 21:42 / nl1.0ug/LND1,1,2,2-Tetrachloroethane SW8260B 02/02/15 21:42 / nl1.0ug/LNDTetrachloroethene SW8260B 02/02/15 21:42 / nl1.0ug/LNDToluene SW8260B 02/02/15 21:42 / nl1.0ug/LND1,1,1-Trichloroethane SW8260B 02/02/15 21:42 / nl1.0ug/LND1,1,2-Trichloroethane SW8260B Report Definitions: RL - Analyte reporting limit.MCL - Maximum contaminant level. QCL - Quality control limit.ND - Not detected at the reporting limit. Page 6 of 15263 LABORATORY ANALYTICAL REPORT Client:Resource Technologies Inc Project:Ebbinghausen Lab ID:B15011740-003 Client Sample ID:Trip Blank Lot#112514 4526 Collection Date:01/27/15 15:10 Matrix:Trip Blank Report Date:02/05/15 DateReceived:01/28/15 Prepared by Billings, MT Branch Analyses Result Units Analysis Date / ByRLMethod MCL/ QCLQualifiers VOLATILE ORGANIC COMPOUNDS 02/02/15 21:42 / nl1.0ug/LNDTrichloroethene SW8260B 02/02/15 21:42 / nl1.0ug/LNDTrichlorofluoromethane SW8260B 02/02/15 21:42 / nl1.0ug/LND1,2,3-Trichloropropane SW8260B 02/02/15 21:42 / nl1.0ug/LNDVinyl chloride SW8260B 02/02/15 21:42 / nl1.0ug/LNDm+p-Xylenes SW8260B 02/02/15 21:42 / nl1.0ug/LNDo-Xylene SW8260B 02/02/15 21:42 / nl1.0ug/LNDXylenes, Total SW8260B 02/02/15 21:42 / nl77-126%REC101 Surr: Dibromofluoromethane SW8260B 02/02/15 21:42 / nl70-130%REC105 Surr: 1,2-Dichloroethane-d4 SW8260B 02/02/15 21:42 / nl79-122%REC95.0 Surr: Toluene-d8 SW8260B 02/02/15 21:42 / nl76-127%REC103 Surr: p-Bromofluorobenzene SW8260B Report Definitions: RL - Analyte reporting limit.MCL - Maximum contaminant level. QCL - Quality control limit.ND - Not detected at the reporting limit. Page 7 of 15264 Project:Ebbinghausen Client:Resource Technologies Inc Work Order:B15011740 QA/QC Summary Report 02/05/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits Qual Prepared by Billings, MT Branch Method:SW8260B Batch: R237677 Lab ID:LCS_020215 02/02/15 19:10Laboratory Control Sample Run: SV5972.I_150202A Benzene 97 71 1331.04.84 ug/L Bromobenzene 105 78 1331.05.24 ug/L Bromochloromethane 109 68 1311.05.44 ug/L Bromodichloromethane 110 67 1381.05.52 ug/L Bromoform 117 64 1361.05.84 ug/L Bromomethane 122 60 1381.06.08 ug/L Carbon tetrachloride 106 61 1441.05.28 ug/L Chlorobenzene 102 78 1361.05.08 ug/L Chlorodibromomethane 117 72 1361.05.84 ug/L Chloroethane 112 64 1361.05.60 ug/L Chloroform 100 69 1331.05.00 ug/L Chloromethane 83 63 1491.04.16 ug/L 1,2-Dibromoethane 110 75 1311.05.52 ug/L 2-Chlorotoluene 101 74 1351.05.04 ug/L Dibromomethane 107 72 1331.05.36 ug/L 1,2-Dichlorobenzene 103 78 1291.05.16 ug/L 4-Chlorotoluene 101 79 1351.05.04 ug/L 1,3-Dichlorobenzene 106 79 1321.05.28 ug/L 1,4-Dichlorobenzene 101 78 1311.05.04 ug/L Dichlorodifluoromethane 96 55 1411.04.80 ug/L 1,1-Dichloroethane 102 72 1301.05.12 ug/L 1,2-Dichloroethane 109 57 1461.05.44 ug/L 1,1-Dichloroethene 117 66 1421.05.84 ug/L cis-1,2-Dichloroethene 104 74 1331.05.20 ug/L trans-1,2-Dichloroethene 112 76 1381.05.60 ug/L 1,2-Dichloropropane 98 72 1351.04.88 ug/L 1,3-Dichloropropane 101 75 1341.05.04 ug/L 2,2-Dichloropropane 87 42 1671.04.36 ug/L 1,1-Dichloropropene 102 72 1401.05.08 ug/L cis-1,3-Dichloropropene 107 75 1321.05.36 ug/L trans-1,3-Dichloropropene 117 77 1451.05.84 ug/L Ethylbenzene 99 78 1311.04.96 ug/L Methyl tert-butyl ether (MTBE)114 58 1511.05.68 ug/L Methyl ethyl ketone 103 55 1452051.6 ug/L Methylene chloride 113 73 1261.05.64 ug/L Styrene 106 76 1341.05.32 ug/L 1,1,1,2-Tetrachloroethane 113 75 1351.05.64 ug/L 1,1,2,2-Tetrachloroethane 102 72 1321.05.12 ug/L Tetrachloroethene 102 78 1371.05.12 ug/L Toluene 101 78 1341.05.04 ug/L 1,1,1-Trichloroethane 107 64 1411.05.36 ug/L 1,1,2-Trichloroethane 103 72 1331.05.16 ug/L Trichloroethene 102 75 1381.05.08 ug/L Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 8 of 15265 Project:Ebbinghausen Client:Resource Technologies Inc Work Order:B15011740 QA/QC Summary Report 02/05/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits Qual Prepared by Billings, MT Branch Method:SW8260B Batch: R237677 Lab ID:LCS_020215 02/02/15 19:10Laboratory Control Sample Run: SV5972.I_150202A Trichlorofluoromethane 114 58 1391.05.72 ug/L 1,2,3-Trichloropropane 108 67 1331.05.40 ug/L Vinyl chloride 85 66 1401.04.24 ug/L m+p-Xylenes 100 78 1331.09.96 ug/L o-Xylene 101 79 1361.05.04 ug/L Xylenes, Total 100 78 1361.015.0 ug/L Surr: 1,2-Dichloroethane-d4 103 70 1301.0 Surr: Dibromofluoromethane 105 77 1261.0 Surr: p-Bromofluorobenzene 100 76 1271.0 Surr: Toluene-d8 103 79 1221.0 Lab ID:BLK_020215 02/02/15 20:06Method Blank Run: SV5972.I_150202A Benzene 0.50ND ug/L Bromobenzene 0.50ND ug/L Bromochloromethane 0.50ND ug/L Bromodichloromethane 0.50ND ug/L Bromoform 0.50ND ug/L Bromomethane 0.50ND ug/L Carbon tetrachloride 0.50ND ug/L Chlorobenzene 0.50ND ug/L Chlorodibromomethane 0.50ND ug/L Chloroethane 0.50ND ug/L Chloroform 0.50ND ug/L Chloromethane 0.50ND ug/L 1,2-Dibromoethane 0.50ND ug/L 2-Chlorotoluene 0.50ND ug/L Dibromomethane 0.50ND ug/L 1,2-Dichlorobenzene 0.50ND ug/L 4-Chlorotoluene 0.50ND ug/L 1,3-Dichlorobenzene 0.50ND ug/L 1,4-Dichlorobenzene 0.50ND ug/L Dichlorodifluoromethane 0.50ND ug/L 1,1-Dichloroethane 0.50ND ug/L 1,2-Dichloroethane 0.50ND ug/L 1,1-Dichloroethene 0.50ND ug/L cis-1,2-Dichloroethene 0.50ND ug/L trans-1,2-Dichloroethene 0.50ND ug/L 1,2-Dichloropropane 0.50ND ug/L 1,3-Dichloropropane 0.50ND ug/L 2,2-Dichloropropane 0.50ND ug/L 1,1-Dichloropropene 0.50ND ug/L cis-1,3-Dichloropropene 0.50ND ug/L trans-1,3-Dichloropropene 0.50ND ug/L Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 9 of 15266 Project:Ebbinghausen Client:Resource Technologies Inc Work Order:B15011740 QA/QC Summary Report 02/05/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits Qual Prepared by Billings, MT Branch Method:SW8260B Batch: R237677 Lab ID:BLK_020215 02/02/15 20:06Method Blank Run: SV5972.I_150202A Ethylbenzene 0.50ND ug/L Methyl tert-butyl ether (MTBE)0.50ND ug/L Methyl ethyl ketone 10ND ug/L Methylene chloride 0.50ND ug/L Styrene 0.50ND ug/L 1,1,1,2-Tetrachloroethane 0.50ND ug/L 1,1,2,2-Tetrachloroethane 0.50ND ug/L Tetrachloroethene 0.50ND ug/L Toluene 0.50ND ug/L 1,1,1-Trichloroethane 0.50ND ug/L 1,1,2-Trichloroethane 0.50ND ug/L Trichloroethene 0.50ND ug/L Trichlorofluoromethane 0.50ND ug/L 1,2,3-Trichloropropane 0.50ND ug/L Vinyl chloride 0.50ND ug/L m+p-Xylenes 0.50ND ug/L o-Xylene 0.50ND ug/L Xylenes, Total 0.50ND ug/L Surr: 1,2-Dichloroethane-d4 102 70 1301.0 Surr: Dibromofluoromethane 103 77 1261.0 Surr: p-Bromofluorobenzene 100 76 1271.0 Surr: Toluene-d8 99 79 1221.0 Lab ID:B15011802-001A_MS 02/03/15 01:56Sample Matrix Spike Run: SV5972.I_150202A Benzene 106 71 1331.05.28 ug/L Bromobenzene 108 78 1331.05.40 ug/L Bromochloromethane 117 68 1311.05.84 ug/L Bromodichloromethane 122 67 1381.06.12 ug/L Bromoform 123 64 1361.06.16 ug/L Bromomethane 64 60 1381.03.18 ug/L Carbon tetrachloride 127 61 1441.06.36 ug/L Chlorobenzene 107 78 1361.05.36 ug/L Chlorodibromomethane 122 72 1361.06.08 ug/L Chloroethane 111 64 1361.05.56 ug/L Chloroform 112 69 1331.05.60 ug/L Chloromethane 82 63 1491.04.08 ug/L 1,2-Dibromoethane 113 75 1311.05.64 ug/L 2-Chlorotoluene 104 74 1351.05.20 ug/L Dibromomethane 115 72 1331.05.76 ug/L 1,2-Dichlorobenzene 106 78 1291.05.28 ug/L 4-Chlorotoluene 108 79 1351.05.40 ug/L 1,3-Dichlorobenzene 106 79 1321.05.28 ug/L 1,4-Dichlorobenzene 104 78 1311.05.20 ug/L Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 10 of 15267 Project:Ebbinghausen Client:Resource Technologies Inc Work Order:B15011740 QA/QC Summary Report 02/05/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits Qual Prepared by Billings, MT Branch Method:SW8260B Batch: R237677 Lab ID:B15011802-001A_MS 02/03/15 01:56Sample Matrix Spike Run: SV5972.I_150202A Dichlorodifluoromethane 98 55 1411.04.88 ug/L 1,1-Dichloroethane 111 72 1301.05.56 ug/L 1,2-Dichloroethane 125 57 1461.06.24 ug/L 1,1-Dichloroethene 126 66 1421.06.28 ug/L cis-1,2-Dichloroethene 111 74 1331.05.56 ug/L trans-1,2-Dichloroethene 125 76 1381.06.24 ug/L 1,2-Dichloropropane 106 72 1351.05.28 ug/L 1,3-Dichloropropane 107 75 1341.05.36 ug/L 2,2-Dichloropropane 115 42 1671.05.76 ug/L 1,1-Dichloropropene 112 72 1401.05.60 ug/L cis-1,3-Dichloropropene 114 75 1321.05.68 ug/L trans-1,3-Dichloropropene 122 77 1451.06.08 ug/L Ethylbenzene 106 78 1311.05.28 ug/L Methyl tert-butyl ether (MTBE)123 58 1511.06.16 ug/L Methyl ethyl ketone 115 55 1452057.6 ug/L Methylene chloride 122 73 1261.06.08 ug/L Styrene 110 76 1341.05.52 ug/L 1,1,1,2-Tetrachloroethane 119 75 1351.05.96 ug/L 1,1,2,2-Tetrachloroethane 110 72 1321.05.52 ug/L Tetrachloroethene 105 78 1371.05.24 ug/L Toluene 107 78 1341.05.36 ug/L 1,1,1-Trichloroethane 121 64 1411.06.04 ug/L 1,1,2-Trichloroethane 111 72 1331.05.56 ug/L Trichloroethene 109 75 1381.05.44 ug/L Trichlorofluoromethane 118 58 1391.05.92 ug/L 1,2,3-Trichloropropane 113 67 1331.05.64 ug/L Vinyl chloride 79 66 1401.03.96 ug/L m+p-Xylenes 105 78 1331.010.5 ug/L o-Xylene 103 79 1361.05.16 ug/L Xylenes, Total 105 78 1361.015.7 ug/L Surr: 1,2-Dichloroethane-d4 106 70 1301.0 Surr: Dibromofluoromethane 110 77 1261.0 Surr: p-Bromofluorobenzene 102 76 1271.0 Surr: Toluene-d8 102 79 1221.0 Lab ID: B15011802-001A_MSD 02/03/15 02:25Sample Matrix Spike Duplicate Run: SV5972.I_150202A Benzene 103 71 133 201.0 2.35.16 ug/L Bromobenzene 112 78 133 201.0 3.65.60 ug/L Bromochloromethane 114 68 131 201.0 2.85.68 ug/L Bromodichloromethane 120 67 138 201.0 2.06.00 ug/L Bromoform 123 64 136 201.0 0.06.16 ug/L Bromomethane 88 60 138 201.0 324.40 ug/L R Carbon tetrachloride 120 61 144 201.0 5.86.00 ug/L Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. R - RPD exceeds advisory limit. Page 11 of 15268 Project:Ebbinghausen Client:Resource Technologies Inc Work Order:B15011740 QA/QC Summary Report 02/05/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits Qual Prepared by Billings, MT Branch Method:SW8260B Batch: R237677 Lab ID:B15011802-001A_MSD 02/03/15 02:25Sample Matrix Spike Duplicate Run: SV5972.I_150202A Chlorobenzene 106 78 136 201.0 0.75.32 ug/L Chlorodibromomethane 123 72 136 201.0 1.36.16 ug/L Chloroethane 114 64 136 201.0 2.15.68 ug/L Chloroform 109 69 133 201.0 2.95.44 ug/L Chloromethane 86 63 149 201.0 4.84.28 ug/L 1,2-Dibromoethane 113 75 131 201.0 0.05.64 ug/L 2-Chlorotoluene 103 74 135 201.0 0.85.16 ug/L Dibromomethane 116 72 133 201.0 0.75.80 ug/L 1,2-Dichlorobenzene 107 78 129 201.0 1.55.36 ug/L 4-Chlorotoluene 106 79 135 201.0 1.55.32 ug/L 1,3-Dichlorobenzene 108 79 132 201.0 2.25.40 ug/L 1,4-Dichlorobenzene 107 78 131 201.0 3.05.36 ug/L Dichlorodifluoromethane 102 55 141 201.0 4.85.12 ug/L 1,1-Dichloroethane 109 72 130 201.0 2.25.44 ug/L 1,2-Dichloroethane 124 57 146 201.0 0.66.20 ug/L 1,1-Dichloroethene 123 66 142 201.0 1.96.16 ug/L cis-1,2-Dichloroethene 111 74 133 201.0 0.05.56 ug/L trans-1,2-Dichloroethene 121 76 138 201.0 3.36.04 ug/L 1,2-Dichloropropane 107 72 135 201.0 1.55.36 ug/L 1,3-Dichloropropane 105 75 134 201.0 2.35.24 ug/L 2,2-Dichloropropane 112 42 167 201.0 2.85.60 ug/L 1,1-Dichloropropene 110 72 140 201.0 2.25.48 ug/L cis-1,3-Dichloropropene 114 75 132 201.0 0.05.68 ug/L trans-1,3-Dichloropropene 122 77 145 201.0 0.76.12 ug/L Ethylbenzene 106 78 131 201.0 0.05.28 ug/L Methyl tert-butyl ether (MTBE)120 58 151 201.0 2.66.00 ug/L Methyl ethyl ketone 111 55 145 20203.555.6 ug/L Methylene chloride 115 73 126 201.0 5.45.76 ug/L Styrene 113 76 134 201.0 2.25.64 ug/L 1,1,1,2-Tetrachloroethane 120 75 135 201.0 0.76.00 ug/L 1,1,2,2-Tetrachloroethane 107 72 132 201.0 2.95.36 ug/L Tetrachloroethene 106 78 137 201.0 0.85.28 ug/L Toluene 107 78 134 201.0 0.05.36 ug/L 1,1,1-Trichloroethane 116 64 141 201.0 4.15.80 ug/L 1,1,2-Trichloroethane 109 72 133 201.0 2.25.44 ug/L Trichloroethene 107 75 138 201.0 1.55.36 ug/L Trichlorofluoromethane 121 58 139 201.0 2.06.04 ug/L 1,2,3-Trichloropropane 114 67 133 201.0 1.45.72 ug/L Vinyl chloride 82 66 140 201.0 4.14.12 ug/L m+p-Xylenes 104 78 133 201.0 0.810.4 ug/L o-Xylene 106 79 136 201.0 2.35.28 ug/L Xylenes, Total 105 78 1361.015.7 ug/L Surr: 1,2-Dichloroethane-d4 108 70 1301.0 Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 12 of 15269 Project:Ebbinghausen Client:Resource Technologies Inc Work Order:B15011740 QA/QC Summary Report 02/05/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits Qual Prepared by Billings, MT Branch Method:SW8260B Batch: R237677 Lab ID:B15011802-001A_MSD 02/03/15 02:25Sample Matrix Spike Duplicate Run: SV5972.I_150202A Surr: Dibromofluoromethane 111 77 1261.0 Surr: p-Bromofluorobenzene 100 76 1271.0 Surr: Toluene-d8 102 79 1221.0 Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 13 of 15270 Shipping container/cooler in good condition? Custody seals intact on all shipping container(s)/cooler(s)? Custody seals intact on all sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time? (Exclude analyses that are considered field parameters such as pH, DO, Res Cl, Sulfite, Ferrous Iron, etc.) Container/Temp Blank temperature: Water - VOA vials have zero headspace? Water - pH acceptable upon receipt? Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes No No No No No No No No No No No No Not Present Not Present Not Present No VOA vials submitted Not Applicable 0.6°C On Ice 1/28/2015Tamara C. Logan Hand Del jrz Date Received: Received by: Login completed by: Carrier name: BL2000\jmueller 1/29/2015 Reviewed by: Reviewed Date: Contact and Corrective Action Comments: None Temp Blank received in all shipping container(s)/cooler(s)? Yes No Not Applicable Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as –dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Standard Reporting Procedures: Workorder Receipt Checklist Resource Technologies Inc B15011740 Page 14 of 15271 Page 15 of 15272 APPENDIX D Laboratory Analytical Reports – Soil Vapor 273 ANALYTICAL REPORT Mark Johnson Resource Technologies, Inc. 1050 E. Main, Ste 4 Bozeman, MT 59715 Phone: E-mail: (406) 585-8005 rti@montana.net Report Date:January 02, 2015 34-1436033Workorder: Ebbighausen 122414 EbbighausenPurchase Order: Project ID: Sampling SiteReceive DateCollect DateLab IDClient Sample ID VW-1 1436033001 12/22/14 12/24/14 Ebbighausen VW-2 1436033002 12/22/14 12/24/14 Ebbighausen ADDRESS 960 West LeVoy Drive, Salt Lake City, Utah, 84123 USA PHONE FAX+1 801 266 7700 +1 801 268 9992 ALS GROUP USA, CORP. Page 1 of 7 Fri, 01/02/15 12:00 PM ENVREP-V3.8 274 ANALYTICAL REPORT Project Manager:Rand Potter Client:Resource Technologies, Inc. Workorder:34-1436033 Analytical Results Sample ID:12/22/2014 12/24/20141436033001Lab ID: Collected: Received: VW-1 Ebbighausen Sampling Parameter:Air Volume 6 LMatrix: Media: Air Sulfur Summa 6 Liter Sampling Site: Analysis:EPA TO-15, Air Analyzed:12/29/2014 18:08 Batch: Instrument ID: IVOA/2784 (HBN: 141287)Percent Solid:NA 5972-W Report Basis:Wet Preparation:Not Applicable Analyte ppb ug/m³MDL (ppb)Qual.RL (ppb)Dilution Analysis Method - EPA TO-15 0.50<0.74ND 0.15 UDichlorodifluoromethane1 0.50<0.31ND 0.15 UChloromethane1 0.50<1.0ND 0.15 UFreon 114 1 0.50<0.38ND 0.15 UVinyl chloride 1 0.50<0.33ND 0.15 U1,3-Butadiene 1 0.50<0.58ND 0.15 UBromomethane1 0.50<0.40ND 0.15 UChloroethane1 0.500.870.16 0.15 JFreon 11 1 0.50<1.1ND 0.15 UFreon 113 1 0.50<0.59ND 0.15 U1,1-Dichloroethene 1 0.50<0.71ND 0.30 UAcetone1 0.50<0.47ND 0.15 UCarbon disulfide 1 0.50<0.52ND 0.15 UMethylene chloride 1 0.50<0.59ND 0.15 Utrans-1,2-Dichloroethene 1 0.50<0.54ND 0.15 UMethyl t-butyl ether 1 0.50<0.53ND 0.15 UVinyl acetate 1 0.50<0.44ND 0.15 U2-Butanone 1 0.50<0.59ND 0.15 Ucis-1,2-Dichloroethene 1 0.50<0.61ND 0.15 U1,1-Dichloroethane 1 1.0<0.54ND 0.15 UEthyl acetate 1 0.50<0.53ND 0.15 UHexane1 0.50<0.73ND 0.15 UChloroform1 0.50<0.44ND 0.15 UTetrahydrofuran1 0.50<0.61ND 0.15 U1,2-Dichloroethane 1 0.50<0.82ND 0.15 U1,1,1-Trichloroethane 1 0.50<0.94ND 0.15 UCarbon tetrachloride 1 0.50<0.48ND 0.15 UBenzene1 0.50<0.52ND 0.15 UCyclohexane1 0.50<0.81ND 0.15 UTrichloroethene1 0.50<0.73ND 0.15 U1,2-Dichloropropane 1 0.50<1.0ND 0.15 UBromodichloromethane1 0.50<0.61ND 0.15 UHeptane1 0.50<0.68ND 0.15 Ucis-1,3-Dichloropropene 1 0.50<0.61ND 0.15 U4-Methyl-2-pentanone 1 0.50<0.68ND 0.15 Utrans-1,3-Dichloropropene 1 0.50<0.82ND 0.15 U1,1,2-Trichloroethane 1 Page 2 of 7 Fri, 01/02/15 12:00 PM ENVREP-V3.8 Results Continued on Next Page 275 ANALYTICAL REPORT Project Manager:Rand Potter Client:Resource Technologies, Inc. Workorder:34-1436033 Analytical Results Sample ID:12/22/2014 12/24/20141436033001Lab ID: Collected: Received: VW-1 Ebbighausen Sampling Parameter:Air Volume 6 LMatrix: Media: Air Sulfur Summa 6 Liter Sampling Site: Analysis:EPA TO-15, Air Analyzed:12/29/2014 18:08 Batch: Instrument ID: IVOA/2784 (HBN: 141287)Percent Solid:NA 5972-W Report Basis:Wet Preparation:Not Applicable Analyte ppb ug/m³MDL (ppb)Qual.RL (ppb)Dilution Analysis Method - EPA TO-15 0.50<0.57ND 0.15 UToluene1 1.0<1.2ND 0.30 U2-Hexanone 1 0.50517.5 0.15Tetrachloroethene 1 0.50<1.3ND 0.15 UDibromochloromethane1 0.50<1.2ND 0.15 U1,2-Dibromoethane 1 0.50<0.69ND 0.15 UChlorobenzene1 0.50<0.65ND 0.15 UEthyl benzene 1 0.50<0.65ND 0.15 Um,p-Xylene 1 0.50<0.65ND 0.15 Uo-Xylene 1 0.50<0.64ND 0.15 UStyrene1 0.50<1.6ND 0.15 UBromoform1 0.50<1.0ND 0.15 U1,1,2,2-Tetrachloroethane 1 0.50<0.74ND 0.15 U4-Ethyl toluene 1 0.50<0.74ND 0.15 U1,3,5-Trimethylbenzene 1 0.50<0.74ND 0.15 U1,2,4-Trimethylbenzene 1 0.50<0.90ND 0.15 U1,3-Dichlorobenzene 1 0.50<0.90ND 0.15 U1,4-Dichlorobenzene 1 1.0<1.6ND 0.30 UBenzyl chloride 1 1.0<1.8ND 0.30 U1,2-Dichlorobenzene 1 1.0<2.2ND 0.30 U1,2,4-Trichlorobenzene 1 1.0<3.2ND 0.30 UHexachlorobutadiene1 NA22053NA JTotal Volatile Organics 1 Sample ID:12/22/2014 12/24/20141436033002Lab ID: Collected: Received: VW-2 Ebbighausen Sampling Parameter:Air Volume 6 LMatrix: Media: Air Sulfur Summa 6 Liter Sampling Site: Analysis:EPA TO-15, Air Analyzed:12/29/2014 19:21 Batch: Instrument ID: IVOA/2784 (HBN: 141287)Percent Solid:NA 5972-W Report Basis:Wet Preparation:Not Applicable Analyte ppb ug/m³MDL (ppb)Qual.RL (ppb)Dilution Analysis Method - EPA TO-15 0.50<0.74ND 0.15 UDichlorodifluoromethane1 0.50<0.31ND 0.15 UChloromethane1 0.50<1.0ND 0.15 UFreon 114 1 0.50<0.38ND 0.15 UVinyl chloride 1 0.50<0.33ND 0.15 U1,3-Butadiene 1 Page 3 of 7 Fri, 01/02/15 12:00 PM ENVREP-V3.8 Results Continued on Next Page 276 ANALYTICAL REPORT Project Manager:Rand Potter Client:Resource Technologies, Inc. Workorder:34-1436033 Analytical Results Sample ID:12/22/2014 12/24/20141436033002Lab ID: Collected: Received: VW-2 Ebbighausen Sampling Parameter:Air Volume 6 LMatrix: Media: Air Sulfur Summa 6 Liter Sampling Site: Analysis:EPA TO-15, Air Analyzed:12/29/2014 19:21 Batch: Instrument ID: IVOA/2784 (HBN: 141287)Percent Solid:NA 5972-W Report Basis:Wet Preparation:Not Applicable Analyte ppb ug/m³MDL (ppb)Qual.RL (ppb)Dilution Analysis Method - EPA TO-15 0.50<0.58ND 0.15 UBromomethane1 0.50<0.40ND 0.15 UChloroethane1 0.500.870.15 0.15 JFreon 11 1 0.50<1.1ND 0.15 UFreon 113 1 0.50<0.59ND 0.15 U1,1-Dichloroethene 1 0.50100430.30 EAcetone1 0.50<0.47ND 0.15 UCarbon disulfide 1 0.50<0.52ND 0.15 UMethylene chloride 1 0.50<0.59ND 0.15 Utrans-1,2-Dichloroethene 1 0.50<0.54ND 0.15 UMethyl t-butyl ether 1 0.50<0.53ND 0.15 UVinyl acetate 1 0.50103.5 0.152-Butanone 1 0.50<0.59ND 0.15 Ucis-1,2-Dichloroethene 1 0.50<0.61ND 0.15 U1,1-Dichloroethane 1 1.0<0.54ND 0.15 UEthyl acetate 1 0.50<0.53ND 0.15 UHexane1 0.502.00.41 0.15 JChloroform1 0.50103.5 0.15Tetrahydrofuran 1 0.50<0.61ND 0.15 U1,2-Dichloroethane 1 0.50<0.82ND 0.15 U1,1,1-Trichloroethane 1 0.50<0.94ND 0.15 UCarbon tetrachloride 1 0.50<0.48ND 0.15 UBenzene1 0.50<0.52ND 0.15 UCyclohexane1 0.50<0.81ND 0.15 UTrichloroethene1 0.50<0.73ND 0.15 U1,2-Dichloropropane 1 0.50<1.0ND 0.15 UBromodichloromethane1 0.50<0.61ND 0.15 UHeptane1 0.50<0.68ND 0.15 Ucis-1,3-Dichloropropene 1 0.50<0.61ND 0.15 U4-Methyl-2-pentanone 1 0.50<0.68ND 0.15 Utrans-1,3-Dichloropropene 1 0.50<0.82ND 0.15 U1,1,2-Trichloroethane 1 0.506.51.7 0.15Toluene 1 1.0<1.2ND 0.30 U2-Hexanone 1 0.501.10.16 0.15 JTetrachloroethene1 0.50<1.3ND 0.15 UDibromochloromethane1 0.50<1.2ND 0.15 U1,2-Dibromoethane 1 Page 4 of 7 Fri, 01/02/15 12:00 PM ENVREP-V3.8 Results Continued on Next Page 277 ANALYTICAL REPORT Project Manager:Rand Potter Client:Resource Technologies, Inc. Workorder:34-1436033 Analytical Results Sample ID:12/22/2014 12/24/20141436033002Lab ID: Collected: Received: VW-2 Ebbighausen Sampling Parameter:Air Volume 6 LMatrix: Media: Air Sulfur Summa 6 Liter Sampling Site: Analysis:EPA TO-15, Air Analyzed:12/29/2014 19:21 Batch: Instrument ID: IVOA/2784 (HBN: 141287)Percent Solid:NA 5972-W Report Basis:Wet Preparation:Not Applicable Analyte ppb ug/m³MDL (ppb)Qual.RL (ppb)Dilution Analysis Method - EPA TO-15 0.50<0.69ND 0.15 UChlorobenzene1 0.503.40.79 0.15Ethyl benzene 1 0.50184.0 0.15m,p-Xylene 1 0.505.11.2 0.15o-Xylene 1 0.50<0.64ND 0.15 UStyrene1 0.50<1.6ND 0.15 UBromoform1 0.50<1.0ND 0.15 U1,1,2,2-Tetrachloroethane 1 0.503.60.73 0.154-Ethyl toluene 1 0.507.21.5 0.151,3,5-Trimethylbenzene 1 0.50204.0 0.151,2,4-Trimethylbenzene 1 0.50<0.90ND 0.15 U1,3-Dichlorobenzene 1 0.50<0.90ND 0.15 U1,4-Dichlorobenzene 1 1.0<1.6ND 0.30 UBenzyl chloride 1 1.0<1.8ND 0.30 U1,2-Dichlorobenzene 1 1.0<2.2ND 0.30 U1,2,4-Trichlorobenzene 1 1.0<3.2ND 0.30 UHexachlorobutadiene1 NA410100NA JTotal Volatile Organics 1 Analysis:EPA TO-15, Air Analyzed:12/29/2014 19:21 Batch: Instrument ID: IVOA/2784 (HBN: 141287)Percent Solid:NA 5972-W Report Basis:Wet Preparation:Not Applicable Tentatively Identified Compound ppb Retention Time Dilution Qual. Analysis Method - EPA TO-15 J7.5621 1Ethanol J18.345.8 1Decane J18.782.7 1Decane, 4-methyl- Comments Quality Control:EPA TO-15 - (HBN: 141287) The LCSD result for 4-methyl-2-pentanone is outside of limits. The acetone result in the CCS is outside of +/-30%. The surrogate recovery for 1435360001 is outside of limits. Report Authorization Analyst Peer ReviewMethod (/S/ is an electronic signature that complies with 21 CFR Part 11) EPA TO-15 /S/ Lisa M. Reid 01/02/2015 10:01 01/02/2015 11:01 /S/ Jorden Baum Page 5 of 7 Fri, 01/02/15 12:00 PM ENVREP-V3.8 278 ANALYTICAL REPORT Project Manager:Rand Potter Client:Resource Technologies, Inc. Workorder:34-1436033 Laboratory Contact Information (801) 266-7700 alslt.lab@ALSGlobal.com www.alsslc.com ALS Environmental 960 W Levoy Drive Salt Lake City, Utah 84123 Phone: Email: Web: The results provided in this report relate only to the items tested. Samples were received in acceptable condition unless otherwise noted. Samples have not been blank corrected unless otherwise noted. This test report shall not be reproduced, except in full, without written approval of ALS. General Lab Comments ALS provides professional analytical services for all samples submitted. ALS is not in a position to interpret the data and assumes no responsibility for the quality of the samples submitted. All quality control samples processed with the samples in this report yielded acceptable results unless otherwise noted. ALS is accredited for specific fields of testing (scopes) in the following testing sectors. The quality system implemented at ALS conforms to accreditation requirements and is applied to all analytical testing performed by ALS. The following table lists testing sector, accreditation body, accreditation number and website. Please contact these accrediting bodies or your ALS project manager for the current scope of accreditation that applies to your analytical testing. Testing Sector Accreditation Body Certificate Number Website Environmental ACLASS (DoD ELAP) Utah (NELAC) Nevada Oklahoma Iowa Florida (TNI) ADE-1420 DATA1 UT00009 UT00009 IA# 376 E871067 http://www.aclasscorp.com http://health.utah.gov/lab/labimp/ http://ndep.nv.gov/bsdw/labservice.htm http://www.deq.state.ok.us/CSDnew/ http://www.iowadnr.gov/InsideDNR/RegulatoryWater.aspx http://www.dep.state.fl.us/labs/bars/sas/qa/ Industrial Hygiene 101574 http://www.aihaaccreditedlabs.orgAIHA (ISO 17025 & AIHA IHLAP/ELLAP) Lead Testing: CPSC ACLASS (ISO 17025, CPSC)ADE-1420 http://www.aclasscorp.com Soil, Dust, Paint ,Air AIHA (ISO 17025, AIHA ELLAP and NLLAP) 101574 http://www.aihaaccreditedlabs.org Dietary Supplements ACLASS (ISO 17025)ADE-1420 http://www.aclasscorp.com Texas (TNI)T104704456-11-1 http://www.tceq.texas.gov/field/qa/lab_accred_certif.html (Standard) Page 6 of 7 Fri, 01/02/15 12:00 PM ENVREP-V3.8 279 ANALYTICAL REPORT Project Manager:Rand Potter Client:Resource Technologies, Inc. Workorder:34-1436033 MDL = Method Detection Limit, a statistical estimate of method/media/instrument sensitivity. RL = Reporting Limit, a verified value of method/media/instrument sensitivity. CRDL = Contract Required Detection Limit Reg. Limit = Regulatory Limit. ND = Not Detected, testing result not detected above the MDL or RL. < This testing result is less than the numerical value. ** No result could be reported, see sample comments for details. U = Qualifier indicates that the analyte was not detected above the MDL. J = Qualifier Indicates that the analyte value is between the MDL and the RL. It is also used to indicate an estimated value for tentatively identified compounds in mass spectrometry where a 1:1 response is assumed. B = Qualifier indicates that the analyte was detected in the blank. E = Qualifier indicates that the analyte result exceeds calibration range. P = Qualifier indicates that the RPD between the two columns is greater than 40%. Result Symbol Definitions Qualifier Symbol Definitions Page 7 of 7 Fri, 01/02/15 12:00 PM ENVREP-V3.8 280 281 282 Bozeman Recreation & Parks Advisory Board P.O. Box 1230 · Bozeman, MT · 59771 Growth Policy Amendment Review PROJECT: The Villas PLANNER: Valerie Sutton/Brian Krueger FROM: Subdivision Review Committee DATE OF REVIEW: 3/6/2015 OVERVIEW: • The subject parcel is a 6.5-acre lot that sits on the northern boundary of the East Gallatin Recreation Area (EGRA). • It is currently not within the city limits and has a county zoning designation of light industrial. • Its current designation in the Community Plan is Park, Recreation, and Open Space. • The applicant is hoping to purchase the land, change the designation to residential by way of a Growth Policy Amendment (GPA), and develop a subdivision on the site. COMMENTS: • Proximity to the old city dump creates liability issues for residential designation similar to those in the Bridger Creek Subdivision. The groundwater and vapor report is inconclusive. However as a subcommittee of the Recreation and Parks Advisory Board this is outside our purview. • There is a neighboring subdivision on Turtle Way that gained residential status through a GPA. Precedent? • In our comments of August, 2014 we stated our opinion that residential was preferable to industrial in proximity to an existing park, however we think that park and open space is a far better designation in this instance; particularly given that the access road to the EGRA runs through the middle of the parcel. RECOMMENDATION: • Having reviewed the amendment process in the Community Plan we cannot recommend this amendment proposal. The amendment does not meet the criteria enumerated it the Plan, chapters 17.3 and 17.4. (Shown in italics where quoted) • The applicant is not the landowner at this time so is not qualified to initiate the amendment. However if the applicant were to purchase the land we still would not endorse the change without seeing evidence that the amendment would create a better use than park and open space. 283 • We do not see that the amendment would “cure a deficiency in the growth policy” or “better respond to the needs of the general community”. This is a fundamental condition of the amendment process and has clearly not been met. • We are concerned about the health and safety issues and feel that the proposal fails the: “negatively affect the livability of the area or the health and safety of the residents” criterion. FISCAL EFFECTS: • None ALTERNATIVES: • The applicant could purchase the parcel and embark on the amendment process in hopes that further groundwater mitigation could solve the pollution liability concerns and present a subdivision plan so attractive that “an extremely compelling case can be made for significant public benefit from the amendment”. Respectfully submitted, Sandy Dodge, Chair, Subdivision Review Committee 284 285 286 287 4/27/15 dparker DATE: April 30, 2015 TO: Greg Sullivan FROM: Doug Parker SUBJECT: Old Bozeman Landfill DISTRIBUTION: Hydrometrics sampled two wells and two vapor extraction wells located on the Hash property adjacent to the historic Bozeman East Gallatin landfill on March 5, 2015. Water samples were sent to Energy Laboratories in Helena and soil vapor samples were sent to ALS laboratories in Salt Lake. Analytical results indicate near neutral water with low levels of nitrate and metals, possibly slightly elevated chloride and only one measurable organic parameter (vinyl chloride in well MW-2). The vinyl chloride concentration of 0.66 μg/L in well MW-2 is above the Montana water quality standard for groundwater of 0.2 μg/L . The vapor samples indicated measurable levels of about 30 volatile organic compounds between the two vapor sample points, but at very low levels. This March 2015 monitoring produced results generally similar to those of RTI collected in December 2014. There were slightly more organic compounds identified in the vapor samples and only vinyl chloride in well MW-2. In December well MW-2 had detectible vinyl chloride, but also reported measureable chloroethane and toluene, which were not detected in March. Vapor extraction wells VW-1 and VW-2 had 2 and 16 measurable volatile organic compounds respectively in December compared to 27 and 22 measurable parameters in March. In December the Total Volatile Organics value for VW-1 was 53 ppb while it was 130 ppb in March; December Total Volatile Organics in VW-2 measured 100 ppb versus 130 ppb in March. The results of both sampling events indicate existence of contaminants in both water and soil vapor consistent with landfill leachate; however, at this point the source is not known. The only parameter that exceeds water quality standards is vinyl chloride. Soil gas standards generally do not exist, but in the attached table the measured values are compared to USEPA’s Reference Concentrations for Chronic Inhalation (RfC) documented in EPA’s Integrated Risk Information System (IRIS) and to EPA Regional Screening Levels for Residential Ambient Air (RSL). None of the measured values exceed the risk based inhalation values for parameters which have RfCs; however RSLs are exceeded for benzene, trimethylbenzene and xylenes at both soil vapor sampling sites. Existing Hydrometrics, Inc. consulting scientists and engineers 288 4/27/15 dparker information is not adequate to determine transport rates, direction or potential impacts to adjacent landowners. The information we’ve gathered is consistent with the information on the site in the CECRA/CERCLIS database. The existing data only provides an indication that historic landfill activities may have had an impact on groundwater and soil vapor. However, it is not clear what the extent of contamination could be, what the exact direction of groundwater flow is and if or where contaminants might affect adjacent landowners. The likely next step at this point would be to initiate additional site investigation steps to better define the nature and extent of contamination. It would be necessary to see the site and obtain some more information to allow development of a detailed study plan. However, it is likely that several additional wells and possibly some additional soil vapor extraction points would be required to further define site conditions. There are a number of residences in the vicinity of the landfill and sampling sites and monitoring of their water supplies (if there are individual wells) may be appropriate. Attachments: Energy Labs Report ALS Report Soil Vapor Summary Hillman Well Log GWIC List 289 ANALYTICAL SUMMARY REPORT The analyses presented in this report were performed by Energy Laboratories, Inc., 3161 E. Lyndale Ave., Helena, MT 59604, unless otherwise noted. Any exceptions or problems with the analyses are noted in the Laboratory Analytical Report, the QA/QC Summary Report, or the Case Narrative. The results as reported relate only to the item(s) submitted for testing. If you have any questions regarding these test results, please call. Lab ID Client Sample ID Collect Date Receive Date Matrix Test Report Approved By: H15030090-001 BCL-1503-100 03/05/15 9:50 03/06/15 Aqueous Metals by ICP/ICPMS, DissolvedConductivity EPH-Sep Funnel ExtractionHydrocarbons, Extractable Petroleum ScreenAnions by Ion ChromatographyNitrogen, Nitrate + NitritepH8260-Volatile Organic Comp, 40 CFR Part 258 App I H15030090-002 BCL-1503-101 03/05/15 10:05 03/06/15 Aqueous Same As Above H15030090-003 BCL-1503-102 03/05/15 10:40 03/06/15 Aqueous Same As Above H15030090-004 TB 4686 03/05/15 9:50 03/06/15 Trip Blank 8260-Volatile Organic Comp, 40 CFR Part 258 App I Hydrometrics Inc Project Name:15012 East Gallatin Landfill Work Order:H15030090 3020 Bozeman Ave Helena, MT 59601 March 24, 2015 Energy Laboratories Inc Helena MT received the following 4 samples for Hydrometrics Inc on 3/6/2015 for analysis. Page 1 of 35290 Project:15012 East Gallatin Landfill CLIENT:Hydrometrics Inc Work Order:H15030090 CASE NARRATIVE 03/24/15Report Date: Tests associated with analyst identified as ELI-B were subcontracted to Energy Laboratories, 1120 S. 27th St., Billings, MT, EPA Number MT00005. Page 2 of 35291 LABORATORY ANALYTICAL REPORT Client:Hydrometrics Inc Project:15012 East Gallatin Landfill Lab ID:H15030090-001 Client Sample ID:BCL-1503-100 Collection Date:03/05/15 09:50 Matrix:Aqueous Report Date:03/24/15 DateReceived:03/06/15 Prepared by Helena, MT Branch Analyses Result Units Analysis Date / ByRLMethod MCL/ QCLQualifiers PHYSICAL PROPERTIES H 03/06/15 15:45 / AHN0.1s.u.7.3pH A4500-H B 03/10/15 10:42 / SRW1umhos/cm787Conductivity @ 25 C A2510 B INORGANICS 03/10/15 15:56 / SRW1mg/L28Chloride E300.0 03/11/15 14:18 / SRW1mg/L23Sulfate E300.0 NUTRIENTS 03/09/15 15:45 / cmm0.01mg/L0.35Nitrogen, Nitrate+Nitrite as N E353.2 METALS, DISSOLVED 03/12/15 20:58 / dck0.0005mg/LNDAntimony E200.8 03/12/15 20:58 / dck0.001mg/LNDArsenic E200.8 03/12/15 20:58 / dck0.003mg/L0.139Barium E200.8 03/12/15 20:58 / dck0.0008mg/LNDBeryllium E200.8 03/12/15 20:58 / dck0.00003mg/LNDCadmium E200.8 03/12/15 20:58 / dck0.01mg/LNDChromium E200.8 03/12/15 20:58 / dck0.01mg/LNDCobalt E200.8 03/12/15 20:58 / dck0.002mg/LNDCopper E200.8 03/12/15 20:58 / dck0.02mg/L0.09Iron E200.8 03/12/15 20:58 / dck0.0003mg/LNDLead E200.8 03/12/15 20:58 / dck0.002mg/LNDNickel E200.8 03/12/15 20:58 / dck0.001mg/LNDSelenium E200.8 03/12/15 20:58 / dck0.0002mg/LNDSilver E200.8 03/12/15 20:58 / dck0.0002mg/LNDThallium E200.8 03/12/15 20:58 / dck0.1mg/LNDVanadium E200.8 03/12/15 20:58 / dck0.008mg/LNDZinc E200.8 VOLATILE ORGANIC COMPOUNDS 03/17/15 14:11 / eli-b1620ug/LNDAcetone SW8260B 03/17/15 14:11 / eli-b163.0ug/LNDAcrylonitrile SW8260B 03/17/15 14:11 / eli-b160.50ug/LNDBenzene SW8260B 03/17/15 14:11 / eli-b160.50ug/LNDBromochloromethane SW8260B 03/17/15 14:11 / eli-b160.50ug/LNDBromodichloromethane SW8260B 03/17/15 14:11 / eli-b160.50ug/LNDBromoform SW8260B 03/17/15 14:11 / eli-b160.50ug/LNDBromomethane SW8260B 03/17/15 14:11 / eli-b161.0ug/LNDCarbon disulfide SW8260B 03/17/15 14:11 / eli-b160.50ug/LNDCarbon tetrachloride SW8260B 03/17/15 14:11 / eli-b160.50ug/LNDChlorobenzene SW8260B 03/17/15 14:11 / eli-b160.50ug/LNDChlorodibromomethane SW8260B 03/17/15 14:11 / eli-b160.50ug/LNDChloroethane SW8260B 03/17/15 14:11 / eli-b160.50ug/LNDChloroform SW8260B 03/17/15 14:11 / eli-b160.50ug/LNDChloromethane SW8260B 03/17/15 14:11 / eli-b161.0ug/LND1,2-Dibromo-3-chloropropane SW8260B Report Definitions: RL - Analyte reporting limit.MCL - Maximum contaminant level. QCL - Quality control limit.ND - Not detected at the reporting limit. H - Analysis performed past recommended holding time. Page 3 of 35292 LABORATORY ANALYTICAL REPORT Client:Hydrometrics Inc Project:15012 East Gallatin Landfill Lab ID:H15030090-001 Client Sample ID:BCL-1503-100 Collection Date:03/05/15 09:50 Matrix:Aqueous Report Date:03/24/15 DateReceived:03/06/15 Prepared by Helena, MT Branch Analyses Result Units Analysis Date / ByRLMethod MCL/ QCLQualifiers VOLATILE ORGANIC COMPOUNDS 03/17/15 14:11 / eli-b160.50ug/LND1,2-Dibromoethane SW8260B 03/17/15 14:11 / eli-b160.50ug/LNDDibromomethane SW8260B 03/17/15 14:11 / eli-b160.50ug/LND1,2-Dichlorobenzene SW8260B 03/17/15 14:11 / eli-b160.50ug/LND1,4-Dichlorobenzene SW8260B 03/17/15 14:11 / eli-b161.0ug/LNDtrans-1,4-Dichloro-2-butene SW8260B 03/17/15 14:11 / eli-b160.50ug/LNDDichlorodifluoromethane SW8260B 03/17/15 14:11 / eli-b160.50ug/LND1,1-Dichloroethane SW8260B 03/17/15 14:11 / eli-b160.50ug/LND1,2-Dichloroethane SW8260B 03/17/15 14:11 / eli-b160.50ug/LND1,1-Dichloroethene SW8260B 03/17/15 14:11 / eli-b160.50ug/LNDcis-1,2-Dichloroethene SW8260B 03/17/15 14:11 / eli-b160.50ug/LNDtrans-1,2-Dichloroethene SW8260B 03/17/15 14:11 / eli-b160.50ug/LND1,2-Dichloropropane SW8260B 03/17/15 14:11 / eli-b160.30ug/LNDcis-1,3-Dichloropropene SW8260B 03/17/15 14:11 / eli-b160.30ug/LNDtrans-1,3-Dichloropropene SW8260B 03/17/15 14:11 / eli-b160.50ug/LNDEthylbenzene SW8260B 03/17/15 14:11 / eli-b1620ug/LND2-Hexanone SW8260B 03/17/15 14:11 / eli-b161.0ug/LNDIodomethane SW8260B 03/17/15 14:11 / eli-b1620ug/LNDMethyl ethyl ketone SW8260B 03/17/15 14:11 / eli-b1620ug/LNDMethyl isobutyl ketone SW8260B 03/17/15 14:11 / eli-b160.50ug/LNDMethylene chloride SW8260B 03/17/15 14:11 / eli-b160.50ug/LNDStyrene SW8260B 03/17/15 14:11 / eli-b160.50ug/LND1,1,1,2-Tetrachloroethane SW8260B 03/17/15 14:11 / eli-b160.50ug/LND1,1,2,2-Tetrachloroethane SW8260B 03/17/15 14:11 / eli-b160.50ug/LNDTetrachloroethene SW8260B 03/17/15 14:11 / eli-b160.50ug/LNDToluene SW8260B 03/17/15 14:11 / eli-b160.50ug/LND1,1,1-Trichloroethane SW8260B 03/17/15 14:11 / eli-b160.50ug/LND1,1,2-Trichloroethane SW8260B 03/17/15 14:11 / eli-b160.50ug/LNDTrichloroethene SW8260B 03/17/15 14:11 / eli-b160.50ug/LNDTrichlorofluoromethane SW8260B 03/17/15 14:11 / eli-b160.50ug/LND1,2,3-Trichloropropane SW8260B 03/17/15 14:11 / eli-b161.0ug/LNDVinyl acetate SW8260B 03/17/15 14:11 / eli-b160.40ug/LNDVinyl chloride SW8260B 03/17/15 14:11 / eli-b161.0ug/LNDm+p-Xylenes SW8260B 03/17/15 14:11 / eli-b160.50ug/LNDo-Xylene SW8260B 03/17/15 14:11 / eli-b160.50ug/LNDXylenes, Total SW8260B 03/17/15 14:11 / eli-b1670-130%REC92.0 Surr: 1,2-Dichloroethane-d4 SW8260B 03/17/15 14:11 / eli-b1677-126%REC97.0 Surr: Dibromofluoromethane SW8260B 03/17/15 14:11 / eli-b1676-127%REC106 Surr: p-Bromofluorobenzene SW8260B 03/17/15 14:11 / eli-b1679-122%REC99.0 Surr: Toluene-d8 SW8260B EXTRACTABLE PETROLEUM HYDROCARBONS-SCREEN ANALYSIS 03/11/15 19:42 / JRS300ug/LNDTotal Extractable Hydrocarbons SW8015M1000 03/11/15 19:42 / JRS40-140%REC87.0 Surr: o-Terphenyl SW8015M Report Definitions: RL - Analyte reporting limit.MCL - Maximum contaminant level. QCL - Quality control limit.ND - Not detected at the reporting limit. Page 4 of 35293 LABORATORY ANALYTICAL REPORT Client:Hydrometrics Inc Project:15012 East Gallatin Landfill Lab ID:H15030090-001 Client Sample ID:BCL-1503-100 Collection Date:03/05/15 09:50 Matrix:Aqueous Report Date:03/24/15 DateReceived:03/06/15 Prepared by Helena, MT Branch Analyses Result Units Analysis Date / ByRLMethod MCL/ QCLQualifiers EXTRACTABLE PETROLEUM HYDROCARBONS-SCREEN ANALYSIS - Note: Total Extractable Hydrocarbons are defined as the total hydrocarbon responses regardless of elution time. Report Definitions: RL - Analyte reporting limit.MCL - Maximum contaminant level. QCL - Quality control limit.ND - Not detected at the reporting limit. Page 5 of 35294 LABORATORY ANALYTICAL REPORT Client:Hydrometrics Inc Project:15012 East Gallatin Landfill Lab ID:H15030090-002 Client Sample ID:BCL-1503-101 Collection Date:03/05/15 10:05 Matrix:Aqueous Report Date:03/24/15 DateReceived:03/06/15 Prepared by Helena, MT Branch Analyses Result Units Analysis Date / ByRLMethod MCL/ QCLQualifiers PHYSICAL PROPERTIES H 03/06/15 15:48 / AHN0.1s.u.7.2pH A4500-H B 03/10/15 10:45 / SRW1umhos/cm791Conductivity @ 25 C A2510 B INORGANICS 03/10/15 16:30 / SRW1mg/L28Chloride E300.0 03/11/15 14:29 / SRW1mg/L23Sulfate E300.0 NUTRIENTS 03/09/15 15:46 / cmm0.01mg/L0.36Nitrogen, Nitrate+Nitrite as N E353.2 METALS, DISSOLVED 03/12/15 21:02 / dck0.0005mg/LNDAntimony E200.8 03/12/15 21:02 / dck0.001mg/LNDArsenic E200.8 03/12/15 21:02 / dck0.003mg/L0.136Barium E200.8 03/12/15 21:02 / dck0.0008mg/LNDBeryllium E200.8 03/12/15 21:02 / dck0.00003mg/LNDCadmium E200.8 03/12/15 21:02 / dck0.01mg/LNDChromium E200.8 03/12/15 21:02 / dck0.01mg/LNDCobalt E200.8 03/12/15 21:02 / dck0.002mg/LNDCopper E200.8 03/12/15 21:02 / dck0.02mg/L0.10Iron E200.8 03/12/15 21:02 / dck0.0003mg/LNDLead E200.8 03/12/15 21:02 / dck0.002mg/L0.002Nickel E200.8 03/12/15 21:02 / dck0.001mg/LNDSelenium E200.8 03/12/15 21:02 / dck0.0002mg/LNDSilver E200.8 03/12/15 21:02 / dck0.0002mg/LNDThallium E200.8 03/12/15 21:02 / dck0.1mg/LNDVanadium E200.8 03/12/15 21:02 / dck0.008mg/LNDZinc E200.8 VOLATILE ORGANIC COMPOUNDS 03/17/15 17:37 / eli-b1620ug/LNDAcetone SW8260B 03/17/15 17:37 / eli-b163.0ug/LNDAcrylonitrile SW8260B 03/17/15 17:37 / eli-b160.50ug/LNDBenzene SW8260B 03/17/15 17:37 / eli-b160.50ug/LNDBromochloromethane SW8260B 03/17/15 17:37 / eli-b160.50ug/LNDBromodichloromethane SW8260B 03/17/15 17:37 / eli-b160.50ug/LNDBromoform SW8260B 03/17/15 17:37 / eli-b160.50ug/LNDBromomethane SW8260B 03/17/15 17:37 / eli-b161.0ug/LNDCarbon disulfide SW8260B 03/17/15 17:37 / eli-b160.50ug/LNDCarbon tetrachloride SW8260B 03/17/15 17:37 / eli-b160.50ug/LNDChlorobenzene SW8260B 03/17/15 17:37 / eli-b160.50ug/LNDChlorodibromomethane SW8260B 03/17/15 17:37 / eli-b160.50ug/LNDChloroethane SW8260B 03/17/15 17:37 / eli-b160.50ug/LNDChloroform SW8260B 03/17/15 17:37 / eli-b160.50ug/LNDChloromethane SW8260B 03/17/15 17:37 / eli-b161.0ug/LND1,2-Dibromo-3-chloropropane SW8260B Report Definitions: RL - Analyte reporting limit.MCL - Maximum contaminant level. QCL - Quality control limit.ND - Not detected at the reporting limit. H - Analysis performed past recommended holding time. Page 6 of 35295 LABORATORY ANALYTICAL REPORT Client:Hydrometrics Inc Project:15012 East Gallatin Landfill Lab ID:H15030090-002 Client Sample ID:BCL-1503-101 Collection Date:03/05/15 10:05 Matrix:Aqueous Report Date:03/24/15 DateReceived:03/06/15 Prepared by Helena, MT Branch Analyses Result Units Analysis Date / ByRLMethod MCL/ QCLQualifiers VOLATILE ORGANIC COMPOUNDS 03/17/15 17:37 / eli-b160.50ug/LND1,2-Dibromoethane SW8260B 03/17/15 17:37 / eli-b160.50ug/LNDDibromomethane SW8260B 03/17/15 17:37 / eli-b160.50ug/LND1,2-Dichlorobenzene SW8260B 03/17/15 17:37 / eli-b160.50ug/LND1,4-Dichlorobenzene SW8260B 03/17/15 17:37 / eli-b161.0ug/LNDtrans-1,4-Dichloro-2-butene SW8260B 03/17/15 17:37 / eli-b160.50ug/LNDDichlorodifluoromethane SW8260B 03/17/15 17:37 / eli-b160.50ug/LND1,1-Dichloroethane SW8260B 03/17/15 17:37 / eli-b160.50ug/LND1,2-Dichloroethane SW8260B 03/17/15 17:37 / eli-b160.50ug/LND1,1-Dichloroethene SW8260B 03/17/15 17:37 / eli-b160.50ug/LNDcis-1,2-Dichloroethene SW8260B 03/17/15 17:37 / eli-b160.50ug/LNDtrans-1,2-Dichloroethene SW8260B 03/17/15 17:37 / eli-b160.50ug/LND1,2-Dichloropropane SW8260B 03/17/15 17:37 / eli-b160.30ug/LNDcis-1,3-Dichloropropene SW8260B 03/17/15 17:37 / eli-b160.30ug/LNDtrans-1,3-Dichloropropene SW8260B 03/17/15 17:37 / eli-b160.50ug/LNDEthylbenzene SW8260B 03/17/15 17:37 / eli-b1620ug/LND2-Hexanone SW8260B 03/17/15 17:37 / eli-b161.0ug/LNDIodomethane SW8260B 03/17/15 17:37 / eli-b1620ug/LNDMethyl ethyl ketone SW8260B 03/17/15 17:37 / eli-b1620ug/LNDMethyl isobutyl ketone SW8260B 03/17/15 17:37 / eli-b160.50ug/LNDMethylene chloride SW8260B 03/17/15 17:37 / eli-b160.50ug/LNDStyrene SW8260B 03/17/15 17:37 / eli-b160.50ug/LND1,1,1,2-Tetrachloroethane SW8260B 03/17/15 17:37 / eli-b160.50ug/LND1,1,2,2-Tetrachloroethane SW8260B 03/17/15 17:37 / eli-b160.50ug/LNDTetrachloroethene SW8260B 03/17/15 17:37 / eli-b160.50ug/LNDToluene SW8260B 03/17/15 17:37 / eli-b160.50ug/LND1,1,1-Trichloroethane SW8260B 03/17/15 17:37 / eli-b160.50ug/LND1,1,2-Trichloroethane SW8260B 03/17/15 17:37 / eli-b160.50ug/LNDTrichloroethene SW8260B 03/17/15 17:37 / eli-b160.50ug/LNDTrichlorofluoromethane SW8260B 03/17/15 17:37 / eli-b160.50ug/LND1,2,3-Trichloropropane SW8260B 03/17/15 17:37 / eli-b161.0ug/LNDVinyl acetate SW8260B 03/17/15 17:37 / eli-b160.40ug/LNDVinyl chloride SW8260B 03/17/15 17:37 / eli-b161.0ug/LNDm+p-Xylenes SW8260B 03/17/15 17:37 / eli-b160.50ug/LNDo-Xylene SW8260B 03/17/15 17:37 / eli-b160.50ug/LNDXylenes, Total SW8260B 03/17/15 17:37 / eli-b1670-130%REC88.0 Surr: 1,2-Dichloroethane-d4 SW8260B 03/17/15 17:37 / eli-b1677-126%REC95.0 Surr: Dibromofluoromethane SW8260B 03/17/15 17:37 / eli-b1676-127%REC103 Surr: p-Bromofluorobenzene SW8260B 03/17/15 17:37 / eli-b1679-122%REC95.0 Surr: Toluene-d8 SW8260B EXTRACTABLE PETROLEUM HYDROCARBONS-SCREEN ANALYSIS 03/11/15 20:30 / JRS300ug/LNDTotal Extractable Hydrocarbons SW8015M1000 03/11/15 20:30 / JRS40-140%REC76.0 Surr: o-Terphenyl SW8015M Report Definitions: RL - Analyte reporting limit.MCL - Maximum contaminant level. QCL - Quality control limit.ND - Not detected at the reporting limit. Page 7 of 35296 LABORATORY ANALYTICAL REPORT Client:Hydrometrics Inc Project:15012 East Gallatin Landfill Lab ID:H15030090-002 Client Sample ID:BCL-1503-101 Collection Date:03/05/15 10:05 Matrix:Aqueous Report Date:03/24/15 DateReceived:03/06/15 Prepared by Helena, MT Branch Analyses Result Units Analysis Date / ByRLMethod MCL/ QCLQualifiers EXTRACTABLE PETROLEUM HYDROCARBONS-SCREEN ANALYSIS - Note: Total Extractable Hydrocarbons are defined as the total hydrocarbon responses regardless of elution time. Report Definitions: RL - Analyte reporting limit.MCL - Maximum contaminant level. QCL - Quality control limit.ND - Not detected at the reporting limit. Page 8 of 35297 LABORATORY ANALYTICAL REPORT Client:Hydrometrics Inc Project:15012 East Gallatin Landfill Lab ID:H15030090-003 Client Sample ID:BCL-1503-102 Collection Date:03/05/15 10:40 Matrix:Aqueous Report Date:03/24/15 DateReceived:03/06/15 Prepared by Helena, MT Branch Analyses Result Units Analysis Date / ByRLMethod MCL/ QCLQualifiers PHYSICAL PROPERTIES H 03/06/15 15:50 / AHN0.1s.u.7.1pH A4500-H B 03/10/15 10:47 / SRW1umhos/cm885Conductivity @ 25 C A2510 B INORGANICS 03/10/15 17:03 / SRW1mg/L31Chloride E300.0 03/11/15 14:40 / SRW1mg/L29Sulfate E300.0 NUTRIENTS 03/09/15 15:51 / cmm0.01mg/LNDNitrogen, Nitrate+Nitrite as N E353.2 METALS, DISSOLVED 03/12/15 21:07 / dck0.0005mg/LNDAntimony E200.8 03/12/15 21:07 / dck0.001mg/L0.001Arsenic E200.8 03/12/15 21:07 / dck0.003mg/L0.138Barium E200.8 03/12/15 21:07 / dck0.0008mg/LNDBeryllium E200.8 03/12/15 21:07 / dck0.00003mg/LNDCadmium E200.8 03/12/15 21:07 / dck0.01mg/LNDChromium E200.8 03/12/15 21:07 / dck0.01mg/LNDCobalt E200.8 03/12/15 21:07 / dck0.002mg/LNDCopper E200.8 03/12/15 21:07 / dck0.02mg/L0.45Iron E200.8 03/12/15 21:07 / dck0.0003mg/LNDLead E200.8 03/12/15 21:07 / dck0.002mg/LNDNickel E200.8 03/12/15 21:07 / dck0.001mg/LNDSelenium E200.8 03/12/15 21:07 / dck0.0002mg/LNDSilver E200.8 03/12/15 21:07 / dck0.0002mg/LNDThallium E200.8 03/12/15 21:07 / dck0.1mg/LNDVanadium E200.8 03/12/15 21:07 / dck0.008mg/LNDZinc E200.8 VOLATILE ORGANIC COMPOUNDS 03/17/15 18:07 / eli-b1620ug/LNDAcetone SW8260B 03/17/15 18:07 / eli-b163.0ug/LNDAcrylonitrile SW8260B 03/17/15 18:07 / eli-b160.50ug/LNDBenzene SW8260B 03/17/15 18:07 / eli-b160.50ug/LNDBromochloromethane SW8260B 03/17/15 18:07 / eli-b160.50ug/LNDBromodichloromethane SW8260B 03/17/15 18:07 / eli-b160.50ug/LNDBromoform SW8260B 03/17/15 18:07 / eli-b160.50ug/LNDBromomethane SW8260B 03/17/15 18:07 / eli-b161.0ug/LNDCarbon disulfide SW8260B 03/17/15 18:07 / eli-b160.50ug/LNDCarbon tetrachloride SW8260B 03/17/15 18:07 / eli-b160.50ug/LNDChlorobenzene SW8260B 03/17/15 18:07 / eli-b160.50ug/LNDChlorodibromomethane SW8260B 03/17/15 18:07 / eli-b160.50ug/LNDChloroethane SW8260B 03/17/15 18:07 / eli-b160.50ug/LNDChloroform SW8260B 03/17/15 18:07 / eli-b160.50ug/LNDChloromethane SW8260B 03/17/15 18:07 / eli-b161.0ug/LND1,2-Dibromo-3-chloropropane SW8260B Report Definitions: RL - Analyte reporting limit.MCL - Maximum contaminant level. QCL - Quality control limit.ND - Not detected at the reporting limit. H - Analysis performed past recommended holding time. Page 9 of 35298 LABORATORY ANALYTICAL REPORT Client:Hydrometrics Inc Project:15012 East Gallatin Landfill Lab ID:H15030090-003 Client Sample ID:BCL-1503-102 Collection Date:03/05/15 10:40 Matrix:Aqueous Report Date:03/24/15 DateReceived:03/06/15 Prepared by Helena, MT Branch Analyses Result Units Analysis Date / ByRLMethod MCL/ QCLQualifiers VOLATILE ORGANIC COMPOUNDS 03/17/15 18:07 / eli-b160.50ug/LND1,2-Dibromoethane SW8260B 03/17/15 18:07 / eli-b160.50ug/LNDDibromomethane SW8260B 03/17/15 18:07 / eli-b160.50ug/LND1,2-Dichlorobenzene SW8260B 03/17/15 18:07 / eli-b160.50ug/LND1,4-Dichlorobenzene SW8260B 03/17/15 18:07 / eli-b161.0ug/LNDtrans-1,4-Dichloro-2-butene SW8260B 03/17/15 18:07 / eli-b160.50ug/LNDDichlorodifluoromethane SW8260B 03/17/15 18:07 / eli-b160.50ug/LND1,1-Dichloroethane SW8260B 03/17/15 18:07 / eli-b160.50ug/LND1,2-Dichloroethane SW8260B 03/17/15 18:07 / eli-b160.50ug/LND1,1-Dichloroethene SW8260B 03/17/15 18:07 / eli-b160.50ug/LNDcis-1,2-Dichloroethene SW8260B 03/17/15 18:07 / eli-b160.50ug/LNDtrans-1,2-Dichloroethene SW8260B 03/17/15 18:07 / eli-b160.50ug/LND1,2-Dichloropropane SW8260B 03/17/15 18:07 / eli-b160.30ug/LNDcis-1,3-Dichloropropene SW8260B 03/17/15 18:07 / eli-b160.30ug/LNDtrans-1,3-Dichloropropene SW8260B 03/17/15 18:07 / eli-b160.50ug/LNDEthylbenzene SW8260B 03/17/15 18:07 / eli-b1620ug/LND2-Hexanone SW8260B 03/17/15 18:07 / eli-b161.0ug/LNDIodomethane SW8260B 03/17/15 18:07 / eli-b1620ug/LNDMethyl ethyl ketone SW8260B 03/17/15 18:07 / eli-b1620ug/LNDMethyl isobutyl ketone SW8260B 03/17/15 18:07 / eli-b160.50ug/LNDMethylene chloride SW8260B 03/17/15 18:07 / eli-b160.50ug/LNDStyrene SW8260B 03/17/15 18:07 / eli-b160.50ug/LND1,1,1,2-Tetrachloroethane SW8260B 03/17/15 18:07 / eli-b160.50ug/LND1,1,2,2-Tetrachloroethane SW8260B 03/17/15 18:07 / eli-b160.50ug/LNDTetrachloroethene SW8260B 03/17/15 18:07 / eli-b160.50ug/LNDToluene SW8260B 03/17/15 18:07 / eli-b160.50ug/LND1,1,1-Trichloroethane SW8260B 03/17/15 18:07 / eli-b160.50ug/LND1,1,2-Trichloroethane SW8260B 03/17/15 18:07 / eli-b160.50ug/LNDTrichloroethene SW8260B 03/17/15 18:07 / eli-b160.50ug/LNDTrichlorofluoromethane SW8260B 03/17/15 18:07 / eli-b160.50ug/LND1,2,3-Trichloropropane SW8260B 03/17/15 18:07 / eli-b161.0ug/LNDVinyl acetate SW8260B 03/17/15 18:07 / eli-b160.40ug/L0.66Vinyl chloride SW8260B 03/17/15 18:07 / eli-b161.0ug/LNDm+p-Xylenes SW8260B 03/17/15 18:07 / eli-b160.50ug/LNDo-Xylene SW8260B 03/17/15 18:07 / eli-b160.50ug/LNDXylenes, Total SW8260B 03/17/15 18:07 / eli-b1670-130%REC94.0 Surr: 1,2-Dichloroethane-d4 SW8260B 03/17/15 18:07 / eli-b1677-126%REC99.0 Surr: Dibromofluoromethane SW8260B 03/17/15 18:07 / eli-b1676-127%REC95.0 Surr: p-Bromofluorobenzene SW8260B 03/17/15 18:07 / eli-b1679-122%REC98.0 Surr: Toluene-d8 SW8260B EXTRACTABLE PETROLEUM HYDROCARBONS-SCREEN ANALYSIS 03/11/15 21:17 / JRS300ug/LNDTotal Extractable Hydrocarbons SW8015M1000 03/11/15 21:17 / JRS40-140%REC79.0 Surr: o-Terphenyl SW8015M Report Definitions: RL - Analyte reporting limit.MCL - Maximum contaminant level. QCL - Quality control limit.ND - Not detected at the reporting limit. Page 10 of 35299 LABORATORY ANALYTICAL REPORT Client:Hydrometrics Inc Project:15012 East Gallatin Landfill Lab ID:H15030090-003 Client Sample ID:BCL-1503-102 Collection Date:03/05/15 10:40 Matrix:Aqueous Report Date:03/24/15 DateReceived:03/06/15 Prepared by Helena, MT Branch Analyses Result Units Analysis Date / ByRLMethod MCL/ QCLQualifiers EXTRACTABLE PETROLEUM HYDROCARBONS-SCREEN ANALYSIS - Note: Total Extractable Hydrocarbons are defined as the total hydrocarbon responses regardless of elution time. Report Definitions: RL - Analyte reporting limit.MCL - Maximum contaminant level. QCL - Quality control limit.ND - Not detected at the reporting limit. Page 11 of 35300 LABORATORY ANALYTICAL REPORT Client:Hydrometrics Inc Project:15012 East Gallatin Landfill Lab ID:H15030090-004 Client Sample ID:TB 4686 Collection Date:03/05/15 09:50 Matrix:Trip Blank Report Date:03/24/15 DateReceived:03/06/15 Prepared by Helena, MT Branch Analyses Result Units Analysis Date / ByRLMethod MCL/ QCLQualifiers VOLATILE ORGANIC COMPOUNDS 03/17/15 18:36 / eli-b1620ug/LNDAcetone SW8260B 03/17/15 18:36 / eli-b163.0ug/LNDAcrylonitrile SW8260B 03/17/15 18:36 / eli-b160.50ug/LNDBenzene SW8260B 03/17/15 18:36 / eli-b160.50ug/LNDBromochloromethane SW8260B 03/17/15 18:36 / eli-b160.50ug/LNDBromodichloromethane SW8260B 03/17/15 18:36 / eli-b160.50ug/LNDBromoform SW8260B 03/17/15 18:36 / eli-b160.50ug/LNDBromomethane SW8260B 03/17/15 18:36 / eli-b161.0ug/LNDCarbon disulfide SW8260B 03/17/15 18:36 / eli-b160.50ug/LNDCarbon tetrachloride SW8260B 03/17/15 18:36 / eli-b160.50ug/LNDChlorobenzene SW8260B 03/17/15 18:36 / eli-b160.50ug/LNDChlorodibromomethane SW8260B 03/17/15 18:36 / eli-b160.50ug/LNDChloroethane SW8260B 03/17/15 18:36 / eli-b160.50ug/LNDChloroform SW8260B 03/17/15 18:36 / eli-b160.50ug/LNDChloromethane SW8260B 03/17/15 18:36 / eli-b161.0ug/LND1,2-Dibromo-3-chloropropane SW8260B 03/17/15 18:36 / eli-b160.50ug/LND1,2-Dibromoethane SW8260B 03/17/15 18:36 / eli-b160.50ug/LNDDibromomethane SW8260B 03/17/15 18:36 / eli-b160.50ug/LND1,2-Dichlorobenzene SW8260B 03/17/15 18:36 / eli-b160.50ug/LND1,4-Dichlorobenzene SW8260B 03/17/15 18:36 / eli-b161.0ug/LNDtrans-1,4-Dichloro-2-butene SW8260B 03/17/15 18:36 / eli-b160.50ug/LNDDichlorodifluoromethane SW8260B 03/17/15 18:36 / eli-b160.50ug/LND1,1-Dichloroethane SW8260B 03/17/15 18:36 / eli-b160.50ug/LND1,2-Dichloroethane SW8260B 03/17/15 18:36 / eli-b160.50ug/LND1,1-Dichloroethene SW8260B 03/17/15 18:36 / eli-b160.50ug/LNDcis-1,2-Dichloroethene SW8260B 03/17/15 18:36 / eli-b160.50ug/LNDtrans-1,2-Dichloroethene SW8260B 03/17/15 18:36 / eli-b160.50ug/LND1,2-Dichloropropane SW8260B 03/17/15 18:36 / eli-b160.30ug/LNDcis-1,3-Dichloropropene SW8260B 03/17/15 18:36 / eli-b160.30ug/LNDtrans-1,3-Dichloropropene SW8260B 03/17/15 18:36 / eli-b160.50ug/LNDEthylbenzene SW8260B 03/17/15 18:36 / eli-b1620ug/LND2-Hexanone SW8260B 03/17/15 18:36 / eli-b161.0ug/LNDIodomethane SW8260B 03/17/15 18:36 / eli-b1620ug/LNDMethyl ethyl ketone SW8260B 03/17/15 18:36 / eli-b1620ug/LNDMethyl isobutyl ketone SW8260B 03/17/15 18:36 / eli-b160.50ug/LNDMethylene chloride SW8260B 03/17/15 18:36 / eli-b160.50ug/LNDStyrene SW8260B 03/17/15 18:36 / eli-b160.50ug/LND1,1,1,2-Tetrachloroethane SW8260B 03/17/15 18:36 / eli-b160.50ug/LND1,1,2,2-Tetrachloroethane SW8260B 03/17/15 18:36 / eli-b160.50ug/LNDTetrachloroethene SW8260B 03/17/15 18:36 / eli-b160.50ug/LNDToluene SW8260B 03/17/15 18:36 / eli-b160.50ug/LND1,1,1-Trichloroethane SW8260B 03/17/15 18:36 / eli-b160.50ug/LND1,1,2-Trichloroethane SW8260B 03/17/15 18:36 / eli-b160.50ug/LNDTrichloroethene SW8260B Report Definitions: RL - Analyte reporting limit.MCL - Maximum contaminant level. QCL - Quality control limit.ND - Not detected at the reporting limit. Page 12 of 35301 LABORATORY ANALYTICAL REPORT Client:Hydrometrics Inc Project:15012 East Gallatin Landfill Lab ID:H15030090-004 Client Sample ID:TB 4686 Collection Date:03/05/15 09:50 Matrix:Trip Blank Report Date:03/24/15 DateReceived:03/06/15 Prepared by Helena, MT Branch Analyses Result Units Analysis Date / ByRLMethod MCL/ QCLQualifiers VOLATILE ORGANIC COMPOUNDS 03/17/15 18:36 / eli-b160.50ug/LNDTrichlorofluoromethane SW8260B 03/17/15 18:36 / eli-b160.50ug/LND1,2,3-Trichloropropane SW8260B 03/17/15 18:36 / eli-b161.0ug/LNDVinyl acetate SW8260B 03/17/15 18:36 / eli-b160.40ug/LNDVinyl chloride SW8260B 03/17/15 18:36 / eli-b161.0ug/LNDm+p-Xylenes SW8260B 03/17/15 18:36 / eli-b160.50ug/LNDo-Xylene SW8260B 03/17/15 18:36 / eli-b160.50ug/LNDXylenes, Total SW8260B 03/17/15 18:36 / eli-b1670-130%REC94.0 Surr: 1,2-Dichloroethane-d4 SW8260B 03/17/15 18:36 / eli-b1677-126%REC94.0 Surr: Dibromofluoromethane SW8260B 03/17/15 18:36 / eli-b1676-127%REC96.0 Surr: p-Bromofluorobenzene SW8260B 03/17/15 18:36 / eli-b1679-122%REC107 Surr: Toluene-d8 SW8260B Report Definitions: RL - Analyte reporting limit.MCL - Maximum contaminant level. QCL - Quality control limit.ND - Not detected at the reporting limit. Page 13 of 35302 Project:15012 East Gallatin Landfill Client:Hydrometrics Inc Work Order:H15030090 QA/QC Summary Report 03/24/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits QualCount Prepared by Helena, MT Branch Method:A2510 B Batch: R104644 Lab ID:SC 150 03/10/15 09:33Initial Calibration Verification Standard Run: PHSC_101-H_150310A Conductivity @ 25 C 104 90 1101.0156umhos/cm Lab ID:SC 5000 03/10/15 09:35Initial Calibration Verification Standard Run: PHSC_101-H_150310A Conductivity @ 25 C 102 90 1101.05090umhos/cm Lab ID:SC 20000 03/10/15 09:37Initial Calibration Verification Standard Run: PHSC_101-H_150310A Conductivity @ 25 C 102 90 1101.020400umhos/cm Lab ID:SC 2ND 1000 03/10/15 09:40Laboratory Control Sample Run: PHSC_101-H_150310A Conductivity @ 25 C 102 90 1101.01020umhos/cm Lab ID:H15030095-002ADUP 03/10/15 10:54Sample Duplicate Run: PHSC_101-H_150310A Conductivity @ 25 C 101.0 0.02100umhos/cm Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 14 of 35303 Project:15012 East Gallatin Landfill Client:Hydrometrics Inc Work Order:H15030090 QA/QC Summary Report 03/24/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits QualCount Prepared by Helena, MT Branch Method:A4500-H B Analytical Run: PHSC_101-H_150306A Lab ID:pH 7 03/06/15 08:28Initial Calibration Verification Standard pH 100 98 1020.17.0 s.u. Lab ID:CCV - pH 7 03/06/15 12:34Continuing Calibration Verification Standard pH 100 98 1020.17.0 s.u. Method:A4500-H B Batch: R104603 Lab ID:H15030087-001ADUP 03/06/15 12:17Sample Duplicate Run: PHSC_101-H_150306A pH 30.1 0.18.5 s.u. Lab ID:H15030091-001ADUP 03/06/15 15:55Sample Duplicate Run: PHSC_101-H_150306A pH 30.1 0.07.7 s.u. Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 15 of 35304 Project:15012 East Gallatin Landfill Client:Hydrometrics Inc Work Order:H15030090 QA/QC Summary Report 03/24/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits QualCount Prepared by Helena, MT Branch Method:E200.8 Analytical Run: ICPMS204-B_150312B Lab ID:ICV STD 03/12/15 11:50Initial Calibration Verification Standard16 Antimony 98 90 1100.0500.0586 mg/L Arsenic 100 90 1100.00500.0597 mg/L Barium 99 90 1100.100.0592 mg/L Beryllium 98 90 1100.00100.0293 mg/L Cadmium 103 90 1100.00100.0310 mg/L Chromium 100 90 1100.0100.0600 mg/L Cobalt 101 90 1100.0100.0604 mg/L Copper 103 90 1100.0100.0619 mg/L Iron 109 90 1100.0200.327 mg/L Lead 99 90 1100.0100.0595 mg/L Nickel 101 90 1100.0100.0607 mg/L Selenium 98 90 1100.00500.0588 mg/L Silver 95 90 1100.00500.0285 mg/L Thallium 96 90 1100.100.0576 mg/L Vanadium 97 90 1100.100.0585 mg/L Zinc 101 90 1100.0100.0604 mg/L Lab ID:ICSA 03/12/15 11:55Interference Check Sample A16 Antimony 0.0507.60E-05 mg/L Arsenic 0.00504.10E-05 mg/L Barium 0.100.000104 mg/L Beryllium 0.0010-4.00E-06 mg/L Cadmium 0.00100.000706 mg/L Chromium 0.0100.00109 mg/L Cobalt 0.0100.000218 mg/L Copper 0.0100.000655 mg/L Iron 102 70 1300.020102mg/L Lead 0.0100.000241 mg/L Nickel 0.0100.000609 mg/L Selenium 0.00500.000374 mg/L Silver 0.00500.000119 mg/L Thallium 0.102.20E-05 mg/L Vanadium 0.100.000154 mg/L Zinc 0.0100.00102 mg/L Lab ID:ICSAB 03/12/15 11:59Interference Check Sample AB16 Antimony 0 00.0504.50E-05 mg/L Arsenic 107 70 1300.00500.0107 mg/L Barium 0 00.100.000119 mg/L Beryllium 0 00.0010-4.00E-06 mg/L Cadmium 108 70 1300.00100.0108 mg/L Chromium 109 70 1300.0100.0218 mg/L Cobalt 103 70 1300.0100.0205 mg/L Copper 104 70 1300.0100.0209 mg/L Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 16 of 35305 Project:15012 East Gallatin Landfill Client:Hydrometrics Inc Work Order:H15030090 QA/QC Summary Report 03/24/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits QualCount Prepared by Helena, MT Branch Method:E200.8 Analytical Run: ICPMS204-B_150312B Lab ID:ICSAB 03/12/15 11:59Interference Check Sample AB16 Iron 104 70 1300.020104mg/L Lead 0 00.0100.000233 mg/L Nickel 106 70 1300.0100.0212 mg/L Selenium 111 70 1300.00500.0111 mg/L Silver 95 70 1300.00500.0189 mg/L Thallium 0 00.104.00E-06 mg/L Vanadium 105 70 1300.100.0211 mg/L Zinc 112 70 1300.0100.0112 mg/L Method:E200.8 Batch: R104741 Lab ID:ICB 03/12/15 13:52Method Blank Run: ICPMS204-B_150312B16 Antimony 1E-05NDmg/L Arsenic 3E-05NDmg/L Barium 3E-05NDmg/L Beryllium 2E-05NDmg/L Cadmium 6E-06NDmg/L Chromium 3E-05NDmg/L Cobalt 2E-05NDmg/L Copper 3E-050.0003 mg/L Iron 0.0002NDmg/L Lead 8E-06NDmg/L Nickel 6E-05NDmg/L Selenium 7E-05NDmg/L Silver 3E-05NDmg/L Thallium 1E-05NDmg/L Vanadium 3E-05NDmg/L Zinc 0.00030.0003 mg/L Lab ID:LFB 03/12/15 13:56Laboratory Fortified Blank Run: ICPMS204-B_150312B16 Antimony 97 85 1150.0500.0487 mg/L Arsenic 98 85 1150.00500.0488 mg/L Barium 100 85 1150.100.0501 mg/L Beryllium 97 85 1150.00100.0484 mg/L Cadmium 102 85 1150.00100.0509 mg/L Chromium 101 85 1150.0100.0504 mg/L Cobalt 99 85 1150.0100.0496 mg/L Copper 101 85 1150.0100.0510 mg/L Iron 107 85 1150.0200.161 mg/L Lead 100 85 1150.0100.0498 mg/L Nickel 101 85 1150.0100.0507 mg/L Selenium 97 85 1150.00500.0486 mg/L Silver 100 85 1150.00500.0199 mg/L Thallium 96 85 1150.100.0480 mg/L Vanadium 98 85 1150.100.0490 mg/L Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 17 of 35306 Project:15012 East Gallatin Landfill Client:Hydrometrics Inc Work Order:H15030090 QA/QC Summary Report 03/24/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits QualCount Prepared by Helena, MT Branch Method:E200.8 Batch: R104741 Lab ID:LFB 03/12/15 13:56Laboratory Fortified Blank Run: ICPMS204-B_150312B16 Zinc 104 85 1150.0100.0524 mg/L Lab ID:H15030082-005CMS 03/12/15 20:41Sample Matrix Spike Run: ICPMS204-B_150312B16 Antimony 99 70 1300.00100.0500 mg/L Arsenic 109 70 1300.00100.0605 mg/L Barium 70 1300.0500.475 mg/L A Beryllium 95 70 1300.00100.0476 mg/L Cadmium 91 70 1300.00100.0457 mg/L Chromium 99 70 1300.00500.0496 mg/L Cobalt 97 70 1300.00500.0494 mg/L Copper 95 70 1300.00500.0513 mg/L Iron 107 70 1300.0200.284 mg/L Lead 101 70 1300.00100.0505 mg/L Nickel 94 70 1300.00500.0526 mg/L Selenium 115 70 1300.00100.0575 mg/L Silver 72 70 1300.00100.0144 mg/L Thallium 98 70 1300.000500.0488 mg/L Vanadium 102 70 1300.0100.0529 mg/L Zinc 96 70 1300.0100.146 mg/L Lab ID:H15030082-005CMSD 03/12/15 20:45Sample Matrix Spike Duplicate Run: ICPMS204-B_150312B16 Antimony 99 70 130 200.0010 0.10.0500 mg/L Arsenic 109 70 130 200.0010 0.50.0602 mg/L Barium 70 130 200.050 1.20.470 mg/L A Beryllium 96 70 130 200.0010 0.60.0479 mg/L Cadmium 90 70 130 200.0010 1.50.0451 mg/L Chromium 99 70 130 200.0050 0.50.0498 mg/L Cobalt 96 70 130 200.0050 1.10.0489 mg/L Copper 95 70 130 200.0050 0.40.0515 mg/L Iron 107 70 130 200.020 0.40.285 mg/L Lead 101 70 130 200.0010 0.30.0507 mg/L Nickel 95 70 130 200.0050 0.70.0530 mg/L Selenium 114 70 130 200.0010 0.80.0570 mg/L Silver 71 70 130 200.0010 1.80.0142 mg/L Thallium 98 70 130 200.00050 0.10.0488 mg/L Vanadium 102 70 130 200.010 0.30.0527 mg/L Zinc 93 70 130 200.010 1.30.145 mg/L Qualifiers: RL - Analyte reporting limit.A - The analyte level was greater than four times the spike level. In accordance with the method % recovery is not calculated. ND - Not detected at the reporting limit. Page 18 of 35307 Project:15012 East Gallatin Landfill Client:Hydrometrics Inc Work Order:H15030090 QA/QC Summary Report 03/24/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits QualCount Prepared by Helena, MT Branch Method:E300.0 Analytical Run: IC102-H_150310A Lab ID:ICV 03/10/15 11:18Initial Calibration Verification Standard Chloride 102 90 1101.0102mg/L Lab ID:CCV031015-1 03/10/15 12:03Continuing Calibration Verification Standard Chloride 102 90 1101.0102mg/L Lab ID:CCV031015-2 03/10/15 16:07Continuing Calibration Verification Standard Chloride 101 90 1101.0101mg/L Method:E300.0 Batch: R104675 Lab ID:ICB 03/10/15 11:30Method Blank Run: IC102-H_150310A Chloride 0.0100.9 mg/L Lab ID:LFB 03/10/15 11:41Laboratory Fortified Blank Run: IC102-H_150310A Chloride 94 90 1101.047.8 mg/L Lab ID:H15030090-002AMS 03/10/15 16:41Sample Matrix Spike Run: IC102-H_150310A Chloride 100 90 1101.078.1 mg/L Lab ID:H15030090-002AMSD 03/10/15 16:52Sample Matrix Spike Duplicate Run: IC102-H_150310A Chloride 103 90 110 201.0 2.179.8 mg/L Method:E300.0 Analytical Run: IC102-H_150311A Lab ID:ICV 03/11/15 11:53Initial Calibration Verification Standard Sulfate 102 90 1101.0408mg/L Lab ID:CCV031115-1 03/11/15 12:16Continuing Calibration Verification Standard Sulfate 102 90 1101.0410mg/L Method:E300.0 Batch: R104717 Lab ID:ICB 03/11/15 11:42Method Blank Run: IC102-H_150311A Sulfate 0.009NDmg/L Lab ID:LFB 03/11/15 12:04Laboratory Fortified Blank Run: IC102-H_150311A Sulfate 97 90 1101.0195mg/L Lab ID:H15030088-001AMS 03/11/15 13:22Sample Matrix Spike Run: IC102-H_150311A Sulfate 101 90 1101.0204mg/L Lab ID:H15030088-001AMSD 03/11/15 13:33Sample Matrix Spike Duplicate Run: IC102-H_150311A Sulfate 101 90 110 201.0 0.4205mg/L Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 19 of 35308 Project:15012 East Gallatin Landfill Client:Hydrometrics Inc Work Order:H15030090 QA/QC Summary Report 03/24/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits QualCount Prepared by Helena, MT Branch Method:E353.2 Analytical Run: FIA203-HE_150309B Lab ID:ICV 03/09/15 15:08Initial Calibration Verification Standard Nitrogen, Nitrate+Nitrite as N 101 90 1100.0101.01 mg/L Lab ID:ICB 03/09/15 15:11Initial Calibration Blank, Instrument Blank Nitrogen, Nitrate+Nitrite as N 0 00.010-0.0285 mg/L Lab ID:CCV 03/09/15 15:32Continuing Calibration Verification Standard Nitrogen, Nitrate+Nitrite as N 109 90 1100.0100.544 mg/L Lab ID:CCV 03/09/15 15:49Continuing Calibration Verification Standard Nitrogen, Nitrate+Nitrite as N 109 90 1100.0100.545 mg/L Method:E353.2 Batch: R104641 Lab ID:LFB 03/09/15 15:09Laboratory Fortified Blank Run: FIA203-HE_150309B Nitrogen, Nitrate+Nitrite as N 102 90 1100.0111.02 mg/L Lab ID:MBLK 03/09/15 15:14Method Blank Run: FIA203-HE_150309B Nitrogen, Nitrate+Nitrite as N 0.003NDmg/L Lab ID:H15030088-001CMS 03/09/15 15:37Sample Matrix Spike Run: FIA203-HE_150309B Nitrogen, Nitrate+Nitrite as N 91 90 1100.0111.20 mg/L Lab ID:H15030088-001CMSD 03/09/15 15:39Sample Matrix Spike Duplicate Run: FIA203-HE_150309B Nitrogen, Nitrate+Nitrite as N 93 90 110 200.011 1.61.22 mg/L Lab ID:H15030090-003BMS 03/09/15 15:52Sample Matrix Spike Run: FIA203-HE_150309B Nitrogen, Nitrate+Nitrite as N 100 90 1100.0110.995 mg/L Lab ID:H15030090-003BMSD 03/09/15 15:53Sample Matrix Spike Duplicate Run: FIA203-HE_150309B Nitrogen, Nitrate+Nitrite as N 95 90 110 200.011 5.10.946 mg/L Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 20 of 35309 Project:15012 East Gallatin Landfill Client:Hydrometrics Inc Work Order:H15030090 QA/QC Summary Report 03/24/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits QualCount Prepared by Helena, MT Branch Method:SW8015M Batch: 28352 Lab ID:MB-28352 03/11/15 17:21Method Blank Run: HHP2_150311A2 Total Extractable Hydrocarbons 300NDug/L Surr: o-Terphenyl 77 40 140 Lab ID:LCS-28352 03/11/15 18:08Laboratory Control Sample Run: HHP2_150311A2 Total Extractable Hydrocarbons 85 60 1403005290ug/L Surr: o-Terphenyl 84 40 140 Lab ID:H15030090-003EMS 03/11/15 22:04Sample Matrix Spike Run: HHP2_150311A2 Total Extractable Hydrocarbons 77 60 1406009550ug/L Surr: o-Terphenyl 78 40 140 Lab ID:H15030090-003EMSD 03/11/15 22:51Sample Matrix Spike Duplicate Run: HHP2_150311A2 Total Extractable Hydrocarbons 81 60 140 206005.510100ug/L Surr: o-Terphenyl 81 40 140 Method:SW8015M Analytical Run: R104723 Lab ID:CCV_0311GC402r-W 03/11/15 16:33Continuing Calibration Verification Standard15 n-Nonane 92 75 125183ug/L n-Decane 90 75 125181ug/L n-Dodecane 91 75 125181ug/L n-Tetradecane 91 75 125183ug/L n-Hexadecane 90 75 125179ug/L n-Octadecane 90 75 125179ug/L n-Nonadecane 89 75 125179ug/L n-Eicosane 90 75 125179ug/L n-Docosane 89 75 125178ug/L n-Tetracosane 89 75 125179ug/L n-Hexacosane 90 75 125179ug/L n-Octacosane 90 75 125179ug/L n-Triacontane 89 75 125177ug/L n-Hexatriacontane 85 75 125171ug/L Surr: o-Terphenyl 89 75 125 Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 21 of 35310 Project:15012 East Gallatin Landfill Client:Hydrometrics Inc Work Order:H15030090 QA/QC Summary Report 03/24/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits QualCount Prepared by Helena, MT Branch Method:SW8260B Batch: B_R239905 Lab ID:lcs031715 03/17/15 10:14Laboratory Control Sample Run: SUB-B23990554 trans-1,4-Dichloro-2-butene 96 50 1421.04.80 ug/L Acetone 121 62 1302060.4 ug/L Acrylonitrile 87 60 1302043.6 ug/L Benzene 100 71 1331.05.00 ug/L Bromochloromethane 98 68 1311.04.88 ug/L Bromodichloromethane 98 67 1381.04.88 ug/L Bromoform 102 64 1361.05.12 ug/L Bromomethane 96 60 1381.04.80 ug/L Carbon disulfide 96 46 1451.04.80 ug/L Carbon tetrachloride 107 61 1441.05.36 ug/L Chlorobenzene 99 78 1361.04.96 ug/L Chlorodibromomethane 102 72 1361.05.08 ug/L Chloroethane 98 64 1361.04.88 ug/L Chloroform 101 69 1331.05.04 ug/L Chloromethane 94 63 1491.04.72 ug/L 1,2-Dibromo-3-chloropropane 107 63 1251.05.36 ug/L 1,2-Dibromoethane 98 75 1311.04.92 ug/L Dibromomethane 94 72 1331.04.68 ug/L 1,2-Dichlorobenzene 108 78 1291.05.40 ug/L 1,4-Dichlorobenzene 108 78 1311.05.40 ug/L Dichlorodifluoromethane 106 55 1411.05.32 ug/L 1,1-Dichloroethane 98 72 1301.04.88 ug/L 1,2-Dichloroethane 98 57 1461.04.88 ug/L 1,1-Dichloroethene 106 66 1421.05.28 ug/L cis-1,2-Dichloroethene 105 74 1331.05.24 ug/L trans-1,2-Dichloroethene 107 76 1381.05.36 ug/L 1,2-Dichloropropane 90 72 1351.04.52 ug/L cis-1,3-Dichloropropene 98 75 1321.04.88 ug/L trans-1,3-Dichloropropene 104 77 1451.05.20 ug/L Ethylbenzene 101 78 1311.05.04 ug/L 2-Hexanone 99 72 1312049.6 ug/L Iodomethane 98 66 1321.04.88 ug/L Methyl ethyl ketone 101 55 1452050.4 ug/L Methyl isobutyl ketone 94 73 1292046.8 ug/L Methylene chloride 92 73 1261.04.60 ug/L Styrene 105 76 1341.05.24 ug/L 1,1,1,2-Tetrachloroethane 100 75 1351.05.00 ug/L 1,1,2,2-Tetrachloroethane 102 72 1321.05.12 ug/L Tetrachloroethene 103 78 1371.05.16 ug/L Toluene 102 78 1341.05.12 ug/L 1,1,1-Trichloroethane 110 64 1411.05.48 ug/L 1,1,2-Trichloroethane 94 72 1331.04.72 ug/L Trichloroethene 97 75 1381.04.84 ug/L Trichlorofluoromethane 107 58 1391.05.36 ug/L Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 22 of 35311 Project:15012 East Gallatin Landfill Client:Hydrometrics Inc Work Order:H15030090 QA/QC Summary Report 03/24/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits QualCount Prepared by Helena, MT Branch Method:SW8260B Batch: B_R239905 Lab ID:lcs031715 03/17/15 10:14Laboratory Control Sample Run: SUB-B23990554 1,2,3-Trichloropropane 104 67 1331.05.20 ug/L Vinyl acetate 90 31 1241.04.48 ug/L Vinyl chloride 96 66 1401.04.80 ug/L m+p-Xylenes 102 78 1331.010.2 ug/L o-Xylene 103 79 1361.05.16 ug/L Xylenes, Total 103 78 1361.015.4 ug/L Surr: 1,2-Dichloroethane-d4 94 70 1301.0 Surr: Dibromofluoromethane 98 77 1261.0 Surr: p-Bromofluorobenzene 99 76 1271.0 Surr: Toluene-d8 95 79 1221.0 Lab ID:blk031715 03/17/15 11:13Method Blank Run: SUB-B23990554 trans-1,4-Dichloro-2-butene 1.0NDug/L Acetone 20NDug/L Acrylonitrile 3.0NDug/L Benzene 1.0NDug/L Bromochloromethane 1.0NDug/L Bromodichloromethane 1.0NDug/L Bromoform 1.0NDug/L Bromomethane 1.0NDug/L Carbon disulfide 1.0NDug/L Carbon tetrachloride 1.0NDug/L Chlorobenzene 1.0NDug/L Chlorodibromomethane 1.0NDug/L Chloroethane 1.0NDug/L Chloroform 1.0NDug/L Chloromethane 1.0NDug/L 1,2-Dibromo-3-chloropropane 1.0NDug/L 1,2-Dibromoethane 1.0NDug/L Dibromomethane 1.0NDug/L 1,2-Dichlorobenzene 1.0NDug/L 1,4-Dichlorobenzene 1.0NDug/L Dichlorodifluoromethane 1.0NDug/L 1,1-Dichloroethane 1.0NDug/L 1,2-Dichloroethane 1.0NDug/L 1,1-Dichloroethene 1.0NDug/L cis-1,2-Dichloroethene 1.0NDug/L trans-1,2-Dichloroethene 1.0NDug/L 1,2-Dichloropropane 1.0NDug/L cis-1,3-Dichloropropene 0.30NDug/L trans-1,3-Dichloropropene 0.30NDug/L Ethylbenzene 1.0NDug/L 2-Hexanone 20NDug/L Iodomethane 1.0NDug/L Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 23 of 35312 Project:15012 East Gallatin Landfill Client:Hydrometrics Inc Work Order:H15030090 QA/QC Summary Report 03/24/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits QualCount Prepared by Helena, MT Branch Method:SW8260B Batch: B_R239905 Lab ID:blk031715 03/17/15 11:13Method Blank Run: SUB-B23990554 Methyl ethyl ketone 20NDug/L Methyl isobutyl ketone 20NDug/L Methylene chloride 1.0NDug/L Styrene 1.0NDug/L 1,1,1,2-Tetrachloroethane 1.0NDug/L 1,1,2,2-Tetrachloroethane 1.0NDug/L Tetrachloroethene 1.0NDug/L Toluene 1.0NDug/L 1,1,1-Trichloroethane 1.0NDug/L 1,1,2-Trichloroethane 1.0NDug/L Trichloroethene 1.0NDug/L Trichlorofluoromethane 1.0NDug/L 1,2,3-Trichloropropane 1.0NDug/L Vinyl acetate 1.0NDug/L Vinyl chloride 0.40NDug/L m+p-Xylenes 1.0NDug/L o-Xylene 1.0NDug/L Xylenes, Total 1.0NDug/L Surr: 1,2-Dichloroethane-d4 94 70 1301.0 Surr: Dibromofluoromethane 97 77 1261.0 Surr: p-Bromofluorobenzene 106 76 1271.0 Surr: Toluene-d8 99 79 1221.0 Lab ID:H15030090-001D 03/17/15 20:05Sample Matrix Spike Run: SUB-B23990554 trans-1,4-Dichloro-2-butene 90 50 1421.04.48 ug/L Acetone 91 62 1302045.6 ug/L Acrylonitrile 89 60 1302044.4 ug/L Benzene 102 71 1331.05.08 ug/L Bromochloromethane 96 68 1311.04.80 ug/L Bromodichloromethane 101 67 1381.05.04 ug/L Bromoform 101 64 1361.05.04 ug/L Bromomethane 105 60 1381.05.24 ug/L Carbon disulfide 94 46 1451.04.68 ug/L Carbon tetrachloride 106 61 1441.05.28 ug/L Chlorobenzene 102 78 1361.05.12 ug/L Chlorodibromomethane 100 72 1361.05.00 ug/L Chloroethane 98 64 1361.04.88 ug/L Chloroform 98 69 1331.04.88 ug/L Chloromethane 90 63 1491.04.52 ug/L 1,2-Dibromo-3-chloropropane 116 63 1251.05.80 ug/L 1,2-Dibromoethane 98 75 1311.04.92 ug/L Dibromomethane 96 72 1331.04.80 ug/L 1,2-Dichlorobenzene 104 78 1291.05.20 ug/L 1,4-Dichlorobenzene 104 78 1311.05.20 ug/L Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 24 of 35313 Project:15012 East Gallatin Landfill Client:Hydrometrics Inc Work Order:H15030090 QA/QC Summary Report 03/24/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits QualCount Prepared by Helena, MT Branch Method:SW8260B Batch: B_R239905 Lab ID:H15030090-001D 03/17/15 20:05Sample Matrix Spike Run: SUB-B23990554 Dichlorodifluoromethane 106 55 1411.05.32 ug/L 1,1-Dichloroethane 101 72 1301.05.04 ug/L 1,2-Dichloroethane 102 57 1461.05.12 ug/L 1,1-Dichloroethene 104 66 1421.05.20 ug/L cis-1,2-Dichloroethene 100 74 1331.05.00 ug/L trans-1,2-Dichloroethene 106 76 1381.05.32 ug/L 1,2-Dichloropropane 96 72 1351.04.80 ug/L cis-1,3-Dichloropropene 102 75 1321.05.12 ug/L trans-1,3-Dichloropropene 106 77 1451.05.28 ug/L Ethylbenzene 104 78 1311.05.20 ug/L 2-Hexanone 102 72 1312050.8 ug/L Iodomethane 90 66 1321.04.52 ug/L Methyl ethyl ketone 99 55 1452049.6 ug/L Methyl isobutyl ketone 101 73 1292050.4 ug/L Methylene chloride 94 73 1261.04.72 ug/L Styrene 106 76 1341.05.28 ug/L 1,1,1,2-Tetrachloroethane 103 75 1351.05.16 ug/L 1,1,2,2-Tetrachloroethane 102 72 1321.05.12 ug/L Tetrachloroethene 106 78 1371.05.28 ug/L Toluene 104 78 1341.05.20 ug/L 1,1,1-Trichloroethane 105 64 1411.05.24 ug/L 1,1,2-Trichloroethane 96 72 1331.04.80 ug/L Trichloroethene 94 75 1381.04.68 ug/L Trichlorofluoromethane 106 58 1391.05.28 ug/L 1,2,3-Trichloropropane 99 67 1331.04.96 ug/L Vinyl acetate 93 31 1241.04.64 ug/L Vinyl chloride 94 66 1401.04.72 ug/L m+p-Xylenes 107 78 1331.010.7 ug/L o-Xylene 104 79 1361.05.20 ug/L Xylenes, Total 106 78 1361.015.9 ug/L Surr: 1,2-Dichloroethane-d4 94 70 1301.0 Surr: Dibromofluoromethane 95 77 1261.0 Surr: p-Bromofluorobenzene 101 76 1271.0 Surr: Toluene-d8 100 79 1221.0 Lab ID:H15030090-001D 03/17/15 20:35Sample Matrix Spike Duplicate Run: SUB-B23990554 trans-1,4-Dichloro-2-butene 96 50 142 201.0 6.94.80 ug/L Acetone 91 62 130 20200.045.6 ug/L Acrylonitrile 90 60 130 20201.845.2 ug/L Benzene 102 71 133 201.0 0.05.08 ug/L Bromochloromethane 97 68 131 201.0 0.84.84 ug/L Bromodichloromethane 101 67 138 201.0 0.05.04 ug/L Bromoform 100 64 136 201.0 0.85.00 ug/L Bromomethane 106 60 138 201.0 1.55.32 ug/L Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 25 of 35314 Project:15012 East Gallatin Landfill Client:Hydrometrics Inc Work Order:H15030090 QA/QC Summary Report 03/24/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits QualCount Prepared by Helena, MT Branch Method:SW8260B Batch: B_R239905 Lab ID:H15030090-001D 03/17/15 20:35Sample Matrix Spike Duplicate Run: SUB-B23990554 Carbon disulfide 96 46 145 201.0 2.54.80 ug/L Carbon tetrachloride 106 61 144 201.0 0.85.32 ug/L Chlorobenzene 103 78 136 201.0 0.85.16 ug/L Chlorodibromomethane 102 72 136 201.0 2.45.12 ug/L Chloroethane 98 64 136 201.0 0.84.92 ug/L Chloroform 99 69 133 201.0 1.64.96 ug/L Chloromethane 94 63 149 201.0 3.54.68 ug/L 1,2-Dibromo-3-chloropropane 118 63 125 201.0 1.45.88 ug/L 1,2-Dibromoethane 95 75 131 201.0 3.34.76 ug/L Dibromomethane 98 72 133 201.0 2.54.92 ug/L 1,2-Dichlorobenzene 106 78 129 201.0 1.55.28 ug/L 1,4-Dichlorobenzene 106 78 131 201.0 1.55.28 ug/L Dichlorodifluoromethane 110 55 141 201.0 3.75.52 ug/L 1,1-Dichloroethane 100 72 130 201.0 0.85.00 ug/L 1,2-Dichloroethane 96 57 146 201.0 6.54.80 ug/L 1,1-Dichloroethene 105 66 142 201.0 0.85.24 ug/L cis-1,2-Dichloroethene 104 74 133 201.0 3.95.20 ug/L trans-1,2-Dichloroethene 107 76 138 201.0 0.75.36 ug/L 1,2-Dichloropropane 98 72 135 201.0 1.74.88 ug/L cis-1,3-Dichloropropene 102 75 132 201.0 0.85.08 ug/L trans-1,3-Dichloropropene 106 77 145 201.0 0.85.32 ug/L Ethylbenzene 106 78 131 201.0 2.35.32 ug/L 2-Hexanone 98 72 131 20204.048.8 ug/L Iodomethane 99 66 132 201.0 9.34.96 ug/L Methyl ethyl ketone 101 55 145 20201.650.4 ug/L Methyl isobutyl ketone 99 73 129 20201.649.6 ug/L Methylene chloride 93 73 126 201.0 1.74.64 ug/L Styrene 106 76 134 201.0 0.85.32 ug/L 1,1,1,2-Tetrachloroethane 104 75 135 201.0 0.85.20 ug/L 1,1,2,2-Tetrachloroethane 103 72 132 201.0 0.85.16 ug/L Tetrachloroethene 107 78 137 201.0 1.55.36 ug/L Toluene 106 78 134 201.0 1.55.28 ug/L 1,1,1-Trichloroethane 106 64 141 201.0 0.85.28 ug/L 1,1,2-Trichloroethane 98 72 133 201.0 2.54.92 ug/L Trichloroethene 98 75 138 201.0 5.04.92 ug/L Trichlorofluoromethane 108 58 139 201.0 2.25.40 ug/L 1,2,3-Trichloropropane 110 67 133 201.0 10.05.48 ug/L Vinyl acetate 91 31 124 201.0 1.74.56 ug/L Vinyl chloride 98 66 140 201.0 4.14.92 ug/L m+p-Xylenes 102 78 133 201.0 5.410.2 ug/L o-Xylene 104 79 136 201.0 0.05.20 ug/L Xylenes, Total 102 78 1361.015.4 ug/L Surr: 1,2-Dichloroethane-d4 93 70 1301.0 Surr: Dibromofluoromethane 97 77 1261.0 Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 26 of 35315 Project:15012 East Gallatin Landfill Client:Hydrometrics Inc Work Order:H15030090 QA/QC Summary Report 03/24/15Report Date: Analyte Result %REC RPDLow Limit High Limit RPDLimitRLUnits QualCount Prepared by Helena, MT Branch Method:SW8260B Batch: B_R239905 Lab ID:H15030090-001D 03/17/15 20:35Sample Matrix Spike Duplicate Run: SUB-B23990554 Surr: p-Bromofluorobenzene 106 76 1271.0 Surr: Toluene-d8 99 79 1221.0 Qualifiers: RL - Analyte reporting limit.ND - Not detected at the reporting limit. Page 27 of 35316 BCL-1503-100 Batch ID: 28352 EXTRACTABLE PETROLEUM HYDROCARBONS (EPH) SCREENING ANALYSIS CHROMATOGRAM Sample Name: H15030090-001E ;0311GC4 , $HC-EPH-SCRN-W, Raw File: G:\Org\4GC\DAT\4GC031115_b\0311GC4.0006.RAW Date & Time Acquired: 3/11/2015 7:42:57 PM Method File: G:\Org\4GC\Methods\GC4_2015_Methods\SR020615A.MET Calibration File: G:\Org\4GC\Cals\GC4_2015CALS\SC020615A.CAL Sample Weight: 1.0068 Dilution: 2 S.A.: 1 Mean RF for C9 to C18 Hydrocarbons: 1811.444 Mean RF for C19 to C36 Hydrocarbons: 1848.389 Mean RF for Total Extractable Hydrocarbons: 1829.917 Rt range for Diesel Range Organics: 7.26 to 17.608 Rt range for C9 to C18 Hydrocarbons: 6.308 to 13.135 Rt range for C19 to C36 Hydrocarbons: 13.185 to 21.17 SURROGATE COMPOUND RT ACTUAL MEASURED %REC *o-Terphenyl_____________13.24 198.649 172.129 86.65 - *1-Chloro-octadecane_____14.015 198.649 174.653 87.92 - DRO Area:23269.02 DRO Amount: 25.26001 TEH Area:32337.77 TEH Amount: 35.10472 C9-C18 Area:17182.72 C9-C18 Amount: 18.84316 C19-C36 Area:7780.234 C19-C36 Amount: 8.361536 5.02 5.07 5.15 5.20 5.70 10.40 12.18 12.22 12.26 12.34 12.40 12.43 13.09 13.24 13.47 13.57 14.01 14.49 15.33 16.93 n-Nonane n-Decane n-Dodecane n-Tetradecane n-Hexadecane n-Octadecane n-Nonadecane *o-Terphenyl n-Eicosane *1-Chloro-octadecane n-Docosane n-Tetracosane n-Hexacosane n-Octacosane n-Triacontane n-Hexatriacontane G:\Org\4GC\DAT\4GC031115_b\0311GC4.0006.RAW H15030090-001E ;0311GC4 , $HC-EPH-SCRN-W, 0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 0 20 40 60 80 100 120 140 160 180 200 Page 28 of 35317 BCL-1503-101 Batch ID: 28352 EXTRACTABLE PETROLEUM HYDROCARBONS (EPH) SCREENING ANALYSIS CHROMATOGRAM Sample Name: H15030090-002E ;0311GC4 , $HC-EPH-SCRN-W, Raw File: G:\Org\4GC\DAT\4GC031115_b\0311GC4.0007.RAW Date & Time Acquired: 3/11/2015 8:30:06 PM Method File: G:\Org\4GC\Methods\GC4_2015_Methods\SR020615A.MET Calibration File: G:\Org\4GC\Cals\GC4_2015CALS\SC020615A.CAL Sample Weight: 1.0184 Dilution: 2 S.A.: 1 Mean RF for C9 to C18 Hydrocarbons: 1811.444 Mean RF for C19 to C36 Hydrocarbons: 1848.389 Mean RF for Total Extractable Hydrocarbons: 1829.917 Rt range for Diesel Range Organics: 7.26 to 17.608 Rt range for C9 to C18 Hydrocarbons: 6.308 to 13.135 Rt range for C19 to C36 Hydrocarbons: 13.185 to 21.17 SURROGATE COMPOUND RT ACTUAL MEASURED %REC *o-Terphenyl_____________13.24 196.387 148.806 75.77 - *1-Chloro-octadecane_____14.015 196.387 153.223 78.02 - DRO Area:16074.43 DRO Amount: 17.25106 TEH Area:27722.24 TEH Amount: 29.75149 C9-C18 Area:9891.567 C9-C18 Amount: 10.72388 C19-C36 Area:7213.523 C19-C36 Amount: 7.66418 5.02 5.07 5.14 5.20 5.39 5.48 5.56 5.71 10.41 12.26 13.09 13.24 14.01 14.48 16.92 17.20 n-Nonane n-Decane n-Dodecane n-Tetradecane n-Hexadecane n-Octadecane n-Nonadecane *o-Terphenyl n-Eicosane *1-Chloro-octadecane n-Docosane n-Tetracosane n-Hexacosane n-Octacosane n-Triacontane n-Hexatriacontane G:\Org\4GC\DAT\4GC031115_b\0311GC4.0007.RAW H15030090-002E ;0311GC4 , $HC-EPH-SCRN-W, 0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 0 20 40 60 80 100 120 140 160 180 200 Page 29 of 35318 BCL-1503-102 Batch ID: 28352 EXTRACTABLE PETROLEUM HYDROCARBONS (EPH) SCREENING ANALYSIS CHROMATOGRAM Sample Name: H15030090-003E ;0311GC4 , $HC-EPH-SCRN-W, Raw File: G:\Org\4GC\DAT\4GC031115_b\0311GC4.0008.RAW Date & Time Acquired: 3/11/2015 9:17:18 PM Method File: G:\Org\4GC\Methods\GC4_2015_Methods\03111508.MET Calibration File: G:\Org\4GC\Cals\GC4_2015CALS\SC020615A.CAL Sample Weight: 1.0017 Dilution: 2 S.A.: 1 Mean RF for C9 to C18 Hydrocarbons: 1811.444 Mean RF for C19 to C36 Hydrocarbons: 1848.389 Mean RF for Total Extractable Hydrocarbons: 1829.917 Rt range for Diesel Range Organics: 7.26 to 17.608 Rt range for C9 to C18 Hydrocarbons: 6.308 to 13.135 Rt range for C19 to C36 Hydrocarbons: 13.185 to 21.17 SURROGATE COMPOUND RT ACTUAL MEASURED %REC *o-Terphenyl_____________13.238 199.661 158.811 79.54 - *1-Chloro-octadecane_____14.012 199.661 161.333 80.8 - DRO Area:12811.58 DRO Amount: 13.9786 TEH Area:25812.55 TEH Amount: 28.16384 C9-C18 Area:8477.798 C9-C18 Amount: 9.344378 C19-C36 Area:5593.984 C19-C36 Amount: 6.042549 5.01 5.07 5.14 5.20 5.40 5.49 5.71 10.40 13.24 13.53 14.01 14.48 n-Nonane n-Decane n-Dodecane n-Tetradecane n-Hexadecane n-Octadecane n-Nonadecane *o-Terphenyl n-Eicosane *1-Chloro-octadecane n-Docosane n-Tetracosane n-Hexacosane n-Octacosane n-Triacontane n-Hexatriacontane G:\Org\4GC\DAT\4GC031115_b\0311GC4.0008.RAW H15030090-003E ;0311GC4 , $HC-EPH-SCRN-W, 0 2 4 6 8 10 12 14 16 18 20 22 24 26 28 30 0 20 40 60 80 100 120 140 160 180 200 Page 30 of 35319 Shipping container/cooler in good condition? Custody seals intact on all shipping container(s)/cooler(s)? Custody seals intact on all sample bottles? Chain of custody present? Chain of custody signed when relinquished and received? Chain of custody agrees with sample labels? Samples in proper container/bottle? Sample containers intact? Sufficient sample volume for indicated test? All samples received within holding time?(Exclude analyses that are considered field parameterssuch as pH, DO, Res Cl, Sulfite, Ferrous Iron, etc.) Container/Temp Blank temperature: Water - VOA vials have zero headspace? Water - pH acceptable upon receipt? Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes Yes No No No No No No No No No No No No R £ £ £ R R R R R R R R R £ £ £ £ £ £ £ £ £ £ £ Not Present Not Present Not Present £ R R No VOA vials submitted Not Applicable £ £ 0.0°C On Ice 3/6/2015Austin H. Nearpass Hand Del TLL Date Received: Received by: Login completed by: Carrier name: BL2000\rwilliams 3/10/2015 Reviewed by: Reviewed Date: Contact and Corrective Action Comments: None Temp Blank received in all shipping container(s)/cooler(s)?Yes NoR £Not Applicable £ Lab measurement of analytes considered field parameters that require analysis within 15 minutes of sampling such as pH, Dissolved Oxygen and Residual Chlorine, are qualified as being analyzed outside of recommended holding time. Solid/soil samples are reported on a wet weight basis (as received) unless specifically indicated. If moisture corrected, data units are typically noted as –dry. For agricultural and mining soil parameters/characteristics, all samples are dried and ground prior to sample analysis. Standard Reporting Procedures: Work Order Receipt Checklist Hydrometrics Inc H15030090 Page 31 of 35320 Page 32 of 35321 Page 33 of 35322 Page 34 of 35323 Page 35 of 35324 ANALYTICAL REPORT Rick Lane Hydrometrics 3020 Bozeman Ave Helena, MT 59601 Phone: E-mail: (406) 443-4150 rlane@hydrometrics.com Report Date:March 12, 2015 34-1506838Workorder: 15012/East Gallatin Landfill HLN 10565Purchase Order: Project ID: Sampling SiteReceive DateCollect DateLab IDClient Sample ID BCL-1503-200 1506838001 03/05/15 03/07/15 East Gallatin Landfi BCL-1503-201 1506838002 03/05/15 03/07/15 East Gallatin Landfi ADDRESS 960 West LeVoy Drive, Salt Lake City, Utah, 84123 USA PHONE FAX+1 801 266 7700 +1 801 268 9992 ALS GROUP USA, CORP. Page 1 of 7 Thu, 03/12/15 6:12 PM ENVREP-V4.0 325 ANALYTICAL REPORT Project Manager:Rand Potter Client:Hydrometrics, Inc. Workorder:34-1506838 Analytical Results Sample ID:03/05/2015 03/07/20151506838001Lab ID: Collected: Received: BCL-1503-200 East Gallatin Landfi Sampling Parameter:NAMatrix: Media: Air Summa 6 Liter Canister Sampling Site: Analysis:EPA TO-15, Air Analyzed:03/10/2015 23:03 Batch: Instrument ID: IVOA/2845 (HBN: 145153)Percent Solid:NA 5972-W Report Basis:Wet Preparation:Not Applicable Analyte ppb ug/m³MDL (ppb)Qual.RL (ppb)Dilution Analysis Method - EPA TO-15 0.50<0.74ND 0.15 UDichlorodifluoromethane1 0.50<0.31ND 0.15 UChloromethane1 0.50<1.0ND 0.15 UFreon 114 1 0.50<0.38ND 0.15 UVinyl chloride 1 0.50<0.33ND 0.15 U1,3-Butadiene 1 0.50<0.58ND 0.15 UBromomethane1 0.50<0.40ND 0.15 UChloroethane1 0.50<0.84ND 0.15 UFreon 11 1 0.50<1.1ND 0.15 UFreon 113 1 0.50<0.59ND 0.15 U1,1-Dichloroethene 1 0.50135.5 0.30Acetone 1 0.500.470.15 0.15 JCarbon disulfide 1 0.502.30.66 0.15Methylene chloride 1 0.50<0.59ND 0.15 Utrans-1,2-Dichloroethene 1 0.50<0.54ND 0.15 UMethyl t-butyl ether 1 0.50<0.53ND 0.15 UVinyl acetate 1 0.50<0.44ND 0.15 U2-Butanone 1 0.50<0.59ND 0.15 Ucis-1,2-Dichloroethene 1 0.50<0.61ND 0.15 U1,1-Dichloroethane 1 1.0<0.54ND 0.15 UEthyl acetate 1 0.50<0.53ND 0.15 UHexane1 0.50<0.73ND 0.15 UChloroform1 0.50175.8 0.15Tetrahydrofuran 1 0.50<0.61ND 0.15 U1,2-Dichloroethane 1 0.50<0.82ND 0.15 U1,1,1-Trichloroethane 1 0.50<0.94ND 0.15 UCarbon tetrachloride 1 0.503.51.1 0.15Benzene 1 0.50<0.52ND 0.15 UCyclohexane1 0.50<0.81ND 0.15 UTrichloroethene1 0.50<0.73ND 0.15 U1,2-Dichloropropane 1 0.50<1.0ND 0.15 UBromodichloromethane1 0.500.980.24 0.15 JHeptane1 0.50<0.68ND 0.15 Ucis-1,3-Dichloropropene 1 0.50<0.61ND 0.15 U4-Methyl-2-pentanone 1 0.50<0.68ND 0.15 Utrans-1,3-Dichloropropene 1 0.50<0.82ND 0.15 U1,1,2-Trichloroethane 1 Page 2 of 7 Thu, 03/12/15 6:12 PM ENVREP-V4.0 Results Continued on Next Page 326 ANALYTICAL REPORT Project Manager:Rand Potter Client:Hydrometrics, Inc. Workorder:34-1506838 Analytical Results Sample ID:03/05/2015 03/07/20151506838001Lab ID: Collected: Received: BCL-1503-200 East Gallatin Landfi Sampling Parameter:NAMatrix: Media: Air Summa 6 Liter Canister Sampling Site: Analysis:EPA TO-15, Air Analyzed:03/10/2015 23:03 Batch: Instrument ID: IVOA/2845 (HBN: 145153)Percent Solid:NA 5972-W Report Basis:Wet Preparation:Not Applicable Analyte ppb ug/m³MDL (ppb)Qual.RL (ppb)Dilution Analysis Method - EPA TO-15 0.5042110.15Toluene 1 1.0<1.2ND 0.30 U2-Hexanone 1 0.502.50.37 0.15 JTetrachloroethene1 0.50<1.3ND 0.15 UDibromochloromethane1 0.50<1.2ND 0.15 U1,2-Dibromoethane 1 0.50<0.69ND 0.15 UChlorobenzene1 0.50112.6 0.15Ethyl benzene 1 0.5053120.15m,p-Xylene 1 0.50184.1 0.15o-Xylene 1 0.50<0.64ND 0.15 UStyrene1 0.50<1.6ND 0.15 UBromoform1 0.50<1.0ND 0.15 U1,1,2,2-Tetrachloroethane 1 0.505.51.1 0.154-Ethyl toluene 1 0.505.61.1 0.151,3,5-Trimethylbenzene 1 0.50234.7 0.151,2,4-Trimethylbenzene 1 0.50162.7 0.151,3-Dichlorobenzene 1 0.50<0.90ND 0.15 U1,4-Dichlorobenzene 1 1.0<1.6ND 0.30 UBenzyl chloride 1 1.0<1.8ND 0.30 U1,2-Dichlorobenzene 1 1.0<2.2ND 0.30 U1,2,4-Trichlorobenzene 1 1.0<3.2ND 0.30 UHexachlorobutadiene1 NA540130NA JTotal Volatile Organics 1 Analysis:EPA TO-15, Air Analyzed:03/10/2015 23:03 Batch: Instrument ID: IVOA/2845 (HBN: 145153)Percent Solid:NA 5972-W Report Basis:Wet Preparation:Not Applicable Tentatively Identified Compound ppb Retention Time Dilution Qual. Analysis Method - EPA TO-15 J18.333.1 1Nonane J18.865.0 1Decane, 2,2-dimethyl- J18.973.1 1Limonene J19.194.8 1Hexane, 3,3-dimethyl- J19.558.5 1C11 Hydrocarbon J19.988.0 1Undecane J7.6332 1Ethanol J8.2037 1Isopropyl Alcohol Page 3 of 7 Thu, 03/12/15 6:12 PM ENVREP-V4.0 327 ANALYTICAL REPORT Project Manager:Rand Potter Client:Hydrometrics, Inc. Workorder:34-1506838 Analytical Results Sample ID:03/05/2015 03/07/20151506838002Lab ID: Collected: Received: BCL-1503-201 East Gallatin Landfi Sampling Parameter:NAMatrix: Media: Air Summa 6 Liter Canister Sampling Site: Analysis:EPA TO-15, Air Analyzed:03/10/2015 23:39 Batch: Instrument ID: IVOA/2845 (HBN: 145153)Percent Solid:NA 5972-W Report Basis:Wet Preparation:Not Applicable Analyte ppb ug/m³MDL (ppb)Qual.RL (ppb)Dilution Analysis Method - EPA TO-15 0.50<0.74ND 0.15 UDichlorodifluoromethane1 0.50<0.31ND 0.15 UChloromethane1 0.50<1.0ND 0.15 UFreon 114 1 0.50<0.38ND 0.15 UVinyl chloride 1 0.50<0.33ND 0.15 U1,3-Butadiene 1 0.50<0.58ND 0.15 UBromomethane1 0.50<0.40ND 0.15 UChloroethane1 0.50<0.84ND 0.15 UFreon 11 1 0.50<1.1ND 0.15 UFreon 113 1 0.50<0.59ND 0.15 U1,1-Dichloroethene 1 0.5026110.30Acetone 1 0.500.590.19 0.15 JCarbon disulfide 1 0.502.70.77 0.15Methylene chloride 1 0.50<0.59ND 0.15 Utrans-1,2-Dichloroethene 1 0.50<0.54ND 0.15 UMethyl t-butyl ether 1 0.50<0.53ND 0.15 UVinyl acetate 1 0.5059200.152-Butanone 1 0.50<0.59ND 0.15 Ucis-1,2-Dichloroethene 1 0.50<0.61ND 0.15 U1,1-Dichloroethane 1 1.0<0.54ND 0.15 UEthyl acetate 1 0.50<0.53ND 0.15 UHexane1 0.50<0.73ND 0.15 UChloroform1 0.5087290.15 ETetrahydrofuran1 0.50<0.61ND 0.15 U1,2-Dichloroethane 1 0.50<0.82ND 0.15 U1,1,1-Trichloroethane 1 0.50<0.94ND 0.15 UCarbon tetrachloride 1 0.504.11.3 0.15Benzene 1 0.50<0.52ND 0.15 UCyclohexane1 0.50<0.81ND 0.15 UTrichloroethene1 0.50<0.73ND 0.15 U1,2-Dichloropropane 1 0.50<1.0ND 0.15 UBromodichloromethane1 0.505.31.3 0.15Heptane 1 0.50<0.68ND 0.15 Ucis-1,3-Dichloropropene 1 0.50<0.61ND 0.15 U4-Methyl-2-pentanone 1 0.50<0.68ND 0.15 Utrans-1,3-Dichloropropene 1 0.50<0.82ND 0.15 U1,1,2-Trichloroethane 1 Page 4 of 7 Thu, 03/12/15 6:12 PM ENVREP-V4.0 Results Continued on Next Page 328 ANALYTICAL REPORT Project Manager:Rand Potter Client:Hydrometrics, Inc. Workorder:34-1506838 Analytical Results Sample ID:03/05/2015 03/07/20151506838002Lab ID: Collected: Received: BCL-1503-201 East Gallatin Landfi Sampling Parameter:NAMatrix: Media: Air Summa 6 Liter Canister Sampling Site: Analysis:EPA TO-15, Air Analyzed:03/10/2015 23:39 Batch: Instrument ID: IVOA/2845 (HBN: 145153)Percent Solid:NA 5972-W Report Basis:Wet Preparation:Not Applicable Analyte ppb ug/m³MDL (ppb)Qual.RL (ppb)Dilution Analysis Method - EPA TO-15 0.50379.9 0.15Toluene 1 1.0<1.2ND 0.30 U2-Hexanone 1 0.501.80.27 0.15 JTetrachloroethene1 0.50<1.3ND 0.15 UDibromochloromethane1 0.50<1.2ND 0.15 U1,2-Dibromoethane 1 0.50<0.69ND 0.15 UChlorobenzene1 0.50132.9 0.15Ethyl benzene 1 0.5058130.15m,p-Xylene 1 0.50214.7 0.15o-Xylene 1 0.500.640.15 0.15 JStyrene1 0.50<1.6ND 0.15 UBromoform1 0.50<1.0ND 0.15 U1,1,2,2-Tetrachloroethane 1 0.506.01.2 0.154-Ethyl toluene 1 0.506.61.3 0.151,3,5-Trimethylbenzene 1 0.50285.6 0.151,2,4-Trimethylbenzene 1 0.50325.4 0.151,3-Dichlorobenzene 1 0.50<0.90ND 0.15 U1,4-Dichlorobenzene 1 1.0<1.6ND 0.30 UBenzyl chloride 1 1.0<1.8ND 0.30 U1,2-Dichlorobenzene 1 1.0<2.2ND 0.30 U1,2,4-Trichlorobenzene 1 1.0<3.2ND 0.30 UHexachlorobutadiene1 NA550130NA JTotal Volatile Organics 1 Analysis:EPA TO-15, Air Analyzed:03/10/2015 23:39 Batch: Instrument ID: IVOA/2845 (HBN: 145153)Percent Solid:NA 5972-W Report Basis:Wet Preparation:Not Applicable Tentatively Identified Compound ppb Retention Time Dilution Qual. Analysis Method - EPA TO-15 J18.345.5 1Decane J18.864.1 1Heptane, 4-ethyl-2,2,6,6-tetramethyl- J18.974.9 1Limonene J19.184.2 1C11 Hydrocarbon J19.314.2 1Decane, 5-methyl- J19.434.4 1Nonane, 2-methyl- J19.559.2 1Hexane, 2,2,5,5-tetramethyl- J19.9819 1Undecane J7.7826 1Ethanol Page 5 of 7 Thu, 03/12/15 6:12 PM ENVREP-V4.0 Results Continued on Next Page 329 ANALYTICAL REPORT Project Manager:Rand Potter Client:Hydrometrics, Inc. Workorder:34-1506838 Analytical Results Sample ID:03/05/2015 03/07/20151506838002Lab ID: Collected: Received: BCL-1503-201 East Gallatin Landfi Sampling Parameter:NAMatrix: Media: Air Summa 6 Liter Canister Sampling Site: Analysis:EPA TO-15, Air Analyzed:03/10/2015 23:39 Batch: Instrument ID: IVOA/2845 (HBN: 145153)Percent Solid:NA 5972-W Report Basis:Wet Preparation:Not Applicable Tentatively Identified Compound ppb Retention Time Dilution Qual. Analysis Method - EPA TO-15 J8.2019 1Isopropyl Alcohol Report Authorization Analyst Peer ReviewMethod (/S/ is an electronic signature that complies with 21 CFR Part 11) EPA TO-15 /S/ Jorden Baum 03/11/2015 16:03 03/12/2015 18:03 /S/ Richard W. Wade Laboratory Contact Information (801) 266-7700 alslt.lab@ALSGlobal.com www.alsslc.com ALS Environmental 960 W Levoy Drive Salt Lake City, Utah 84123 Phone: Email: Web: Page 6 of 7 Thu, 03/12/15 6:12 PM ENVREP-V4.0 330 ANALYTICAL REPORT Project Manager:Rand Potter Client:Hydrometrics, Inc. Workorder:34-1506838 The results provided in this report relate only to the items tested. Samples were received in acceptable condition unless otherwise noted. Samples have not been blank corrected unless otherwise noted. This test report shall not be reproduced, except in full, without written approval of ALS. General Lab Comments ALS provides professional analytical services for all samples submitted. ALS is not in a position to interpret the data and assumes no responsibility for the quality of the samples submitted. All quality control samples processed with the samples in this report yielded acceptable results unless otherwise noted. ALS is accredited for specific fields of testing (scopes) in the following testing sectors. The quality system implemented at ALS conforms to accreditation requirements and is applied to all analytical testing performed by ALS. The following table lists testing sector, accreditation body, accreditation number and website. Please contact these accrediting bodies or your ALS project manager for the current scope of accreditation that applies to your analytical testing. Testing Sector Accreditation Body Certificate Number Website Environmental ACLASS (DoD ELAP) Utah (NELAC) Nevada Oklahoma Iowa Florida (TNI) ADE-1420 DATA1 UT00009 UT00009 IA# 376 E871067 http://www.aclasscorp.com http://health.utah.gov/lab/labimp/ http://ndep.nv.gov/bsdw/labservice.htm http://www.deq.state.ok.us/CSDnew/ http://www.iowadnr.gov/InsideDNR/RegulatoryWater.aspx http://www.dep.state.fl.us/labs/bars/sas/qa/ Industrial Hygiene 101574 http://www.aihaaccreditedlabs.orgAIHA (ISO 17025 & AIHA IHLAP/ELLAP) Lead Testing: CPSC ACLASS (ISO 17025, CPSC) ADE-1420 http://www.aclasscorp.com Soil, Dust, Paint ,Air AIHA (ISO 17025, AIHA ELLAP and NLLAP) 101574 http://www.aihaaccreditedlabs.org Dietary Supplements ACLASS (ISO 17025)ADE-1420 http://www.aclasscorp.com Texas (TNI)T104704456-11-1 http://www.tceq.texas.gov/field/qa/lab_accred_certif.html (Standard) MDL = Method Detection Limit, a statistical estimate of method/media/instrument sensitivity. RL = Reporting Limit, a verified value of method/media/instrument sensitivity. CRDL = Contract Required Detection Limit Reg. Limit = Regulatory Limit. ND = Not Detected, testing result not detected above the MDL or RL. < This testing result is less than the numerical value. ** No result could be reported, see sample comments for details. U = Qualifier indicates that the analyte was not detected above the MDL. J = Qualifier Indicates that the analyte value is between the MDL and the RL. It is also used to indicate an estimated value for tentatively identified compounds in mass spectrometry where a 1:1 response is assumed. B = Qualifier indicates that the analyte was detected in the blank. E = Qualifier indicates that the analyte result exceeds calibration range. P = Qualifier indicates that the RPD between the two columns is greater than 40%. Result Symbol Definitions Qualifier Symbol Definitions Page 7 of 7 Thu, 03/12/15 6:12 PM ENVREP-V4.0 331 Bozeman East Gallatin Landfill Vapor Extraction RfC * RSL** Parameter ppb μg/m3 ppb μg/m3 mg/m3 μg/m3 Acetone 3/5/2015 5.5 13 11 26 na 3200 Benzene 3/5/2015 1.1 3.5 1.3 4.1 30 3.1 Butanone, 2-3/5/2015 20 59 520 C11 Hydrocarbon 3/5/2015 8.5 4.2 Carbon disulfide 3/5/2015 0.15 0.47 0.19 0.59 700 73 Decane 3/5/2015 5.5 Decane, 2,2-dimethyl-3/5/2015 5 Decane, 5-methyl-3/5/2015 4.2 Dichlorobenzene, 1,3- 3/5/2015 2.7 16 5.4 32 Ethanol 3/5/2015 32 26 Ethyl toluene, 4-3/5/2015 1.1 5.5 1.2 6 Ethylbenzene 3/5/2015 2.6 11 2.9 13 1000 100 Heptane 3/5/2015 0.24 0.98 1.3 5.3 na Heptane, 4-ethyl-2,2,6,6-tetramethyl- 3/5/2015 4.1 Hexane, 3,3-dimethyl 3/5/2015 4.8 700*** Hexane, 2,2,5,5-tetramethyl- 3/5/2015 9.2 73 Isopropyl Alcohol 3/5/2015 37 19 Limonene 3/5/2015 3.1 4.9 Methylene Chloride 3/5/2015 0.66 2.3 0.77 2.7 90 63 Nonane 3/5/2015 3.1 Nonane, 2-methyl- 3/5/2015 4.4 Styrene 3/5/2015 0.15 0.64 1000 100 Tetrachloroethene 3/5/2015 0.37 2.5 0.27 1.8 4.2 Tetrahydrofuran 3/5/2015 5.8 17 29 87 2000 Tolulene 3/5/2015 11 42 9.9 37 5000 520 Total Volatile Organics 3/5/2015 130 540 130 550 Trimethylbenzene, 1,2,4- 3/5/2015 4.7 23 5.6 28 0.73 Trimethylbenzene, 1,3,5- 3/5/2015 1.1 5.6 1.3 6.6 Undecane 3/5/2015 8 9.2 Xylene, m,p- 3/5/2015 12 53 13 58 100**** 10 Xylene, o- 3/5/2015 4.1 18 4.7 21 10 * RfC = Reference Concentration for Chronic Inhalation Exposure from EPA's Integrated Risk Information System (IRIS) ** RSL = Regional Screening Level for Resident Ambient Air (TR=1E6, HQ=0.0=1 Nov 2104 *** fC for n-Hexane **** Xylenes Highlighted cells indicate "Tentatively Identified" parameters 200 201Sample Date 332